The work concerned the electrochemical behaviors of Y(III) on W and Ni electrodes in molten LiCl-KCl salts by a series of electrochemical techniques. The electrochemical reaction of Y(III) to Y(0) proceeded in a one-step reduction process with the ex-change of three electrons, Y(III)+3e–→Y(0). Compared with the cyclic voltam{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"本文以HNO3/HBrO3/KMnO4为氧化插层体系制备低温可膨胀石墨,研究了制备低温可膨胀石墨的最佳条件和物料配比,讨论了插层试剂对起始膨胀温度的影响,提出了氧化插层的机理.研究表明:制备低温可膨胀石墨的反应温度为室温(25 ℃);反应时间40 min;石墨、硝酸、溴酸钠、高锰酸钾的最佳质量比为1∶[KG-·2]3∶[KG-·2]0.1∶[KG-·2]0.07,由此方法制得的可膨胀石墨起始膨胀温度为130 ℃,600 ℃时膨胀容积为350 mL/g.","authors":[{"authorName":"王玲","id":"d1b4dfb1-fb80-4d6c-9463-6dd5a9ef0c99","originalAuthorName":"王玲"},{"authorName":"宋克敏","id":"7ba9f0c4-a15c-4e31-b5c0-71ebfe50b321","originalAuthorName":"宋克敏"},{"authorName":"张帅华","id":"04a361b4-c49e-47f6-9287-f2a3641ca4ef","originalAuthorName":"张帅华"},{"authorName":"李庆","id":"35378a05-2d8c-496e-8f2c-427146518ba2","originalAuthorName":"李庆"},{"authorName":"李云鹏","id":"97ac836b-8c14-49e7-b5ac-4a713b63eae4","originalAuthorName":"李云鹏"},{"authorName":"刘敏","id":"98d1b463-3fca-4433-82c7-53cd187dd809","originalAuthorName":"刘敏"}],"doi":"","fpage":"844","id":"6d7f159f-45ec-4658-8be0-b340c7b2c6de","issue":"4","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报 "},"keywords":[{"id":"92040a07-0558-4b76-a064-fc22707ca573","keyword":"低温可膨胀石墨","originalKeyword":"低温可膨胀石墨"},{"id":"ef720930-377f-4c29-ae14-ba62d4de682e","keyword":"起始膨胀温度","originalKeyword":"起始膨胀温度"},{"id":"bd68e9b8-3a05-478e-a319-5652bc1f98c4","keyword":"膨胀容积","originalKeyword":"膨胀容积"},{"id":"d35e9d9b-f660-4fd3-86f9-6cd72c931ae7","keyword":"插层试剂","originalKeyword":"插层试剂"},{"id":"a636249a-ed7a-4a83-b70f-0ad2b125455e","keyword":"溴酸钠","originalKeyword":"溴酸钠"}],"language":"zh","publisherId":"gsytb200904042","title":"高倍率低温可膨胀石墨制备的研究","volume":"28","year":"2009"},{"abstractinfo":"使用低温可膨胀石墨，通过“原位膨胀-机械剥离”的方法制备了 PMMA/EG 复合材料，研究了可膨胀石墨含量对其电导率的影响。电导率、SEM、动态流变等测试表明膨胀后的石墨片层在树脂基体中分散良好；从10~20 phr 开始，石墨鳞片相互接触形成网络结构显著地提高电导率，最高达12个数量级。