{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":3,"startPagecode":1},"records":[{"abstractinfo":"以R-(-)/S-(+)-4-(N,N-dimethylaminosulfonyl)-7-(3-iso-thiocyanatopyrrolidino)-2,1,3-benzoxadiazole (DBD-PyNCS)为手性荧光衍生化试剂,用反相高效液相色谱法(RP-HPLC)对DL-肾上腺素对映体进行分离.衍生化反应是在含有7%吡啶的溶剂中,65 ℃温度条件下反应35 min,生成具有荧光特性的肾上腺素非对映体衍生物(λex=460 nm, λem=550 nm).生成的非对映体衍生物在流动相为乙腈-水(体积比为28∶72),流速为1.0 mL/min时,在DiamonsilTMC18色谱柱(150 mm×4.6 mm i.d.,5 μm)上分离度可达2.6.肾上腺素对映体在0.07 g/L～0.50 g/L时与峰面积呈良好的线性关系(r=0.9995),峰面积测定结果的相对标准偏差为4.3%(n=7),最低检测限为12 ng/L(S/N=3).","authors":[{"authorName":"金东日","id":"bf9b8e83-f511-4540-ae5f-5cfcbb387cd0","originalAuthorName":"金东日"},{"authorName":"马奎蓉","id":"641df62f-6062-470c-8cf2-3203c4eb917a","originalAuthorName":"马奎蓉"},{"authorName":"张小勇","id":"c641972c-6e58-473f-b311-147a8060ac9f","originalAuthorName":"张小勇"},{"authorName":"吴信子","id":"b3ebf795-f70d-4459-a47d-adde26712e4c","originalAuthorName":"吴信子"},{"authorName":"崔胜云","id":"b4a273bf-869e-415f-8d04-a6f210405a99","originalAuthorName":"崔胜云"},{"authorName":"<span style=\"color:red\">朱</span><span style=\"color:red\">玉兰</span>","id":"c435ec07-a576-44e1-ba7c-8e4342fca2b9","originalAuthorName":"朱玉兰"},{"authorName":"丰冈利正","id":"055e08e8-24e5-4d2f-9b62-550efac72f62","originalAuthorName":"丰冈利正"}],"doi":"10.3321/j.issn:1000-8713.2002.04.004","fpage":"304","id":"0addb74d-7a75-4f36-bbe6-d975e67307c6","issue":"4","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"f494bd53-fec3-42d8-9e4a-b10aefa77e51","keyword":"手性荧光衍生化试剂","originalKeyword":"手性荧光衍生化试剂"},{"id":"4948b8d2-057c-444e-8a2f-92c4be56ac3d","keyword":"反相高效液相色谱法","originalKeyword":"反相高效液相色谱法"},{"id":"ef3a9bc1-2198-4837-bf49-47f3cced331b","keyword":"肾上腺素对映体","originalKeyword":"肾上腺素对映体"}],"language":"zh","publisherId":"sp200204004","title":"手性荧光衍生化反相高效液相色谱法分离肾上腺素对映体","volume":"20","year":"2002"},{"abstractinfo":"以硼氢化钾(KBH4)为还原剂,采用化学镀法制备了纳米Ni-B包覆Al复合粉末,研究了镀液组分及工艺对包覆效果的影响,获得了制备复合粉末的优化条件.采用SEM,XRD,ICP和BET对复合粉末的表面形貌、物相结构、元素组成和比表面积进行了表征分析.