{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":2,"startPagecode":1},"records":[{"abstractinfo":"以多钒酸铵为原料,采用返溶除杂、溶液<span style=\"color:red\">脱氨</span>、溶析结晶的方法,制备了纯度大于99.5％的偏钒酸钠产品.通过研究表明:影响<span style=\"color:red\">脱氨</span>过程<span style=\"color:red\">脱氨</span>时间的主要因素为溶液终点pH值;最佳溶析结晶条件为[V]浓度150 ～ 200g/L,pH值为7.3 ～8.1,结晶剂与溶液体积比为1∶1,结晶时间为1h,钒收率达到了97.7％.","authors":[{"authorName":"殷兆迁","id":"e0880a38-e569-4baa-86bd-424a7202bf3f","originalAuthorName":"殷兆迁"},{"authorName":"李千文","id":"100f4c5f-f8c3-41b9-8dae-25bde4c2d174","originalAuthorName":"李千文"},{"authorName":"彭一村","id":"8b1c8cf0-f397-410f-9bfa-b97b63a1c9ae","originalAuthorName":"彭一村"},{"authorName":"吴刘柱","id":"63da2f9a-126d-434d-870c-eb76c0e05f0e","originalAuthorName":"吴刘柱"},{"authorName":"潘少彦","id":"c1d6ce6b-fa96-4726-b0c1-633222efb426","originalAuthorName":"潘少彦"}],"doi":"10.7513/j.issn.1004-7638.2015.02.004","fpage":"17","id":"7f3b89ba-a6b2-451f-854c-2b28555ee7ca","issue":"2","journal":{"abbrevTitle":"GTFT","coverImgSrc":"journal/img/cover/gtft1.jpg","id":"28","issnPpub":"1004-7638","publisherId":"GTFT","title":"钢铁钒钛"},"keywords":[{"id":"ca0b9c97-9a48-4f37-a25f-fa9252701491","keyword":"偏钒酸钠","originalKeyword":"偏钒酸钠"},{"id":"ba308191-e868-4607-9c10-2fbadd5b1dd8","keyword":"多钒酸铵","originalKeyword":"多钒酸铵"},{"id":"05028441-e161-434d-b507-924550fb30a7","keyword":"<span style=\"color:red\">脱氨</span>","originalKeyword":"脱氨"},{"id":"8f9df3a6-9b72-4943-b692-78b9ff5f51d3","keyword":"钒收率","originalKeyword":"钒收率"}],"language":"zh","publisherId":"gtft201502004","title":"偏钒酸钠制取技术研究","volume":"36","year":"2015"},{"abstractinfo":"采用<span style=\"color:red\">脱氨</span>剂去除稀土废水氨氮,并对处理的影响因素进行了探讨.试验结果表明,投加量<span style=\"color:red\">脱氨</span>剂为1000 mg/L、反应时间为60min、反应pH为9时,可将稀土废水中的NH3-N从14436mg/L降低到2435mg/L,去除率达到83.13%,并可大大降低处理成本,因此,该方法可以作为稀土废水的前处理方法.","authors":[{"authorName":"简放陵","id":"3d526830-801a-4d3d-adc6-a9688c8635db","originalAuthorName":"简放陵"},{"authorName":"吴凯丽","id":"157735d4-9335-4441-a478-595bfe53cf19","originalAuthorName":"吴凯丽"},{"authorName":"谢勇","id":"1eab0c30-b293-4209-b0da-47a323c5b2ed","originalAuthorName":"谢勇"}],"doi":"10.3969/j.issn.1004-0277.2010.06.010","fpage":"52","id":"9f0627f5-87d0-4cf9-8071-678cefd6fe80","issue":"6","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"ab11e851-5b96-451b-bc43-88829714fa43","keyword":"稀土废水","originalKeyword":"稀土废水"},{"id":"c282dc55-7c2a-4ce8-8cbc-4b3d5e5244eb","keyword":"氨氮","originalKeyword":"氨氮"},{"id":"10a1bb53-c538-4d7f-bf65-47a001a9196b","keyword":"<span