采用原位膨胀法可以制备逾渗阈值较小的导电复合材料，填充少量低温可膨胀石墨就可以大幅度提高 PMMA电导率。","authors":[{"authorName":"殷先德","id":"7978aada-bb1a-4491-8106-90e707c908da","originalAuthorName":"殷先德"},{"authorName":"薛白","id":"fd7e2d3f-f509-454d-b868-45db4d1cc956","originalAuthorName":"薛白"},{"authorName":"包建军","id":"2d400db8-35a4-457d-96d5-14aa37f33fd3","originalAuthorName":"包建军"}],"doi":"10.3969/j.issn.1001-9731.2015.15.021","fpage":"15109","id":"11c12381-c0f0-46b3-af1c-70716c570a8e","issue":"15","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"c24d57a8-6ce1-468d-aa3a-023993158faa","keyword":"低温可膨胀石墨","originalKeyword":"低温可膨胀石墨"},{"id":"3d111780-ca60-4794-84ac-58df302fa5b8","keyword":"原位膨胀","originalKeyword":"原位膨胀"},{"id":"2190f0d6-9e56-4ecd-8f7b-02d32170afd7","keyword":"PMMA","originalKeyword":"PMMA"},{"id":"dcc0a8c8-5f57-4738-bee2-9b7669dbdf92","keyword":"电导率","originalKeyword":"电导率"}],"language":"zh","publisherId":"gncl201515021","title":"原位膨胀法制备 PMMA/EG 复合材料及其导电和流变性能的研究","volume":"","year":"2015"},{"abstractinfo":"采用一种新型的水交换法制备工艺,以天然石墨、高锰酸钾、浓硫酸为原料,制得了在160℃时即可发生膨胀的低温可膨胀石墨.采用热失重分析(TGA)、傅立叶转换红外光谱分析(FT-IR)、X射线衍射(XRD)和扫描电镜(SEM)对其结构进行了表征与分析.结果表明,通过水交换法使得插入石墨层间的主要物质为水,水在低温下瞬间汽化对石墨片层产生张力,导致石墨低温膨胀.因此,石墨发生膨胀时无有害小分子释放,对环境友好.","authors":[{"authorName":"卢亚云","id":"54bc6952-4f57-4f44-ad0f-84e21cf4a50f","originalAuthorName":"卢亚云"},{"authorName":"谢林生","id":"882a01ec-508a-4766-91d0-50c947825abb","originalAuthorName":"谢林生"},{"authorName":"汤先文","id":"a9b8441a-f8a8-4ab8-9e58-12c831e7d8ce","originalAuthorName":"汤先文"},{"authorName":"马玉录","id":"f5837208-8539-4c5b-a35d-8f3f9d0b5e55","originalAuthorName":"马玉录"}],"doi":"","fpage":"97","id":"4370b830-e394-47e9-82f2-cb087c9e607a","issue":"18","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"1f941c21-d5a4-4e07-bc4f-32c57397bd2d","keyword":"石墨","originalKeyword":"石墨"},{"id":"e0940cc3-8262-4e96-bb9e-34988e89a214","keyword":"低温可膨胀","originalKeyword":"低温可膨胀"},{"id":"a0f96fa7-e53c-4dea-b696-324a5cfaada6","keyword":"膨胀石墨","originalKeyword":"膨胀石墨"},{"id":"2ed32897-25d5-4c68-a7ef-1f0426e46005","keyword":"水交换法","originalKeyword":"水交换法"}],"language":"zh","publisherId":"cldb200918028","title":"水交换法制备低温可膨胀石墨的研究","volume":"23","year":"2009"},{"abstractinfo":"以D50为0.99 μm的微米石墨为原料,采用KMnO4-HNO3-HClO4-HAc氧化插层反应体系制备可膨胀石墨.通过6因素5水平的正交实验,得出了影响反应体系的主要因素是冰乙酸用量、反应温度和硝酸与高氯酸比例.当反应工艺为:m(C)∶m(KMnO4)=1∶0.4,V(HNO3)∶V(HClO4)=1∶1,m(C)∶V(冰乙酸)=1∶1.5,反应温度为45℃,反应时间为110 