1.中南大学资源加工与生物工程学院,长沙,410083;
2.中南大学资源加工与生物工程学院,长沙,410083;
3.中南大学资源加工与生物工程学院，长沙 410083; 中南大学生物冶金教育部重点实验室，长沙 410083;
4.中南大学资源加工与生物工程学院，长沙 410083; 中南大学生物冶金教育部重点实验室，长沙 410083;
5.中南大学资源加工与生物工程学院，长沙 410083; 中南大学生物冶金教育部重点实验室，长沙 410083;
6.中南大学资源加工与生物工程学院，长沙 410083; 中南大学生物冶金教育部重点实验室，长沙 410083;
7.CSIRO Process Science a{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"碳纳米管用氨水、乙二胺四乙酸(EDTA)进行表面改性, 然后通过硫代乙酰胺、醋酸锌、水和表面改性的碳纳米管在水浴超声条件下发生溶液化学反应, 在碳纳米管表面包裹了一层分布均匀、致密的ZnS纳米晶粒. 用XRD、TEM、SAED、SEM、FTIR、PL等表征手段对材料进行了结构及性能表征. 研究结果表明: 对碳纳米管进行乙二胺四乙酸处理是实现ZnS纳米晶粒在碳纳米管表面均匀、致密包裹的重要因素, 碳纳米管/ZnS复合材料的光致发光性较之相同方法合成的ZnS, 俘获态发射峰蓝移6nm, 而能带边缘发射峰蓝移16nm. 通过对FTIR及不同表面改性碳纳米管的对比试验研究, 给出了碳纳米管/ZnS复合材料的形成机理.","authors":[{"authorName":"焦志辉","id":"64e3683d-a61c-44b8-a2c0-dedf4ed1168a","originalAuthorName":"焦志辉"},{"authorName":"张孝彬","id":"76ae2e76-cae6-43c6-9714-0bc8df010f56","originalAuthorName":"张孝彬"},{"authorName":"程继鹏","id":"19dfb0b8-37da-4b5a-9ba1-a7657599bb87","originalAuthorName":"程继鹏"},{"authorName":"陶新永","id":"88b0cfa4-d7b5-45aa-872f-8f91cb1f26fe","originalAuthorName":"陶新永"},{"authorName":"贺狄龙","id":"d97d7ef2-0741-4774-964e-5a5e642592d9","originalAuthorName":"贺狄龙"}],"categoryName":"|","doi":"10.3724/SP.J.1077.2008.00491","fpage":"491","id":"e673a408-bc99-4a29-b2b4-231a30531f7c","issue":"3","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"08e1eeb9-0dff-4585-8536-1e53a94fa653","keyword":"碳纳米管","originalKeyword":"碳纳米管"},{"id":"717690f7-9de6-4237-b36a-7df0ea501c24","keyword":" ZnS","originalKeyword":" ZnS"},{"id":"936cd75f-ec61-4b55-ab7b-50e15065c9d7","keyword":" coating","originalKeyword":" coating"},{"id":"1a3a7f9f-f78c-4b03-94dc-458dfeffc9f2","keyword":" photoluminescence","originalKeyword":" photoluminescence"}],"language":"zh","publisherId":"1000-324X_2008_3_7","title":"碳纳米管/ZnS复合材料的制备及其性能表征","volume":"23","year":"2008"},{"abstractinfo":"碳纳米管用氨水、乙二胺四乙酸(EDTA)进行表面改性,然后通过硫代乙酰胺,醋酸锌、水和表面改性的碳纳米管在水浴超声条件下发生溶液化学反应,在碳纳米管表面包裹了一层分布均匀、致密的ZnS纳米晶粒.用XRD,TEM,SAED、SEM,FTIR、PL等表征手段对材料进行了结构及性能表征.研究结果表明:对碳纳米管进行乙二胺四乙酸处理是实现ZnS纳米晶粒在碳纳米管表面均匀、致密包裹的重要因素,碳纳米管/ZnS复合材料的光致发光性较之相同方法合成的ZnS,俘获态发射峰蓝移6nm,而能带边缘发射峰蓝移16nm.