style=\"color:red\">脱氨</span>剂","originalKeyword":"脱氨剂"}],"language":"zh","publisherId":"xitu201006010","title":"<span style=\"color:red\">脱氨</span>剂去除稀土废水氨氮的研究","volume":"31","year":"2010"},{"abstractinfo":"分析沉钒废水脱除氨氮过程中汽提<span style=\"color:red\">脱氨</span>塔结垢形成原因,主要是由于在高温、碱性条件下,沉钒废水中钙、镁离子极易与水中碳酸根、氢氧根、硅酸根等离子发生复杂反应,形成钙镁垢.提出解决<span style=\"color:red\">脱氨</span>塔结垢措施:①向沉钒废水中加入质量比例0.02％的阻垢分散剂KL101;②采取定期清洗汽提<span style=\"color:red\">脱氨</span>塔管道、换热器、鲍尔环填料等方法.通过实施以上措施后,汽提<span style=\"color:red\">脱氨</span>塔运行周期由不足7d提高到40d以上,实现长周期、安全稳定连续运行,<span style=\"color:red\">脱氨</span>后的沉钒废水NH3-N浓度不大于30 mg/L,达标排放.","authors":[{"authorName":"滕晓慧","id":"397ec714-d1f9-4a7f-a6bc-190d237eea0f","originalAuthorName":"滕晓慧"}],"doi":"10.7513/j.issn.1004-7638.2015.01.009","fpage":"48","id":"44b08d2d-51a5-4ff6-ac1e-3e5ab6d5585f","issue":"1","journal":{"abbrevTitle":"GTFT","coverImgSrc":"journal/img/cover/gtft1.jpg","id":"28","issnPpub":"1004-7638","publisherId":"GTFT","title":"钢铁钒钛"},"keywords":[{"id":"8a59308f-7433-466e-96ae-3c50937e9768","keyword":"沉钒废水","originalKeyword":"沉钒废水"},{"id":"13b119ac-07c0-4f6b-8cfa-360edc100cfb","keyword":"氨氮","originalKeyword":"氨氮"},{"id":"6730d758-792f-4c73-8a2b-6a3c594fca04","keyword":"汽提","originalKeyword":"汽提"},{"id":"88fe38bd-6a82-465f-be3c-11b940095ddb","keyword":"<span style=\"color:red\">脱氨</span>塔","originalKeyword":"脱氨塔"},{"id":"b0ab4077-ccc5-4188-a07f-44714925b745","keyword":"结垢","originalKeyword":"结垢"}],"language":"zh","publisherId":"gtft201501009","title":"沉钒废水汽提<span style=\"color:red\">脱氨</span>塔结垢成因及对策","volume":"36","year":"2015"},{"abstractinfo":"","authors":[{"authorName":"余玉叶","id":"46570e93-cc83-4668-8d18-5e67848a04ef","originalAuthorName":"余玉叶"},{"authorName":"赵国良","id":"9e1605f3-e71b-4018-a7e2-a4421a0479ff","originalAuthorName":"赵国良"},{"authorName":"刘幸海","id":"0c06bfda-38ad-4346-a5ec-a4b08afe5f67","originalAuthorName":"刘幸海"}],"doi":"10.3969/j.issn.1000-0518.2005.06.028","fpage":"694","id":"99bcc2d6-6ed7-485b-a789-f77df3e7c944","issue":"6","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"739040c2-a27a-4ffd-861f-956ab082de6f","keyword":"二氯化六氨合镍(Ⅱ),<span style=\"color:red\">脱氨</span>动力学,热分析,非等温法","originalKeyword":"二氯化六氨合镍(Ⅱ),脱氨动力学,热分析,非等温法"}],"language":"zh","publisherId":"yyhx200506028","title":"二氯化六氨合镍(Ⅱ)配合物的<span style=\"color:red\">脱氨</span>反应动力学机理","volume":"22","year":"2005"},{"abstractinfo":"采用离子膜电解法对高浓度氨氮废水进行<span style=\"color:red\">脱氨</span>预处理,对影响氨氮去除的几种因素进行了研究.6 V、60℃下去除率在75%以上.