min时,可以制得最大膨胀体积的可膨胀石墨.","authors":[{"authorName":"张广昊","id":"630c81d0-44e3-4afa-8d55-fef063608589","originalAuthorName":"张广昊"},{"authorName":"聂浩宇","id":"d8606a54-4c22-4ad4-b769-5249926dba8d","originalAuthorName":"聂浩宇"},{"authorName":"王秀昀","id":"84d2dce5-07c0-447b-bdf6-ef17b78b7df9","originalAuthorName":"王秀昀"},{"authorName":"阚丽丽","id":"e3631016-71c9-4baa-a7e3-e0ee9060e11d","originalAuthorName":"阚丽丽"},{"authorName":"陈厚和","id":"a5a5f25d-e4fd-42be-9b0e-e5406ccf3f7e","originalAuthorName":"陈厚和"}],"doi":"","fpage":"581","id":"395f9684-fbcf-4d6f-933d-d2367543f6c7","issue":"2","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报 "},"keywords":[{"id":"f8d3560b-2f12-4d6d-9ba0-22221e759f3e","keyword":"微米石墨","originalKeyword":"微米石墨"},{"id":"dbbcbd4d-f0bb-489a-a328-aa64aa561f18","keyword":"可膨胀石墨","originalKeyword":"可膨胀石墨"},{"id":"05f4c10b-03f5-4ebd-b6b3-f908dc982cc6","keyword":"正交实验","originalKeyword":"正交实验"}],"language":"zh","publisherId":"gsytb201502054","title":"微米可膨胀石墨的制备","volume":"34","year":"2015"},{"abstractinfo":"在不改变石墨原始结构与成分的基础上,利用冲击波对可膨胀石墨进行爆轰,收集爆轰灰,进行X射线衍射、SEM的测量分析以及BET法测定比表面积.结果表明,可膨胀石墨经过爆轰后,得到了颗粒大小为1μm～10μm的石墨粉,比表面积由8.096 m2/g增大至47.48 m2/g,并且孔隙变得更为均匀,常规研磨设备是无法达到这种效果的.为石墨的细化提供了一种更为简便快捷而又节省能源的方法.","authors":[{"authorName":"孙贵磊","id":"adcb0db9-1513-47ed-a130-ed439d1aa110","originalAuthorName":"孙贵磊"},{"authorName":"李晓杰","id":"72bb3b75-2f38-4087-b40d-995e1974b4db","originalAuthorName":"李晓杰"},{"authorName":"闫鸿浩","id":"6b40bcfc-223a-4db4-b93f-565cf6f43b92","originalAuthorName":"闫鸿浩"}],"doi":"10.3969/j.issn.1007-8827.2007.03.008","fpage":"242","id":"8bc89aa2-3314-4d50-9dff-6554d1205f8a","issue":"3","journal":{"abbrevTitle":"XXTCL","coverImgSrc":"journal/img/cover/XXTCL.jpg","id":"70","issnPpub":"1007-8827","publisherId":"XXTCL","title":"新型炭材料"},"keywords":[{"id":"7de3b2e2-33b6-4c65-8bb3-1f48627f44cb","keyword":"爆轰","originalKeyword":"爆轰"},{"id":"6633972d-d1c0-4ef8-87ec-707e0c9c53f9","keyword":"可膨胀石墨","originalKeyword":"可膨胀石墨"},{"id":"3ee5ff39-61e2-42b9-9ec2-63d4d2a3f3a2","keyword":"X射线","originalKeyword":"X射线"},{"id":"3254dc44-180a-417a-9259-ca86197e8a90","keyword":"BET","originalKeyword":"BET"}],"language":"zh","publisherId":"xxtcl200703008","title":"爆轰裂解可膨胀石墨制备石墨微粉","volume":"22","year":"2007"},{"abstractinfo":"用硝酸（65％）和乙酸酐混合液、高锰酸钾和天然鳞片石墨反应制备无硫可膨胀石墨，最佳反应条件是：石墨、乙酸酐、硝酸、高锰酸钾的重量比为1：0．8：0．5：0．07，反应时间为40min，反应温度为30℃，可膨胀石墨的膨胀容积为280mL／g；不含硫，含氮量为1．27％，其终端产品柔性石墨不含氮．