通过对FTIR及不同表面改性碳纳米管的对比试验研究,给出了碳纳米管/ZnS复合材料的形成机理.","authors":[{"authorName":"焦志辉","id":"3b822537-d094-429d-af05-6402552d8cb6","originalAuthorName":"焦志辉"},{"authorName":"张孝彬","id":"e64c7f6e-2ce5-4e72-b7cd-8677d78dfe78","originalAuthorName":"张孝彬"},{"authorName":"程继鹏","id":"c2f65290-fe50-469c-af42-5d721ea4abdf","originalAuthorName":"程继鹏"},{"authorName":"陶新永","id":"e7c5d8ff-644c-4c59-b815-f254f0ecb1f0","originalAuthorName":"陶新永"},{"authorName":"贺狄龙","id":"15db2590-f7ff-4b0a-8f4d-ab55ab3bc3cc","originalAuthorName":"贺狄龙"}],"doi":"10.3321/j.issn:1000-324X.2008.03.015","fpage":"491","id":"6e4759d8-2cdf-4587-b081-a6d64170122b","issue":"3","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"cb7cae59-59f2-45ee-9ec0-5f94eea28642","keyword":"碳纳米管","originalKeyword":"碳纳米管"},{"id":"1ccf4681-d824-4cd7-bf26-8b7a723a8fc5","keyword":"ZnS","originalKeyword":"ZnS"},{"id":"87d43b43-5b9e-4d4e-85db-71a3fc494a6b","keyword":"包裹","originalKeyword":"包裹"},{"id":"47856924-6892-419d-886d-3b92ad09ebba","keyword":"光致发光","originalKeyword":"光致发光"}],"language":"zh","publisherId":"wjclxb200803015","title":"碳纳米管/ZnS复合材料的制备及其性能表征","volume":"23","year":"2008"},{"abstractinfo":"对干法熄焦和稳定熄焦的技术特点和优势进行了分析比较.指出:干法熄焦回收占焦炉能耗的35%～40%的红焦显热是稳定熄焦所不具备的优势;干法熄焦改善焦炭质量是稳定熄焦所无法比拟的;干法熄焦在减少对环境污染方面显著优于稳定熄焦;各国能源情况和能源价格的差异决定了这些国家选择哪一种熄焦方式.","authors":[{"authorName":"郑文华","id":"232bbd03-2f87-44fe-a2b4-3fe561fd7d72","originalAuthorName":"郑文华"},{"authorName":"张晓光","id":"b29c3448-20f9-4a6b-8f4d-bf4c0405b924","originalAuthorName":"张晓光"}],"doi":"","fpage":"70","id":"7dca7c54-37c8-4515-85ce-b6739323c608","issue":"11","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"c5065eb8-8d4b-4374-a68a-f940e8d650be","keyword":"干法熄焦","originalKeyword":"干法熄焦"},{"id":"30c03b4a-4710-43b4-ae61-3c192e57cee2","keyword":"稳定熄焦","originalKeyword":"稳定熄焦"},{"id":"ed92f3b0-8758-4ac2-a3b3-5f9633fd2d06","keyword":"比较","originalKeyword":"比较"}],"language":"zh","publisherId":"gt200411018","title":"干法熄焦和稳定熄焦","volume":"39","year":"2004"},{"abstractinfo":"为了研究一种脱硫活性好、机械强度大的成型活性焦,用正交试验法制备成型活性焦,并对各因素进行方差分析和效应考察,得到了用榆林废弃的半焦焦粉制备耐压强度高、脱硫效果好的成型活性焦的工艺条件.使用微机控制电子万能试验机进行耐压强度的测量,利用氮气等温吸附方法测量了原料及成品活性焦的孔结构.