脱除的氨氮以浓氨水的形式回收,实现废物资源化.废水经<span style=\"color:red\">脱氨</span>后出水基本无色,COD也有一定降低.综合考虑能耗后,得出本实验条件下适宜的操作条件,去除率平均接近64%,为工业化应用提供了依据.","authors":[{"authorName":"张梅玲","id":"c2b28d3c-1d0e-4e4a-819a-93f001c5ca97","originalAuthorName":"张梅玲"},{"authorName":"蔚东升","id":"206928b3-3b28-4f6b-91a3-8154f3e85a85","originalAuthorName":"蔚东升"},{"authorName":"顾国锋","id":"9eab20f9-4683-4cb7-990d-40f5dab3d52b","originalAuthorName":"顾国锋"},{"authorName":"陈慧婷","id":"06268877-9712-44ee-8a7d-a72583f872c8","originalAuthorName":"陈慧婷"},{"authorName":"陶阳宇","id":"7537d1ff-dc37-4827-9ac1-e3d5a0fdb161","originalAuthorName":"陶阳宇"},{"authorName":"赵玉明","id":"d0734bb2-9a8b-425b-b2d2-d39447dc4c43","originalAuthorName":"赵玉明"}],"doi":"10.3969/j.issn.1007-8924.2007.02.013","fpage":"61","id":"e6206183-8f2d-4989-ac2a-ca4003949e03","issue":"2","journal":{"abbrevTitle":"MKXYJS","coverImgSrc":"journal/img/cover/MKXYJS.jpg","id":"54","issnPpub":"1007-8924","publisherId":"MKXYJS","title":"膜科学与技术   "},"keywords":[{"id":"18d76d51-6a04-4c81-837b-1692d9a66e1b","keyword":"阳离子交换膜","originalKeyword":"阳离子交换膜"},{"id":"49cb60a6-b952-4f48-9d07-e7f68628946c","keyword":"电解","originalKeyword":"电解"},{"id":"fe8d1825-0363-4e73-a37b-f7a3de235dcf","keyword":"味精废水","originalKeyword":"味精废水"},{"id":"57f9e2d2-62f5-4ce4-a57b-d1641e219411","keyword":"氨氮","originalKeyword":"氨氮"}],"language":"zh","publisherId":"mkxyjs200702013","title":"离子膜电解去除味精废水中氨氮的研究","volume":"27","year":"2007"},{"abstractinfo":"研究了工作温度、起始氨压和球磨处理对无水CaCl<SUB>2</SUB>的吸放氨性能的影响. 结果发现, 球磨2h样品在温度20℃和氨压0.55MPa的条件下, 15min内即可完全氨化, 形成CaCl<SUB>2</SUB>(NH<SUB>3</SUB>)<SUB>8</SUB>, 其吸氨量可达55.1wt%, 相当于储氢量9.72wt%. CaCl<SUB>2</SUB>(NH<SUB>3</SUB>)<SUB>8</SUB>在20～300℃的范围内可通过三步反应实现完全<span style=\"color:red\">脱氨</span>, <span style=\"color:red\">脱氨</span>反应受温度和压力控制, 其中6个NH<SUB>3</SUB>分子在常温、常压下即可脱附. 如果与NH<SUB>3</SUB>分解催化剂联用, 可能是一种较好的以NH<SUB>3</SUB>为介质的高容量储氢材料. 进一步研究表明, 较高的工作温度和起始氨压可以提高CaCl<SUB>2</SUB>的吸氨动力学性能, 而球磨时间的增加可以显著降低其放氨工作温度, 