结果表明:纳米Ni-B在Al表面包覆连续、均匀,且纳米Ni-B呈非晶态,粒径80～100 nm,化学组成约为Ni_(72)B_(28),纳米Ni-B/Al复合粉末比表面积达到了26.21m~2·g~(-1).","authors":[{"authorName":"程志鹏","id":"e43ec2d5-e455-4933-9607-fe445d562212","originalAuthorName":"程志鹏"},{"authorName":"徐继明","id":"fdcbbef4-bc8d-4a2a-886a-1e73a10b42de","originalAuthorName":"徐继明"},{"authorName":"<span style=\"color:red\">朱</span><span style=\"color:red\">玉兰</span>","id":"65c162a9-9ead-452d-aea6-c7417dae2883","originalAuthorName":"朱玉兰"},{"authorName":"李栋","id":"0dc05b6a-b998-43d4-83c4-3783e633b2ff","originalAuthorName":"李栋"},{"authorName":"杨毅","id":"9c31ee8f-a52a-4d9f-ac02-59ea7289281f","originalAuthorName":"杨毅"},{"authorName":"李凤生","id":"ab91749b-d63e-4875-a5b2-3c8f41e56c9f","originalAuthorName":"李凤生"}],"doi":"10.3969/j.issn.1001-4381.2010.01.005","fpage":"19","id":"9e2232b7-efbd-4651-94c9-63d714386cd4","issue":"1","journal":{"abbrevTitle":"CLGC","coverImgSrc":"journal/img/cover/CLGC.jpg","id":"9","issnPpub":"1001-4381","publisherId":"CLGC","title":"材料工程"},"keywords":[{"id":"e976cdc9-2b09-400d-a604-4657045e3efa","keyword":"化学镀","originalKeyword":"化学镀"},{"id":"b7d5d33b-d37f-4006-9ba2-35506a2c92a8","keyword":"铝粉","originalKeyword":"铝粉"},{"id":"207dfa35-0a4d-4cfa-9739-734d06309b27","keyword":"包覆","originalKeyword":"包覆"},{"id":"0996da04-ad69-44ed-94d1-641bb19b06f3","keyword":"纳米复合粉末","originalKeyword":"纳米复合粉末"}],"language":"zh","publisherId":"clgc201001005","title":"化学镀法制备纳米Ni-B包覆Al复合粉末","volume":"","year":"2010"},{"abstractinfo":"基于量子一次一密和量子密钥分配,提出了一种在签名及验证过程中没有仲裁参与操作的量子签名协议.在签名过程中,将消息转化为量子比特,在量子比特上进行签名并附上和消息相关的身份信息.签名消息的传输文件采用帧结构的形式,在验证过程中,通信双方完全读取帧文件内容需要相互确认身份,并留下与消息相关的身份信息,因此满足了签名协议的不可否认性.","authors":[{"authorName":"周锐","id":"732dbfd0-9b75-46ae-ad93-3f3ec435ab17","originalAuthorName":"周锐"},{"authorName":"<span style=\"color:red\">朱</span><span style=\"color:red\">玉兰</span>","id":"1b77f948-a95a-4c9a-8e20-e7c30788e040","originalAuthorName":"朱玉兰"},{"authorName":"聂义友","id":"dbae4468-a6c7-4db3-ae1e-5abd3ffc0dbb","originalAuthorName":"聂义友"},{"authorName":"黄亦斌","id":"47f3b351-4d55-427b-ae50-4d314ccfe1fc","originalAuthorName":"黄亦斌"}],"doi":"10.3969/j.issn.1007-5461.2009.04.011","fpage":"442","id":"d30d1d9e-a9bf-404d-a1bf-5d061780ebc6","issue":"4","journal":{"abbrevTitle":"LZDZXB","coverImgSrc":"journal/img/cover/LZDZXB.jpg","id":"53","issnPpub":"1007-5461","publisherId":"LZDZXB","title":"量子电子学报   "},"keywords":[{"id":"bdb9d094-26ac-4e01-b08e-1a9f58e024ca","keyword":"量子光学","originalKeyword":"量子光学"},{"id":"f485f3d5-63b9-4238-a02b-d612f96b06a7","keyword":"量子签名协议","originalKeyword":"量子签名协议"},{"id":"447307bb-bfb1-482b-a1d1-93c881b3fc91","keyword":"量子一次一密","originalKeyword":"量子一次一密"},{"id":"46007199-4809-481d-baeb-233b3dfb659c","keyword":"帧结构","originalKeyword":"帧结构"}],"language":"zh","publisherId":"lzdzxb200904011","title":"不完全依赖仲裁的量子签名协议","volume":"26","year":"2009"},{"abstractinfo":"","authors":[{"authorName":"周建峰","id":"f8502bee-e552-4418-b247-7bdfe605a34d","originalAuthorName":"周建峰"},{"authorName":"陆惠锋","id":"d15b0023-b8c7-4de8-9692-78909e26aa69","originalAuthorName":"陆惠锋"},{"authorName":"顾惠丹","id":"cdffcaab-aa60-453c-ba94-18b37ad15b04","originalAuthorName":"顾惠丹"},{"authorName":"<span style=\"color:red\">朱</span><span style=\"color:red\">玉兰</span>","id":"aef20a3b-fc2f-471d-ae8a-38de33e7edc2","originalAuthorName":"朱玉兰"},{"authorName":"屠树江","id":"01a8892a-d3d1-4b5e-827a-837348665266","originalAuthorName":"屠树江"}],"doi":"10.3969/j.issn.1000-0518.2005.08.025","fpage":"918","id":"c68488b9-af44-4666-9e18-a6314e614ef7","issue":"8","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"3fd42041-efa6-48fa-91cc-b88faddda9b9","keyword":"芳基咪唑","originalKeyword":"芳基咪唑"},{"id":"7e81a534-b51d-4abb-88bb-43f1acecad81","keyword":"二苯基二(甲)酮","originalKeyword":"二苯基二(甲)酮"},{"id":"9821f384-ae4f-442e-b8a3-54ee436edd35","keyword":"芳醛","originalKeyword":"芳醛"},{"id":"f9da67d8-5baf-4554-ab81-2a7a0d183421","keyword":"微波辐射","originalKeyword":"微波辐射"},{"id":"a6375a66-759b-45bc-b1a8-01fa5c28ac24","keyword":"合成","originalKeyword":"合成"}],"language":"zh","publisherId":"yyhx200508025","title":"微波辐射下一步合成2-芳基-4,5-二苯基咪唑衍生物","volume":"22","year":"2005"},{"abstractinfo":"简要综述了中高能重离子碰撞中K介子的产生及研究进展。重点介绍了K介子协变动力学模型,并在此框架内分析了中高能重离子碰撞中K＋介子以及与其伴随产生的Λ超子的集体流特征。结果表明：协变动力学模型能够很好地给出K＋介子和Λ超子的微分直接流。相对而言,软势给出的集体流与实验值符合更好。同时,通过对不同输运模型中K介子准粒子模型的基本属性进行对比分析,明确了协变动力学模型中K介子准粒子模型的质量及能量随核物质密度的变化特征,以及周围核子的运动对于K介子基本属性的影响。","authors":[{"authorName":"王艳艳","id":"349db626-5022-44aa-b8a7-f8039ec5a312","originalAuthorName":"王艳艳"},{"authorName":"<span style=\"color:red\">朱</span><span style=\"color:red\">玉兰</span>","id":"5d3dc1a8-160a-42ca-9637-eed714772e32","originalAuthorName":"朱玉兰"},{"authorName":"邢永忠","id":"bbe2620b-41c4-4b05-ac91-14392f07dee0","originalAuthorName":"邢永忠"},{"authorName":"郑玉明","id":"71800e59-a30c-4f6c-bc98-43e989de9d39","originalAuthorName":"郑玉明"}],"doi":"","fpage":"408","id":"de37f477-4138-47b2-b482-e04c4d1eff69","issue":"4","journal":{"abbrevTitle":"YZHWLPL","coverImgSrc":"journal/img/cover/YZHWLPL.jpg","id":"78","issnPpub":"1007-4627","publisherId":"YZHWLPL","title":"原子核物理评论   "},"keywords":[{"id":"877d6d27-669b-4cdc-8afd-123e6c22f8cc","keyword":"K介子","originalKeyword":"K介子"},{"id":"c4209eab-ee16-49be-9cd4-421f76cdda36","keyword":"协变动力学","originalKeyword":"协变动力学"},{"id":"30fab57f-13a7-4dca-b6d6-385cbf53ac75","keyword":"准粒子模型","originalKeyword":"准粒子模型"},{"id":"852e0434-0316-4c50-9b89-a2bcd60e826f","keyword":"基本属性","originalKeyword":"基本属性"}],"language":"zh","publisherId":"yzhwlpl201104005","title":"K介子协变动力学及其准粒子模型的性质","volume":"28","year":"2011"},{"abstractinfo":"利用浮游植物荧光仪对暴露于不同浓度白<span style=\"color:red\">玉兰</span>落叶水浸出液下微囊藻生长、最大光合作用效率（ Fv／Fm ）、实际光合作用效率[ Y（Ⅱ）]、光能利用效率（ alpha）和最大相对电子传递速率（ rETRmax）进行为期15 d的检测，分析白<span style=\"color:red\">玉兰</span>落叶浸出液对微囊藻的抑制效应和叶绿素荧光特性影响．结果发现，白<span style=\"color:red\">玉兰</span>落叶浸出液能有效抑制微囊藻的生长，呈明显浓度抑制型变化，抑藻能力随时间的延长而下降．低浓度（0．4、0．8、1．2、1．6 g·L－1）浸出液胁迫下，对微囊藻叶绿素荧光参数无显著影响；高浓度（2．0 g·L－1）浸出液胁迫下，在早期（4 d内）对荧光参数有极显著抑制作用．三维荧光图谱表明，在投量为2．0 g·L－1时，第15天色氨酸及酪氨酸荧光峰强度约为1．2 g·L－1投量情况下的1／3，同时腐殖酸的荧光峰强度减弱．第7—15天，藻细胞生长的半抑制浓度EC50值最小约为0．5—0．7 g·L－1．","authors":[{"authorName":"汪小雄","id":"c90bde08-7207-409e-bc7a-f2c3903e19a7","originalAuthorName":"汪小雄"},{"authorName":"姜成春","id":"2097f91e-86bc-4ca8-9181-210f1f765f48","originalAuthorName":"姜成春"},{"authorName":"汪晓军","id":"a0b650f2-10ce-4f92-81f1-dd2b5d7f527b","originalAuthorName":"汪晓军"},{"authorName":"谢炜平","id":"1fb5cbcc-f171-4640-bd4a-ad4f34cc87d2","originalAuthorName":"谢炜平"},{"authorName":"<span style=\"color:red\">朱</span>佳","id":"fffbf2f4-502a-45b0-a995-ece07f58e171","originalAuthorName":"朱佳"}],"doi":"10.7524/j.issn.0254-6108.2015.10.2015040901","fpage":"1867","id":"a73bb082-84d3-4c2b-8949-ae453749498d","issue":"10","journal":{"abbrevTitle":"HJHX","coverImgSrc":"journal/img/cover/HJHX.jpg","id":"43","issnPpub":"0254-6108","publisherId":"HJHX","title":"环境化学   "},"keywords":[{"id":"6770b89e-f759-4aa4-8f68-f29155f29808","keyword":"白<span style=\"color:red\">玉兰</span>","originalKeyword":"白玉兰"},{"id":"e3af230f-e85d-49f9-9c67-6707fbacb0a2","keyword":"铜绿微囊藻","originalKeyword":"铜绿微囊藻"},{"id":"424eb814-d01f-47c4-8963-5dc5f51c57ff","keyword":"化感作用","originalKeyword":"化感作用"},{"id":"daed3db0-9bb8-4e24-b959-f2549da04d24","keyword":"浮游植物荧光仪","originalKeyword":"浮游植物荧光仪"}],"language":"zh","publisherId":"hjhx201510015","title":"白<span