{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"研究了在AZ31B镁合金表面以硫酸镍和碱式碳酸镍为主盐镀液体系化学镀Ni-P.通过扫描电镜(SEM)、能谱分析(EDX)、X射线衍射(XRD)及动电位极化曲线分析,探讨了2种不同镀层的组织形貌、物相成分及耐蚀性.结果表明:两种不同镍盐体系均能得到致密、均匀、无缺陷的Ni-P镀层;磷的含量相近,质量分数分别为6.67%,6.60%,属于中磷镀层;镀层的腐蚀电位分别为-0.24,-0.37 V(vs SCE).比较两种镀层发现,以硫酸镍为主盐体系得到的镀层晶胞更细小,均匀、致密;镀层腐蚀电位正移了0.1 V,钝化区间更为明显,耐蚀性能更为优异.","authors":[{"authorName":"徐二领","id":"d7d5b00a-bc7b-4a16-9366-70c9d48c8cf9","originalAuthorName":"徐二领"},{"authorName":"董云会","id":"6e92e033-b555-4e36-9b3d-46594c1dde6a","originalAuthorName":"董云会"}],"doi":"","fpage":"23","id":"797aef63-37b2-4136-9367-a90cb0a4fc05","issue":"7","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"a126da7f-e0b3-4ca9-903a-6051e689e527","keyword":"化学镀Ni-P","originalKeyword":"化学镀Ni-P"},{"id":"22182f79-5f66-4efa-9bd1-971b5b206a9d","keyword":"镁合金","originalKeyword":"镁合金"},{"id":"bd106d50-abc6-4867-ad31-5525506b680d","keyword":"硫酸镍镀液","originalKeyword":"硫酸镍镀液"},{"id":"f1a54024-9dd1-4cb6-8e7f-b642c48ada8b","keyword":"碱式碳酸镍镀液","originalKeyword":"碱式碳酸镍镀液"},{"id":"1f2e07bd-4e73-45f0-bab0-474012bfdac4","keyword":"耐蚀性","originalKeyword":"耐蚀性"}],"language":"zh","publisherId":"clbh200807009","title":"两种镍盐体系中镁合金表面化学镀Ni-P层的结构性能","volume":"41","year":"2008"},{"abstractinfo":"为了比较镁合金化学镀镍中主盐性质的影响,分别采用硫酸镍(NiSO4·6H2O)和碱式碳酸镍[NiCO3·2Ni(OH)2·2H2O]为主盐对AZ91D镁合金进行化学镀镍.采用扫描电镜(SEM)比较了镀层的表面形貌和组织结构,用能谱(EDS)对2种主盐所得镀层进行成分分析,采用中性盐雾试验比较了不同主盐化学镀镍后镀层的耐腐蚀性,并通过热震和锉刀试验比较两者的结合力,最后在3.5%NaCl溶液中进行动电位极化曲线测试.结果表明,碱式碳酸镍作为镁合金化学镀主盐所得的镀层为高磷镀层,且致密性、耐腐蚀性和结合力均好于硫酸镍作为主盐的镀液.","authors":[{"authorName":"李东栋","id":"2add38b0-12d6-4404-9c33-39ac9eeef6c1","originalAuthorName":"李东栋"},{"authorName":"王凤平","id":"ebf246d2-5846-471d-9307-8dbb5c40f2c2","originalAuthorName":"王凤平"}],"doi":"","fpage":"37","id":"eff2180a-eab5-4b1a-8672-05897bda90a0","issue":"7","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"547801bf-f1c7-4c9b-84f1-08c8355f689e","keyword":"化学镀镍","originalKeyword":"化学镀镍"},{"id":"d6882ad9-3ba2-4c41-9807-a7ac385104bd","keyword":"镁合金","originalKeyword":"镁合金"},{"id":"c7f3afc4-e08a-4418-957b-1fd9028c0823","keyword":"主盐性质","originalKeyword":"主盐性质"}],"language":"zh","publisherId":"clbh200807013","title":"硫酸镍和碱式碳酸镍主盐对镁合金化学镀镍的影响","volume":"41","year":"2008"},{"abstractinfo":"研究了pH值、无机盐、丁炔二醇等对光亮镀镍体系中添加剂吡啶丙基硫代甜菜碱(PPS)吸光度的影响,建立了测定PPS浓度的紫外分光光度分析法.