提高其放氨动力学性能.","authors":[{"authorName":"林仁波","id":"346d594f-04c9-435e-8458-5b84016f3cdb","originalAuthorName":"林仁波"},{"authorName":"刘永锋","id":"986c00bb-8d03-465f-a221-c14adef58c64","originalAuthorName":"刘永锋"},{"authorName":"高明霞","id":"30b242dc-4858-415a-abb8-2af67a0e6a6a","originalAuthorName":"高明霞"},{"authorName":"王建辉","id":"5f992bdb-fafe-487b-9039-49137104c1ec","originalAuthorName":"王建辉"},{"authorName":"葛红卫","id":"fcd64524-3bb9-41d5-97a6-9c293e2bb918","originalAuthorName":"葛红卫"},{"authorName":"潘洪革","id":"5638359b-3486-4354-b5e2-96211f862758","originalAuthorName":"潘洪革"}],"categoryName":"|","doi":"10.3724/SP.J.1077.2008.01059","fpage":"1059","id":"4671a212-c083-450b-a1c6-ab7829ba3f06","issue":"5","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"f52b8875-92f5-42d5-9b66-d95738dd43a3","keyword":"储氢材料","originalKeyword":"储氢材料"},{"id":"67a43323-986f-44dd-a97e-3066a791243d","keyword":" fuel cell","originalKeyword":" fuel cell"},{"id":"f4b17f43-e656-4291-a8e1-455fbf3e8790","keyword":" metal chloride","originalKeyword":" metal chloride"},{"id":"680ea256-c846-4113-b551-1513830e32c4","keyword":" ammonia absorption/desorption","originalKeyword":" ammonia absorption/desorption"}],"language":"zh","publisherId":"1000-324X_2008_5_39","title":"新型氨基储氢材料CaCl<SUB>2</SUB>的性能研究","volume":"23","year":"2008"},{"abstractinfo":"研究了工作温度,起始氨压和球磨处理对无水CaCl2的吸放氨性能的影响.结果发现,球磨2h样品在温度20℃和氨压0.55MPa的条件下,15min内即可完全氨化,形成CaCl2(NH3)8,其吸氨量可达55.1wt%,相当于储氢量9.72wt%.CaCl2(NH3)8在20-300℃的范围内可通过三步反应实现完全<span style=\"color:red\">脱氨</span>,<span style=\"color:red\">脱氨</span>反应受温度和压力控制,其中6个NH3分子在常温、常压下即可脱附.如果与NH3分解催化剂联用,可能是一种较好的以NH3为介质的高容量储氢材料.进一步研究表明,较高的工作温度和起始氨压可以提高CaCl2的吸氨动力学性能,而球磨时间的增加可以显著降低其放氨工作温度,提高其放氨动力学性能.","authors":[{"authorName":"林仁波","id":"e145c6fe-95ca-4e30-965f-3a7eb5c9ef31","originalAuthorName":"林仁波"},{"authorName":"刘永锋","id":"6938a89d-cda4-4117-97d4-737c975b327d","originalAuthorName":"刘永锋"},{"authorName":"高明霞","id":"8ed495ef-f0b5-4187-820b-d9d14d726826","originalAuthorName":"高明霞"},{"authorName":"王建辉","id":"d5be0051-cd47-4687-97cd-931d51fa4c6c","originalAuthorName":"王建辉"},{"authorName":"葛红卫","id":"370a08c6-3596-4dab-b415-773b9cc602ed","originalAuthorName":"葛红卫"},{"authorName":"潘洪革","id":"765c0c79-879b-47d4-a539-914f607addcf","originalAuthorName":"潘洪革"}],"doi":"10.3321/j.issn:1000-324X.2008.05.039","fpage":"1059","id":"01773692-daa3-46e3-863c-ed6cd88e2dbe","issue":"5","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"2829a4ad-9f2e-4e87-9b10-e1412011048f","keyword":"储氢材料","originalKeyword":"储氢材料"},{"id":"9e39bc88-fd90-489a-b4d9-4d7623bb0171","keyword":"燃料电池","originalKeyword":"燃料电池"},{"id":"dd85a9d9-8e50-426a-9229-1846a72f4665","keyword":"金属氯化物","originalKeyword":"金属氯化物"},{"id":"34c96d81-1e50-4242-8d6d-4f56b6ccf12a","keyword":"吸放氨性能","originalKeyword":"吸放氨性能"}],"language":"zh","publisherId":"wjclxb200805039","title":"新型氨基储氢材料CaCl2的性能研究","volume":"23","year":"2008"},{"abstractinfo":"用焦亚硫酸钠、海波上层液分别处理沉钒废水,研究表明:海波上层液还原沉钒废水COD高达2 878 mg/L,远超排放标准;用焦亚硫酸钠还原沉钒废水,中和、沉淀能够获取低COD废水、低铁含铬渣.