最优条件下制备的活性焦碘吸附值为304.8mg/g;比表面积为303.6m2/g;孔容为0.229 9mL/g;前5h的脱硫量达到80%以上,满足烧结烟气脱硫的要求.","authors":[{"authorName":"郑亚旭","id":"c8c4daae-4d37-4186-8a01-e2fd3a03ef47","originalAuthorName":"郑亚旭"},{"authorName":"张建良","id":"efeafeb9-e24c-470a-83af-c39eb6601ae5","originalAuthorName":"张建良"},{"authorName":"刘征建","id":"446a1285-9ea0-4514-a9c1-96242374467a","originalAuthorName":"刘征建"},{"authorName":"杨成杰","id":"6876a7ea-0f83-49a5-b3cb-e73deeb2bbbf","originalAuthorName":"杨成杰"},{"authorName":"付亚清","id":"51c00fa7-7c6b-4fb5-96a2-fa67bdb5e0af","originalAuthorName":"付亚清"}],"doi":"","fpage":"11","id":"2021b33d-c32a-4593-9bd6-62fbe3445a0d","issue":"5","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"d5982521-b96b-42d0-9d6a-35dde4c78ff6","keyword":"钢铁冶金","originalKeyword":"钢铁冶金"},{"id":"1ae480b0-4d2d-4447-aace-29af7e2ee70d","keyword":"烧结","originalKeyword":"烧结"},{"id":"95dedeb6-7d67-4a61-a068-4cdf8b0f6a8a","keyword":"半焦","originalKeyword":"半焦"},{"id":"c8985ff0-24b7-4353-bce7-d931acfeec83","keyword":"活性焦","originalKeyword":"活性焦"},{"id":"7c233fa1-3590-4a49-b38a-c9e86ff66b69","keyword":"烟气脱硫","originalKeyword":"烟气脱硫"}],"language":"zh","publisherId":"gtyjxb201005003","title":"半焦制备烧结烟气脱硫用活性焦","volume":"22","year":"2010"},{"abstractinfo":"缚硫焦是在高硫炼焦煤中加入缚硫剂,使之“缚”住其中尽可能多的硫在炼铁时直接进入炉渣,减少生铁中硫的污染。用缚硫焦和高硫焦分别进行炼铁试验,结果表明:用缚硫焦在小高炉中炼出的铸造生铁,其合格率巳达到90％以上,取得的各项炼铁技术经济指标均显示出有一定的优越性。在炼铁试验中,曾分层从高炉中取出焦炭、矿石、熔剂、生铁和炉渣五种炉料的样品,经过大量分析,得出在分别用缚硫焦和高硫焦炼铁期间五种炉料中沿高炉高度方向的含硫量变化,从而比较清楚地掌握了硫在高炉内的活动规律。这对进一步研究提高缚硫效果以及生铁的硫化和脱硫机理,有一定的意义。","authors":[{"authorName":"龙世刚","id":"d9558673-995c-482b-a19d-5f46f657e314","originalAuthorName":"龙世刚"}],"categoryName":"|","doi":"","fpage":"169","id":"6f2a962c-4737-4ac4-ba3e-2762e118561f","issue":"3","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[],"language":"zh","publisherId":"0412-1961_1977_3_6","title":"缚硫焦炼铁试验","volume":"13","year":"1977"},{"abstractinfo":"介绍了干熄焦技术的原理和特点,国外干熄焦技术的发展以及国内干熄焦技术的应用现状,并对我国大力发展干熄焦的必要性进行了综述.","authors":[{"authorName":"刘智平","id":"dc022f59-f944-42a0-adef-ebdda62e890b","originalAuthorName":"刘智平"}],"doi":"10.3969/j.issn.1001-1447.2004.01.016","fpage":"58","id":"23593c24-cf70-4023-82ad-d68031a17f38","issue":"1","journal":{"abbrevTitle":"GTYJ","coverImgSrc":"journal/img/cover/GTYJ.jpg","id":"29","issnPpub":"1001-1447","publisherId":"GTYJ","title":"钢铁研究"},"keywords":[{"id":"ca5b42e8-9190-4467-8484-bdf20c07caa8","keyword":"干熄焦","originalKeyword":"干熄焦"},{"id":"afaf127a-3375-4d76-9455-9e85fc5ef54a","keyword":"技术发展及应用","originalKeyword":"技术发展及应用"},{"id":"cbb70d4e-d0d0-4335-b0f9-ca86cc2f4ea0","keyword":"综述","originalKeyword":"综述"}],"language":"zh","publisherId":"gtyj200401016","title":"干熄焦技术及其应用","volume":"32","year":"2004"},{"abstractinfo":"用半焦制备柱状活性焦，用CO2做活化剂，通过正交实验考察了各种因素对活性焦性能的影响。