该方法快速、准确,可用于工业光亮镀镍电解液中PPS浓度的现场分析.","authors":[{"authorName":"高灿柱","id":"a7f9b885-10c8-4fef-9a06-ae20403e7c00","originalAuthorName":"高灿柱"},{"authorName":"郑莹","id":"1a288545-b92e-4ea1-8f49-e6a92fec407f","originalAuthorName":"郑莹"},{"authorName":"常宏文","id":"821cf3b3-dcb3-4d2e-a3c3-35749f2f839a","originalAuthorName":"常宏文"},{"authorName":"隋华","id":"87e0fe29-6e4e-46e5-8956-67d6f2bd4bf1","originalAuthorName":"隋华"}],"doi":"10.3969/j.issn.1001-1560.2001.08.018","fpage":"42","id":"9d62b6ac-2946-4937-9bae-4c22141b217e","issue":"8","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"acb13615-0788-4877-96a6-7bcba2e9701c","keyword":"光亮镀镍","originalKeyword":"光亮镀镍"},{"id":"823d9797-9dc7-4743-a694-8b6471fc7ed7","keyword":"添加剂","originalKeyword":"添加剂"},{"id":"173052a9-f0f0-4902-8e42-d6162f16c317","keyword":"吡啶 丙基硫代甜菜碱","originalKeyword":"吡啶 丙基硫代甜菜碱"},{"id":"acebe030-c172-4e54-afbb-041236ed0f7d","keyword":"分析","originalKeyword":"分析"}],"language":"zh","publisherId":"clbh200108018","title":"镀镍液中吡啶丙基硫代甜菜碱的测定","volume":"34","year":"2001"},{"abstractinfo":"采用紫外分光光度分析法研究了pH值、无机盐、丁炔二醇等对光亮镀镍体系中添加剂吡啶鎓羟丙基硫代甜菜碱(PPSOH)吸光度的影响,建立了电镀液中测定PPSOH浓度的分析方法,并应用于电镀实验中.\n","authors":[{"authorName":"郑莹","id":"d7e66b6d-f373-4163-a1bf-1f6fd9eba461","originalAuthorName":"郑莹"},{"authorName":"高灿柱","id":"e8efc892-76b0-400e-9e9d-560be9ddb642","originalAuthorName":"高灿柱"},{"authorName":"隋华","id":"3e1aee43-f637-4ba8-82d9-994408ca4b48","originalAuthorName":"隋华"}],"doi":"10.3969/j.issn.1001-1560.2002.06.021","fpage":"46","id":"63850ca3-2e44-4261-b425-17a9eba44c1b","issue":"6","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"4edb9e7b-7efd-4c8d-ab24-42ac826f75fb","keyword":"光亮镀镍","originalKeyword":"光亮镀镍"},{"id":"56e0948b-0967-438b-9eb1-0d1c5aa011b2","keyword":"添加剂","originalKeyword":"添加剂"},{"id":"b508bfd2-c8eb-4675-b0ae-4a8f58ebef7d","keyword":"吡啶鎓羟丙基硫代甜菜碱","originalKeyword":"吡啶鎓羟丙基硫代甜菜碱"},{"id":"471d0dbc-c08b-4e5d-8f85-19cd0b314563","keyword":"分析","originalKeyword":"分析"}],"language":"zh","publisherId":"clbh200206021","title":"光亮镀镍液中吡啶鎓羟丙基硫代甜菜碱的测定","volume":"35","year":"2002"},{"abstractinfo":"以七水硫酸锌(ZnSO4.7H2O)和碳酸氢铵(NH4HCO3)为原料,以聚乙二醇-400(PEG-400)为模板,通过室温固相反应制备了碳酸锌(ZnCO3)和碱式碳酸锌(ZnCO3.3Zn(OH)2.H2O,basic zinc carbon-ate,BZC)。通过XRD测试及其半定量成分分析,研究了PEG-400剂量和NH4HCO3与ZnSO4.7H2O摩尔比x值对合成产物物相的影响。总结了PEG-400模板辅助合成ZnCO3和BZC的反应机制。