用焦亚硫酸钠处理沉钒废水工业运行技术条件:焦亚硫酸钠加入倍数3.1 ～3.2,还原反应时间15 ～ 30 min.处理后废水经汽提<span style=\"color:red\">脱氨</span>塔<span style=\"color:red\">脱氨</span>后,排向污水处理厂的废水未检出六价铬,COD平均值65 mg/L,符合辽宁省地方排放标准《污水综合排放标准》DB21/1627-2008排放限值,所得含铬渣中铁含量较低(以Fe2O3计0.27％),铬含量高(以Cr2O3计41.6％).含铬渣经煅烧窑煅烧、炉外法冶炼出牌号JCr95金属铬(Cr≥95％)产品,质量合格.","authors":[{"authorName":"滕晓慧","id":"96afa0f0-7428-4348-8979-d0b8476c497f","originalAuthorName":"滕晓慧"},{"authorName":"庄立军","id":"11687e72-487c-43e1-8525-b1f14580ca33","originalAuthorName":"庄立军"},{"authorName":"李文慧","id":"360bd6cb-faa3-4be9-830b-c758d78924fb","originalAuthorName":"李文慧"}],"doi":"10.7513/j.issn.1004-7638.2016.02.013","fpage":"73","id":"3738fb12-9668-4209-adc0-52b56f993f5f","issue":"2","journal":{"abbrevTitle":"GTFT","coverImgSrc":"journal/img/cover/gtft1.jpg","id":"28","issnPpub":"1004-7638","publisherId":"GTFT","title":"钢铁钒钛"},"keywords":[{"id":"96c92aa1-b803-4d46-8949-8ed0eb96047b","keyword":"沉钒废水","originalKeyword":"沉钒废水"},{"id":"8fbdc315-86bf-420d-b14c-13f227af9f43","keyword":"海波上层液","originalKeyword":"海波上层液"},{"id":"590dfd18-9181-4e39-81f5-c489036afdd5","keyword":"焦亚硫酸钠","originalKeyword":"焦亚硫酸钠"},{"id":"5b8ef5fc-6c2c-4fc3-ad0e-111aa3bedccf","keyword":"还原","originalKeyword":"还原"},{"id":"f1caec36-4ea3-476a-bf76-1227ecd489c0","keyword":"COD","originalKeyword":"COD"},{"id":"9df71155-c22e-495a-8be6-2a866f580979","keyword":"含铬渣","originalKeyword":"含铬渣"},{"id":"46a8b3f1-9418-4a06-a218-1212cb194cbf","keyword":"金属铬","originalKeyword":"金属铬"}],"language":"zh","publisherId":"gtft201602013","title":"低COD处理沉钒废水回收低铁含铬渣冶炼金属铬","volume":"37","year":"2016"},{"abstractinfo":"用SiCl4为原料,通过水解和氨解的方法,制备了不同含氮量的硅氧氮先驱体.先驱体通过<span style=\"color:red\">脱氨</span>基原位聚合,再经过无机化转变成为成分均匀的硅氧氮粉体,用所得粉体热压烧结制备了硅氧氮材料.测试分析结果表明,氮的引入使氧化硅的析晶温度提高了150℃;适量析晶显著提高材料的力学性能;烧结温度为1400℃时,氮的质量分数为24.3%材料的强度和韧性最大,分别达到156MPa和1.8MPa*m1/2,比SiO2基体的强度和韧性提高了4.58倍和2.25倍.","authors":[{"authorName":"张俊宝","id":"6ae81381-6a63-4dff-99fa-875b86788482","originalAuthorName":"张俊宝"},{"authorName":"温广武","id":"f2d12c03-9332-4aa2-b342-b46247951baf","originalAuthorName":"温广武"},{"authorName":"贾德昌","id":"575fe085-ab34-417d-a6bb-b2b5b62c0230","originalAuthorName":"贾德昌"},{"authorName