最优方案为炭化温度600℃、炭化时间60min、活化温度850℃、活化时间90min、CO2流量100ml/min。最优条件下制备的活性焦碘吸附值为304.8mg/g，活性焦的比表面积由原来的3.371m2/g增加到303.6m2/g；孔容由原来的0.001823ml/g增加到0.2299ml/g；微孔面积大大增加，平均孔径达到了微孔的要求(＜5nm)；耐压强度很高，前5个小时之内的脱硫量达到80%以上，满足烧结烟气脱硫的要求。","authors":[{"authorName":"郑亚旭\t张建良\t刘征建\t杨成杰\t付亚清","id":"48b26d2a-6a71-4557-b2fb-470431371cfd","originalAuthorName":"郑亚旭\t张建良\t刘征建\t杨成杰\t付亚清"}],"categoryName":"|","doi":"","fpage":"11","id":"29e6c5bc-09d6-4516-ac21-52c0c623796b","issue":"5","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"1a12d0a1-062f-4a99-add8-511a876e006c","keyword":"钢铁冶金;烧结;半焦;活性焦;烟气脱硫","originalKeyword":"钢铁冶金;烧结;半焦;活性焦;烟气脱硫"}],"language":"zh","publisherId":"1001-0963_2010_5_7","title":"半焦制备烧结烟气脱硫用活性焦","volume":"22","year":"2010"},{"abstractinfo":"对玉米秆、树叶、棉花秆和稻壳等四种生物质在不同条件下热解制备的焦进行了脱硫性能实验.结果显示,在所研究的四种生物质中,玉米秆焦的脱硫性能最佳,而稻壳焦的脱硫性能最差.热解温度是影响生物质焦脱硫性能的一个重要因素,随热解温度从400℃到600℃,焦的脱硫效率增加,但热解温度进一步增加到850℃时,焦的脱硫效率降低.热解速度亦影响焦的脱硫性能.快速热解制得的焦的脱硫效率比慢速热解的高.随烟气温度的升高,脱硫效率表现出减少的趋势.","authors":[{"authorName":"张军","id":"96929c05-d6b0-451a-884f-19eb0f6f6f09","originalAuthorName":"张军"},{"authorName":"林晓芬","id":"000b11da-775b-42e7-9334-849fee9343e2","originalAuthorName":"林晓芬"},{"authorName":"印佳敏","id":"b2c75ccf-33b4-4cb5-959f-d93bd0dcabe8","originalAuthorName":"印佳敏"},{"authorName":"范志林","id":"1b343d93-8a3f-4b3e-bd6c-83fde8b1faf2","originalAuthorName":"范志林"},{"authorName":"徐益谦","id":"e44223f3-dab4-417b-9d31-a50581b68427","originalAuthorName":"徐益谦"}],"doi":"","fpage":"537","id":"897a6634-1eb5-4b2c-8184-642f66829d54","issue":"3","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报 "},"keywords":[{"id":"1b9e25d5-eae6-45b2-a0e4-11e021198743","keyword":"生物质","originalKeyword":"生物质"},{"id":"ec077340-f4e8-49fa-8173-db733a4fb489","keyword":"脱硫","originalKeyword":"脱硫"},{"id":"23ed5fc2-d9e3-4791-a543-ae9f6cc5c5dc","keyword":"焦","originalKeyword":"焦"},{"id":"51468feb-f058-44a9-903e-9c3689915ea3","keyword":"烟气温度","originalKeyword":"烟气温度"}],"language":"zh","publisherId":"gcrwlxb200503053","title":"生物质焦脱硫性能实验研究","volume":"26","year":"2005"},{"abstractinfo":"炼焦设备中湿法熄焦的熄焦机的工作条件极为恶劣,分析了造成熄焦机腐蚀的原因,曾采用氯化聚乙烯涂料防护,后改用喷涂不锈钢防护层.