结果表明,PEG-400包覆ZnSO4.7H2O颗粒形成模板,模板层的厚度影响固相反应的微观机制———薄层单向扩散与厚层互扩散,局部微环境的酸碱性决定着产物物相,酸性抑制ZnCO3水解,碱性促进ZnCO3水解生成BZC。由据此设计的较高x值(x=3.0)、较低PEG-400剂量(70μL)的合成工艺,制备了单相BZC粉体。","authors":[{"authorName":"刘长友","id":"03e4a4c0-9206-4704-9447-3b77525559f6","originalAuthorName":"刘长友"},{"authorName":"介万奇","id":"34b58d9c-345a-4f56-bde6-64d6d3d0df0b","originalAuthorName":"介万奇"},{"authorName":"王涛","id":"514e0842-24eb-47a1-ac65-2700baab4c52","originalAuthorName":"王涛"},{"authorName":"查钢强","id":"3a85cd1d-6949-4688-817e-09556cf4d3a0","originalAuthorName":"查钢强"},{"authorName":"谷智","id":"7a7b7581-2f52-4519-8e06-c7e36fe8b604","originalAuthorName":"谷智"},{"authorName":"孙晓燕","id":"41ee83fa-266c-4abc-b950-fddde0b3b2f5","originalAuthorName":"孙晓燕"}],"doi":"","fpage":"537","id":"7a2cd20e-8aa1-4e41-8765-a13b079dba33","issue":"4","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"ff4d5589-f540-422e-856e-34555de035b5","keyword":"碳酸锌","originalKeyword":"碳酸锌"},{"id":"0902b3af-4fde-4b02-be04-fe95d463c33c","keyword":"碱式碳酸锌","originalKeyword":"碱式碳酸锌"},{"id":"485a9e37-86f6-4854-8656-2381e1807d7c","keyword":"固相反应","originalKeyword":"固相反应"},{"id":"466470b5-c5df-4298-a74a-6b462e50966f","keyword":"合成","originalKeyword":"合成"}],"language":"zh","publisherId":"gncl201204034","title":"室温固相反应合成碱式碳酸锌","volume":"43","year":"2012"},{"abstractinfo":"通过腐蚀实验和阳极极化曲线研究了硫酸镍主盐配制的化学镀镍液成分和温度对AZ91D镁合金的腐蚀行为的影响,比较了碱式碳酸镍主盐和硫酸镍主盐两种镀镍液的腐蚀性以及施镀后的镀层质量.结果表明:硫酸镍镀液的腐蚀性比碱式碳酸镍镀液大,在低温下,镁合金在硫酸镍镀液中表面的氟化镁膜不致密,镀液对基材的腐蚀性高;而在高温下,Mg2+与F-的反应性增强,氟化反应完全,形成的氟化镁钝化膜致密性高,可保护镁合金基体免遭镀液的腐蚀.在施镀温度下,镀液中F-的缓蚀作用,可使SO24-离子对镁合金的腐蚀速率大大降低.","authors":[{"authorName":"胡波年","id":"e1b84693-7158-4bef-91cd-fb8ba99fa404","originalAuthorName":"胡波年"},{"authorName":"陈珏伶","id":"c00fd12f-0a59-48ae-a67e-ee826e156733","originalAuthorName":"陈珏伶"},{"authorName":"余刚","id":"3cff9ca3-8caa-4ade-81ea-e775a74d14fd","originalAuthorName":"余刚"},{"authorName":"刘正","id":"4cb66506-c780-40cc-9d78-e1092bb0bdf1","originalAuthorName":"刘正"},{"authorName":"叶立元","id":"8d4c4e67-b3bb-4777-a11c-ab2c800144d8","originalAuthorName":"叶立元"}],"doi":"","fpage":"463","id":"7b056da0-6549-4f41-b91d-79d6c3b95db3","issue":"3","journal":{"abbrevTitle":"ZGYSJSXB","coverImgSrc":"journal/img/cover/ZGYSJSXB.jpg","id":"88","issnPpub":"1004-0609","publisherId":"ZGYSJSXB","title":"中国有色金属学报"},"keywords":[{"id":"e8cf761c-c179-4f08-aff0-df06d18c8184","keyword":"AZ91D镁合金","originalKeyword":"AZ91D镁合金"},{"id":"e7bd9ea8-6847-4121-977b-0991f0d98ef4","keyword":"镀液腐蚀","originalKeyword":"镀液腐蚀"},{"id":"5679f332-169d-4f86-8fb3-9fb6e7dc8e63","keyword":"化学镀镍","originalKeyword":"化学镀镍"},{"id":"261df234-69a3-44af-bbea-0c200fff2f49","keyword":"硫酸镍","originalKeyword":"硫酸镍"}],"language":"zh","publisherId":"zgysjsxb200503024","title":"镁合金在镀液中的腐蚀行为","volume":"15","year":"2005"},{"abstractinfo":"以碳酸铵和硝酸锌为原料对碱式碳酸锌前驱体的合成实验进行了分析研究.实验发现,碳酸铵与硝酸锌的物质的量比是碱式碳酸锌合成中影响碱式碳酸锌收率的主要因素,当物质的量比为1.5时碱式碳酸锌的收率最高.X射线衍射(XRD)、热分析(DSC-TG)和扫描电子显微镜(SEM)对实验样品的测试表明,所得碱式碳酸锌前驱体的主要存在形式为Zn4CO3(OH)6·H2O,其煅烧产物为晶粒尺寸在20~50nm之间的六方ZnO纳米粒子,粒子呈近球形,分散性好.","authors":[{"authorName":"刘萍","id":"cfbf1516-3d86-4fa7-a062-ce7b49bdf849","originalAuthorName":"刘萍"},{"authorName":"陈长春","id":"a3e15ed1-4b9a-4bf8-9958-3880a74170f2","originalAuthorName":"陈长春"},{"authorName":"陆春华","id":"ca87cbbf-5313-477b-af8a-4ca8d527a6b8","originalAuthorName":"陆春华"}],"doi":"","fpage":"49","id":"6d732d45-1ed2-47e7-a9b9-c1f9f4792893","issue":"z3","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"e11d199c-a5c3-46cb-9d6c-1937d71b8522","keyword":"碱式碳酸锌","originalKeyword":"碱式碳酸锌"},{"id":"b86de1d1-6b1e-449f-9d02-d97552f2dd85","keyword":"氧化锌","originalKeyword":"氧化锌"},{"id":"8f8018b8-af4e-4d4e-bfc3-f7ecf7227d14","keyword":"正交实验","originalKeyword":"正交实验"}],"language":"zh","publisherId":"cldb2008z3017","title":"纳米氧化锌制备所需碱式碳酸锌的实验研究","volume":"22","year":"2008"},{"abstractinfo":"在稀土湿法冶金生产工艺中实现了锌与稀土的萃取分离,制备出优于国标的碱式碳酸锌产品,对该产品进行了X射线衍射分析和经过原子吸收光谱对产品进行碳含量的分析,确定合成的碱式碳酸锌主要是以Zn5(CO3)2(OH)6形式存在.","authors":[{"authorName":"李慧琴","id":"5c2082dd-af46-41c7-9966-483c296da538","originalAuthorName":"李慧琴"},{"authorName":"张瑞祥","id":"494e63be-30da-49f7-9107-b9d4ace83d5f","originalAuthorName":"张瑞祥"},{"authorName":"刘海旺","id":"2ba512a9-4b5a-4c04-ab80-c0d9843d90b6","originalAuthorName":"刘海旺"},{"authorName":"王士智","id":"85402b85-d869-4d78-9b88-f080c4e498f8","originalAuthorName":"王士智"}],"doi":"10.3969/j.issn.1004-0277.2006.06.016","fpage":"62","id":"e3840bba-2892-4b23-8dfa-a5500acf5761","issue":"6","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"95855758-0e0a-486d-9721-2d6a0203f94f","keyword":"锌","originalKeyword":"锌"},{"id":"f5645938-19ae-4bdd-9ade-89d8219475e4","