迄今为止，未见文献报道．","authors":[{"authorName":"宋克敏","id":"941ede1c-cb00-422b-baf6-c9dbb06fa23a","originalAuthorName":"宋克敏"},{"authorName":"刘金鹏","id":"81484e0c-6eac-4b7d-b18c-847ce1798ef7","originalAuthorName":"刘金鹏"},{"authorName":"靳通收","id":"a8013688-73a3-4761-9314-cc2d1096a1a9","originalAuthorName":"靳通收"},{"authorName":"李国山","id":"98203f25-c278-433a-ae93-b1c20c004936","originalAuthorName":"李国山"}],"categoryName":"|","doi":"","fpage":"252","id":"24fefed5-f091-4247-9bd2-f72d7dd29443","issue":"2","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"8f4f2c83-0916-48c3-b890-a92e6efd846a","keyword":"无硫可膨胀石墨","originalKeyword":"无硫可膨胀石墨"},{"id":"70211c41-a042-40b2-bc00-df5d0db1e753","keyword":" preparation","originalKeyword":" preparation"},{"id":"d4c64cbf-6d72-4935-87b2-541bf6b23cb1","keyword":" acetic anhydride","originalKeyword":" acetic anhydride"},{"id":"613e2f04-560f-45b2-b489-f3904bbd96d7","keyword":" 65% nitric acid","originalKeyword":" 65% nitric acid"}],"language":"zh","publisherId":"1000-324X_1997_2_23","title":"制备无硫可膨胀石墨的研究","volume":"12","year":"1997"},{"abstractinfo":"以报废液体推进剂硝酸-27S、鳞片石墨、高锰酸钾、硫酸和冰醋酸为原料,采用化学氧化法制备高倍可膨胀石墨.考察了高锰酸钾、硝酸-27S(水吸收液)、冰醋酸用量等因素对可膨胀石墨膨胀容积的影响;通过正交实验确定最佳工艺;采用扫描电镜(SEM)和X射线衍射(XRD)对可膨胀石墨进行表征.结果表明:最佳工艺为鳞片石墨(g):高锰酸钾(g):硝酸-27S(水吸收液)(mL):硫酸(mL):冰醋酸(mL)=1∶1∶1.25∶1.25∶2,于40℃下反应90 min,所获可膨胀石墨的最大膨胀容积为320 mL·g-1;对膨胀容积影响最大的因素为KMnO4用量;SEM和XRD证实了石墨层间化合物的存在.","authors":[{"authorName":"陈雅萍","id":"4e760a28-e593-40f8-9b8e-6fcaec225c5f","originalAuthorName":"陈雅萍"},{"authorName":"罗瑞盈","id":"ffb677a2-0b38-4794-9696-9a5826010065","originalAuthorName":"罗瑞盈"},{"authorName":"李舒艳","id":"ef444bd4-2445-4b3c-bc10-e3d7f732a5dc","originalAuthorName":"李舒艳"},{"authorName":"张剑","id":"8578d58b-aacd-4cba-bc40-06bf26e1cbca","originalAuthorName":"张剑"},{"authorName":"李辉","id":"ba554550-ef53-4474-aaa8-8a0f9eb27658","originalAuthorName":"李辉"},{"authorName":"王煊军","id":"56a5b366-c913-45a0-b22e-bf4714ac56e8","originalAuthorName":"王煊军"},{"authorName":"张江松","id":"e86a2877-9739-4641-99f9-155e2b94b1d7","originalAuthorName":"张江松"}],"doi":"","fpage":"465","id":"edd8ea44-77b5-4765-aa55-e105f458a16a","issue":"6","journal":{"abbrevTitle":"XXTCL","coverImgSrc":"journal/img/cover/XXTCL.jpg","id":"70","issnPpub":"1007-8827","publisherId":"XXTCL","title":"新型炭材料"},"keywords":[{"id":"7a72a0fb-9524-4386-bf01-2ab5ad4032bb","keyword":"硝酸-27S","originalKeyword":"硝酸-27S"},{"id":"a0d8bfdb-61c6-4ac9-88eb-3c43e861d941","keyword":"正交实验","originalKeyword":"正交实验"},{"id":"fd3a136b-e819-4c13-9897-07e9d575ccdf","keyword":"可膨胀石墨","originalKeyword":"可膨胀石墨"},{"id":"16ae973d-8a46-4f36-8afe-087baf578e6f","keyword":"制备","originalKeyword":"制备"}],"language":"zh","publisherId":"xxtcl201106011","title":"利用硝酸-27S制备高倍可膨胀石墨","volume":"26","year":"2011"},{"abstractinfo":"本文利用环氧树脂E-51和固化剂聚醚胺WHR-H023(质量比为3∶1)制成树脂基体.