":"雷廷权","id":"7b0e6d5f-9540-4a23-a457-ba4ab6ec8855","originalAuthorName":"雷廷权"},{"authorName":"周玉","id":"87d04b3c-4590-4702-b0da-c726fdb4943f","originalAuthorName":"周玉"}],"doi":"10.3969/j.issn.1005-5053.2001.03.009","fpage":"39","id":"48add12c-2ba8-4f69-912a-0c60d6270f1a","issue":"3","journal":{"abbrevTitle":"HKCLXB","coverImgSrc":"journal/img/cover/HKCLXB.jpg","id":"41","issnPpub":"1005-5053","publisherId":"HKCLXB","title":"航空材料学报"},"keywords":[{"id":"a0a49e2c-289e-4a3e-809b-28111b2194ac","keyword":"硅氧氮","originalKeyword":"硅氧氮"},{"id":"2874585f-ef94-4f73-9903-e04e49fd48ff","keyword":"先驱体","originalKeyword":"先驱体"},{"id":"a900c6c0-db76-494e-a810-b48e02ff11aa","keyword":"热分解","originalKeyword":"热分解"},{"id":"67def984-549d-4bc8-8271-4c1fa2982e19","keyword":"力学性能","originalKeyword":"力学性能"}],"language":"zh","publisherId":"hkclxb200103009","title":"硅氧氮陶瓷的先驱体法合成及性能的研究","volume":"21","year":"2001"},{"abstractinfo":"以纯铜片为原料,经过碳酸氢铵-氨水溶铜、常压<span style=\"color:red\">脱氨</span>、焙烧等3个阶段,得到了活性氧化铜粉.用扫描电镜(SEM)、X射线衍射(XRD)、电感耦合等离子体原子发射光谱(ICP-AES)等方法对所得活性氧化铜粉的性能进行了表征.结果表明,采用该方法得到的活性氧化铜粉纯度达到99％以上,金属杂质含量和溶解速率完全符合电镀级氧化铜粉的要求,可以直接用于线路板的电镀铜.","authors":[{"authorName":"符飞燕","id":"f8bc8316-af05-4bb8-a57a-e1877323c8d4","originalAuthorName":"符飞燕"},{"authorName":"王克军","id":"806b63e6-1ec7-46f7-ac9b-4a29d5b9829a","originalAuthorName":"王克军"},{"authorName":"黄革","id":"5d538bde-2cea-403b-a376-f9fafe916e93","originalAuthorName":"黄革"},{"authorName":"周仲承","id":"c8f8675c-e6df-4faf-85b3-01b7c13e7256","originalAuthorName":"周仲承"},{"authorName":"高四","id":"78570212-d5ec-4a2c-a0aa-5a37bb578588","originalAuthorName":"高四"},{"authorName":"刘荣胜","id":"686eeab4-6936-446e-a743-59a0b5a5fda3","originalAuthorName":"刘荣胜"}],"doi":"","fpage":"8","id":"cd2f78d9-6e8f-46ad-8be8-544f916117ea","issue":"9","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰   "},"keywords":[{"id":"fd6df979-b785-476c-9f38-faf6161bf26e","keyword":"氧化铜","originalKeyword":"氧化铜"},{"id":"5ad6d982-2c86-47f2-a291-83d489e58c11","keyword":"制备","originalKeyword":"制备"},{"id":"8984eb5f-98bd-4604-bc06-fcaded8fb3c3","keyword":"表征","originalKeyword":"表征"},{"id":"06d598f0-ccad-4387-b51a-155ac1ca2d8a","keyword":"印制电路板","originalKeyword":"印制电路板"},{"id":"3d05f350-1fd9-4cfa-9b4e-61222f13729a","keyword":"酸性镀铜","originalKeyword":"酸性镀铜"}],"language":"zh","publisherId":"ddyts201209003","title":"电镀级活性氧化铜粉的制备","volume":"31","year":"2012"}],"totalpage":2,"totalrecord":12}