keyword":"稀土","originalKeyword":"稀土"},{"id":"f02d34b4-a0fc-4049-ba62-298ef69d9727","keyword":"萃取分离","originalKeyword":"萃取分离"},{"id":"56ea2d24-16e3-495d-aa85-d941e6ae16d8","keyword":"碱式碳酸锌","originalKeyword":"碱式碳酸锌"}],"language":"zh","publisherId":"xitu200606016","title":"锌与稀土分离及碱式碳酸锌的制备","volume":"27","year":"2006"},{"abstractinfo":"介绍了用高锰酸钾处理转化镍-铁合金镀液为亮镍镀液的工艺过程,结果表明,转化后的镀液澄清,试镀工件质量良好,方法简单易行,具有良好的经济性和可行性.","authors":[{"authorName":"蔡元兴","id":"7173cf4c-2ea5-470f-80d6-f39600eeec5f","originalAuthorName":"蔡元兴"}],"doi":"10.3969/j.issn.1001-1560.2006.12.022","fpage":"72","id":"7f2e81a3-a6b7-479c-a839-d1d9a1ca6c73","issue":"12","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"a55ea88f-4a32-4531-b11c-fc22c193cd96","keyword":"镍-铁合金镀液","originalKeyword":"镍-铁合金镀液"},{"id":"ff65835c-6144-4115-aab2-16e57f1d5efb","keyword":"高锰酸钾","originalKeyword":"高锰酸钾"},{"id":"67934843-8739-4658-a5a0-eb14ab9a189b","keyword":"亮镍镀液","originalKeyword":"亮镍镀液"},{"id":"e2f24e72-db6f-4395-a114-641e46df3aa2","keyword":"转化","originalKeyword":"转化"}],"language":"zh","publisherId":"clbh200612022","title":"镍-铁合金镀液的转化","volume":"39","year":"2006"},{"abstractinfo":"黑镍镀液是镀镍工序中常用的一种工序,它的电镀效果较好.但是其镀液的分析方法却很复杂,且鲜有资料系统地提出其详细的分析资料.现提供一种黑镍镀液中主要成分硫酸镍、硫酸锌、硫酸镍铵、硫氰酸铵及硼酸的分析方法,以供大家参考.","authors":[{"authorName":"李成虹","id":"8926fac8-ee2b-4840-8732-566bdb97fabf","originalAuthorName":"李成虹"}],"doi":"10.3969/j.issn.1001-3849.2004.03.010","fpage":"36","id":"606be320-1656-4b19-9938-ddccd4ce64ab","issue":"3","journal":{"abbrevTitle":"DDYJS","coverImgSrc":"journal/img/cover/DDYJS.jpg","id":"20","issnPpub":"1001-3849","publisherId":"DDYJS","title":"电镀与精饰 "},"keywords":[{"id":"007c5658-fe97-4ba2-8e30-9a28cc34a338","keyword":"黑镍镀液","originalKeyword":"黑镍镀液"},{"id":"ba977eeb-6b75-44d8-abb7-fbcda3f90727","keyword":"硫酸镍","originalKeyword":"硫酸镍"},{"id":"535d3590-ad00-4fd8-b886-101b5f7cd91c","keyword":"硫酸锌","originalKeyword":"硫酸锌"},{"id":"b7d7f0a8-cc4e-4832-a731-58164af44dfd","keyword":"硫酸镍铵","originalKeyword":"硫酸镍铵"},{"id":"b2cfe5a3-6680-4f73-aeb0-6c8454f4dc58","keyword":"硫氰酸铵","originalKeyword":"硫氰酸铵"},{"id":"29982d74-03dc-4915-b1d3-ebf61ed57f36","keyword":"硼酸","originalKeyword":"硼酸"}],"language":"zh","publisherId":"ddjs200403010","title":"黑镍镀液的分析","volume":"26","year":"2004"}],"totalpage":3689,"totalrecord":36890}