介绍了施工情况,分析了效果及存在的不足.","authors":[{"authorName":"倪波","id":"f9be0a1c-3ac3-4ebd-89c4-38d6e5cca2b0","originalAuthorName":"倪波"}],"doi":"10.3969/j.issn.1005-748X.2003.05.014","fpage":"226","id":"a406141f-b0a8-481a-8bec-0e23675a9504","issue":"5","journal":{"abbrevTitle":"FSYFH","coverImgSrc":"journal/img/cover/FSYFH.jpg","id":"25","issnPpub":"1005-748X","publisherId":"FSYFH","title":"腐蚀与防护"},"keywords":[{"id":"c4915308-a2a7-4d60-94e3-b0e0bc360d5c","keyword":"熄焦机","originalKeyword":"熄焦机"},{"id":"aa421e58-226a-4832-8b12-a9ebf21f495a","keyword":"腐蚀防护","originalKeyword":"腐蚀防护"},{"id":"26c8c73b-f4a2-4892-a138-f61d12a64de1","keyword":"喷涂","originalKeyword":"喷涂"},{"id":"e020bcde-6e98-4d78-b0fb-2a79ac1712ec","keyword":"不锈钢防护层","originalKeyword":"不锈钢防护层"}],"language":"zh","publisherId":"fsyfh200305014","title":"熄焦机的腐蚀防护","volume":"24","year":"2003"},{"abstractinfo":"本文在自行研制的加压热重分析仪上对气化半焦的加压燃烧特性进行了较为系统的研究.讨论了五种半焦在不同压力、不同粒径条件下的TG-DTG曲线,并对它们加以比较.分析了半焦种类、总压和试样粒径对最大失重速率、最大失重峰温度、燃尽时间、燃尽温度等的影响,井使用平均质量反应性指数对半焦反应性加以评价.","authors":[{"authorName":"陈晓平","id":"d06ca074-edb4-4aba-94aa-063f0973d362","originalAuthorName":"陈晓平"},{"authorName":"谷小兵","id":"8083621e-1488-4ba1-8cf8-acb7bcf5041f","originalAuthorName":"谷小兵"},{"authorName":"段钰锋","id":"1956b463-cc2d-4c4c-a3ad-34259a32b4cc","originalAuthorName":"段钰锋"},{"authorName":"赵长遂","id":"99f370c5-65f6-4a17-b3e5-67b99d1c95ec","originalAuthorName":"赵长遂"},{"authorName":"吴新","id":"f0fa2bb0-33d5-48b7-a883-a4c50a99e5cb","originalAuthorName":"吴新"}],"doi":"","fpage":"345","id":"3e86ca20-d59b-4d0d-8f47-098d6cbe1f23","issue":"2","journal":{"abbrevTitle":"GCRWLXB","coverImgSrc":"journal/img/cover/GCRWLXB.jpg","id":"32","issnPpub":"0253-231X","publisherId":"GCRWLXB","title":"工程热物理学报 "},"keywords":[{"id":"31624a16-154e-4121-9e4d-a1e5f0ab9f6b","keyword":"半焦","originalKeyword":"半焦"},{"id":"d740fbb7-6930-4c91-a1a6-52eaf6aaafaa","keyword":"加压热重分析仪","originalKeyword":"加压热重分析仪"},{"id":"636337b9-9b5c-4e2a-ba27-8d79e62b99dd","keyword":"燃烧特性","originalKeyword":"燃烧特性"},{"id":"29d5828f-5d40-4977-be9d-c9a36a0a4fec","keyword":"反应性","originalKeyword":"反应性"}],"language":"zh","publisherId":"gcrwlxb200402050","title":"半焦加压燃烧特性研究","volume":"25","year":"2004"}],"totalpage":91,"totalrecord":903}
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