采用H2 SO4和HNO3对颗粒尺寸为80目的可膨胀石墨进行表面酸化处理,制备亲水性酸化可膨胀石墨;并将酸化处理的可膨胀石墨及未经酸化处理的可膨胀石墨分别对上述树脂基体进行阻燃改性,石墨添加量为5％、10％和15％.借助红外光谱分析仪检测酸化处理的可膨胀石墨表面羧基、羟基等官能团的接枝情况;利用极限氧指数分析仪和万能材料试验机分别测试改性树脂基体材料的极限氧指数(LOI)及拉伸性能;采用扫描电子显微镜(SEM)观察改性树脂基体材料的断面.研究结果表明,酸化可膨胀石墨比未经酸化处理的可膨胀石墨对环氧树脂基体的阻燃效果更佳,且拉伸性能下降更少.","authors":[{"authorName":"冯古雨","id":"2e59c6b1-5801-4268-a39f-8217ed760a69","originalAuthorName":"冯古雨"},{"authorName":"曹海建","id":"01f91ad8-f98a-4ebb-a8ea-55a31b4ed882","originalAuthorName":"曹海建"},{"authorName":"张坤","id":"fad0011d-6d80-4eb5-9373-ffadeddbd1bf","originalAuthorName":"张坤"},{"authorName":"钱坤","id":"632653e5-6172-4388-8030-b79b2dfa7eac","originalAuthorName":"钱坤"}],"doi":"10.14136/j.cnki.issn 1673-2812.2016.05.018","fpage":"772","id":"478c8e01-2faf-412b-a246-6fafd32b4f17","issue":"5","journal":{"abbrevTitle":"CLKXYGCXB","coverImgSrc":"journal/img/cover/CLKXYGCXB.jpg","id":"13","issnPpub":"1673-2812","publisherId":"CLKXYGCXB","title":"材料科学与工程学报"},"keywords":[{"id":"b34ee690-9f6b-4bc5-a76f-485b95d53e63","keyword":"可膨胀石墨","originalKeyword":"可膨胀石墨"},{"id":"99e1de53-3156-4737-9d31-c08d6ac9e398","keyword":"环氧树脂E51","originalKeyword":"环氧树脂E51"},{"id":"93148150-fd5d-4ed5-a94e-8e746ae0179a","keyword":"聚醚胺WHR-H023","originalKeyword":"聚醚胺WHR-H023"},{"id":"13a6aafb-c32b-4328-9685-a988a1bdb07d","keyword":"极限氧指数","originalKeyword":"极限氧指数"},{"id":"3786280d-6edd-4777-b656-15ed64a62320","keyword":"拉伸性能","originalKeyword":"拉伸性能"}],"language":"zh","publisherId":"clkxygc201605018","title":"可膨胀石墨对环氧树脂的阻燃改性","volume":"34","year":"2016"},{"abstractinfo":"研究了一种以冰醋酸为反应介质,在少量浓H2SO4存在下,以重铬酸钾作为氧化剂制备低硫可膨胀石墨的新方法.在最佳制备条件下,可膨胀石墨产品的含硫量仅为0.68 %,膨胀石墨产品的含硫量为0.08 %,膨胀容积260 mL.g-1,水分0.105 %,挥发分5.5 %,灰分0.76 %,pH值5,并采用紫外分光光度计对产品进行了分析.","authors":[{"authorName":"李冀辉","id":"f68c62fc-7bcc-4f12-aea6-e2ebddc72e80","originalAuthorName":"李冀辉"},{"authorName":"黎梅","id":"c3c56066-a643-4565-bc7e-ddea3f134a1e","originalAuthorName":"黎梅"},{"authorName":"扈海英","id":"044d1416-b945-488c-b791-914cb8d46da6","originalAuthorName":"扈海英"},{"authorName":"高风格","id":"e8206034-aa00-4dde-8092-a442089d7275","originalAuthorName":"高风格"}],"doi":"10.3969/j.issn.1007-8827.1999.01.013","fpage":"65","id":"bf1e23dc-72eb-41bc-b89b-a0a3dff6d64a","issue":"1","journal":{"abbrevTitle":"XXTCL","coverImgSrc":"journal/img/cover/XXTCL.jpg","id":"70","issnPpub":"1007-8827","publisherId":"XXTCL","title":"新型炭材料"},"keywords":[{"id":"0bbe43d0-98af-4aab-b8b9-b82de53cc9c7","keyword":"低硫可膨胀石墨","originalKeyword":"低硫可膨胀石墨"},{"id":"00b86ac6-1e28-44d1-a31f-66558377111e","keyword":"制备","originalKeyword":"制备"},{"id":"d39d7a4d-c63c-4db9-9f80-e4ced27a593b","keyword":"介质","originalKeyword":"介质"},{"id":"1dc3e19f-c30c-41de-9e76-b14a0cb0131a","keyword":"含硫量","originalKeyword":"含硫量"}],"language":"zh","publisherId":"xxtcl199901013","title":"制备低硫可膨胀石墨的新方法","volume":"14","year":"1999"},{"abstractinfo":"采用化学氧化法,以石墨粉(≤30μm)为原料,硫酸与高锰酸钾为氧化剂,以及磷酸为辅助插层剂制备出具有高膨胀体积的可膨胀石墨(EG).通过XRD、Raman、SEM、EDS、FT-IR以及TG-DTA等测试手段对材料的微观结构、形貌、谱学特性及热稳定性进行表征分析.实验结果表明,当硫酸与磷酸体积比为2:1时,EG氧化-插层效果最好,在 400℃时膨胀体积达102ml/g.同时EG片层中含有P、S、Mn等元素,表明可能插入了磷酸、硫酸以及Mn的磷酸二氢盐、硫酸盐等物质.TG-DTA显示,EG的起始膨胀温度在160℃左右,且石墨在氧化-插层后,有序结构没有被完全破坏,部分石墨仍具有很好的耐热氧性.另外,探讨了EG可能的形成及膨胀机理.","authors":[{"authorName":"蒋文俊","id":"b08806d9-6ac2-43b5-a4b2-7b67c0f87727","originalAuthorName":"蒋文俊"},{"authorName":"方劲","id":"75ec9660-2492-4408-91bd-5c2422d87e09","originalAuthorName":"方劲"},{"authorName":"李哲曌","id":"c6557106-73c1-4d23-86e4-802f20ae696d","originalAuthorName":"李哲曌"},{"authorName":"杨绪杰","id":"98ffc298-e384-4b6c-a224-b62fb6778997","originalAuthorName":"杨绪杰"},{"authorName":"陆路德","id":"63b09a79-132f-4a28-8e33-dc9159242051","originalAuthorName":"陆路德"},{"authorName":"查培法","id":"42705f01-3910-4195-9c0c-91b658e8337e","originalAuthorName":"查培法"},{"authorName":"浦龙娟","id":"1fddf6e3-6d6d-4d78-aad6-54db009076c6","originalAuthorName":"浦龙娟"}],"doi":"","fpage":"200","id":"d61a9e69-cb38-43ba-9981-fecfd61753ac","issue":"2","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"87eb3762-a4e4-46f8-a9cd-3b5b37a9bd05","keyword":"石墨粉(≤30μm)","originalKeyword":"石墨粉(≤30μm)"},{"id":"d656bf4c-ed9e-4c98-891b-100017336882","keyword":"氧化-插层","originalKeyword":"氧化-插层"},{"id":"3247dd50-fad6-44c6-95b9-9718fd8a0a7b","keyword":"可膨胀石墨","originalKeyword":"可膨胀石墨"},{"id":"5188e252-008f-4e84-9f58-514db1d9bd55","keyword":"谱学特性","originalKeyword":"谱学特性"},{"id":"e2e511df-2b76-4d83-9627-a131f582e456","keyword":"表征","originalKeyword":"表征"}],"language":"zh","publisherId":"gncl201002006","title":"可膨胀石墨的制备及谱学特性研究","volume":"41","year":"2010"}],"totalpage":2604,"totalrecord":26033}