style=\"color:red\">玉兰</span>落叶水浸出液抑制蓝藻生长和叶绿素荧光特性分析?","volume":"","year":"2015"},{"abstractinfo":"文中阐述了上<span style=\"color:red\">朱</span>车金矿的矿山概况、矿产资源、开采条件,结合矿山实际开采情况,采用类比法、价格法(经济盈亏平衡)对生产经济技术指标进行对比分析,及时调整了矿山工业指标,达到了经济、合理利用矿产资源的目的.","authors":[{"authorName":"唐俊智","id":"5e9bc3c8-dd53-4cd8-9325-633c95343c86","originalAuthorName":"唐俊智"}],"doi":"10.3969/j.issn.1001-1277.2006.11.006","fpage":"19","id":"8194c2ad-4362-423b-a975-dddc804890d2","issue":"11","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"c1734631-b747-41c3-bfef-5d76ff8b1771","keyword":"工业指标","originalKeyword":"工业指标"},{"id":"75e42fda-8c3b-43c8-8410-f3f95a49e706","keyword":"选择论证","originalKeyword":"选择论证"},{"id":"08308e7e-96b1-4c09-848f-dcfba760e94b","keyword":"上<span style=\"color:red\">朱</span>车金矿","originalKeyword":"上朱车金矿"}],"language":"zh","publisherId":"huangj200611006","title":"上<span style=\"color:red\">朱</span>车金矿工业指标的选择论证","volume":"27","year":"2006"},{"abstractinfo":"<span style=\"color:red\">朱</span>林西金矿床位于金山金矿田的中北部，是与韧-脆性剪切带有关的石英脉型、蚀变岩型金矿床。在综合研究和利用矿区以往地质地球化学资料基础上，选取矿区40号勘探线为典型地质剖面，对该剖面坑探工程控制的Ⅰ号金矿带进行系统采样和数据分析与统计计算。利用相关分析、聚类分析、因子分析方法，确定了金矿床的原生晕组合特征。通过绘制和分析原生晕元素轴向异常分布图和叠加图、地球化学参数计算图，初步归纳了矿床构造叠加晕总体特征，并分析了矿体原生晕特征的地质意义以及对深部盲矿体预测的应用。研究认为：As与 Au关系密切， As、Sb和Hg为金矿体的前缘指示元素组合；Pb、Zn、Cu分布于矿体周围，为矿体的近矿晕指示元素组合；Mo、Mn和Co元素为矿体的尾晕元素组合；尾晕的反带异常、前缘晕与尾晕叠加等特征对深部盲矿体预测有重要指示作用。","authors":[{"authorName":"丁高明","id":"cbc1409a-9e45-46b6-bb75-db95a0195d0d","originalAuthorName":"丁高明"},{"authorName":"卢树东","id":"a2c04c96-4776-4c99-9a8e-b043f1aae1ed","originalAuthorName":"卢树东"},{"authorName":"刘国荣","id":"15652333-9439-409c-959a-68a073a3abde","originalAuthorName":"刘国荣"},{"authorName":"肖淳","id":"a155b016-6e42-489e-b96a-e3d229caabce","originalAuthorName":"肖淳"}],"doi":"10.11792/hj20160904","fpage":"14","id":"d8f67118-529e-436d-8123-01d216051050","issue":"9","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"0fcef0d1-3d1f-4d6e-af5d-15512a7085bb","keyword":"原生晕","originalKeyword":"原生晕"},{"id":"77fe5818-8291-4e86-a483-91a6f5b4c95c","keyword":"<span style=\"color:red\">朱</span>林西金矿床","originalKeyword":"朱林西金矿床"},{"id":"966cb335-b420-440f-b0c4-b36d5399d98b","keyword":"金山金矿田","originalKeyword":"金山金矿田"},{"id":"7e2a1521-13ac-43d6-baa7-4835389f98eb","keyword":"盲矿体预测","originalKeyword":"盲矿体预测"}],"language":"zh","publisherId":"huangj201609004","title":"江西金山金矿田<span style=\"color:red\">朱</span>林西金矿床矿体原生晕特征","volume":"37","year":"2016"},{"abstractinfo":"LS-DYNA可以满足用户对某些材料本构关系子程序开发的要求.本文首先编制了各向同性线弹性材料本构模型子程序,计算单轴拉伸作用,得到材料子程序开发的可行性;另外主要编制了飞机风挡材料采用的具有应变率效应的非线性粘弹性<span style=\"color:red\">朱</span>-王-唐本构模型,结果能很好地对<span style=\"color:red\">朱</span>-王-唐模型进行描述,特别是应变率对该模型的影响.并用于真实风挡的计算,得到的数值结果与试验值比较吻合.","authors":[{"authorName":"冯震宙","id":"080ef325-5d8f-4493-baf2-395f9753a380","originalAuthorName":"冯震宙"},{"authorName":"王新军","id":"dbefb237-85be-4f86-ad6c-49a7fc3c44a0","originalAuthorName":"王新军"},{"authorName":"王富生","id":"1ad4e6d3-6e44-4be2-a4b4-a6a02a67cbae","originalAuthorName":"王富生"},{"authorName":"高行山","id":"c47026b5-8556-45b2-aff0-8ec452dcfe5e","originalAuthorName":"高行山"},{"authorName":"岳珠峰","id":"3ba1b48c-b919-450a-b7f0-ceced749af77","originalAuthorName":"岳珠峰"}],"doi":"10.3969/j.issn.1673-2812.2007.02.027","fpage":"269","id":"fd2e2c8d-9c37-4d2d-88a5-3819edd6ff21","issue":"2","journal":{"abbrevTitle":"CLKXYGCXB","coverImgSrc":"journal/img/cover/CLKXYGCXB.jpg","id":"13","issnPpub":"1673-2812","publisherId":"CLKXYGCXB","title":"材料科学与工程学报"},"keywords":[{"id":"ab9ca95b-98bf-4375-a3e3-afaffca62712","keyword":"非线性粘弹性本构关系","originalKeyword":"非线性粘弹性本构关系"},{"id":"17f17c9c-7394-4776-9321-b9a856ebaace","keyword":"材料子程序","originalKeyword":"材料子程序"},{"id":"5f2336c9-4355-43bf-a0aa-96f88fd1efe0","keyword":"风挡","originalKeyword":"风挡"},{"id":"f159c787-014f-46b7-ace7-1c65e7f345e6","keyword":"应变率","originalKeyword":"应变率"}],"language":"zh","publisherId":"clkxygc200702027","title":"<span style=\"color:red\">朱</span>-王-唐非线性粘弹性本构模型在有限元分析中的实现及其应用","volume":"25","year":"2007"},{"abstractinfo":"","authors":[{"authorName":"一生","id":"dda2ff4a-f111-4f7c-9cc4-1d8b2b804a61","originalAuthorName":"一生"}],"doi":"10.3969/j.issn.1000-6826.2001.01.011","fpage":"12","id":"42fa4344-5948-453c-acf8-c3d248a2e2da","issue":"1","journal":{"abbrevTitle":"JSSJ","coverImgSrc":"journal/img/cover/3abe017a-2574-4821-8152-4ae974ef0471.jpg","id":"47","issnPpub":"1000-6826","publisherId":"JSSJ","title":"金属世界"},"keywords":[{"id":"c55c09ab-e029-4603-8152-4a02033f5802","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"jssj200101011","title":"红墙金瓦倍关情——访故宫文物专家<span style=\"color:red\">朱</span>家","volume":"","year":"2001"}],"totalpage":3,"totalrecord":26}