金属学报(英文版), 2013, 26(3): 265-270. doi: 10.1007/s40195-012-0175-4
{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以硝酸铁、硝酸铬、柠檬酸、乙二醇为原料,采用溶胶-凝胶法制备了纳米近红外高反射率黑色陶瓷颜料,探讨了Fe/Cr摩尔比、水解温度、溶液pH值、金属离子浓度、煅烧温度等因素对溶胶-凝胶过程及样品性能的影响.结果表明,在Fe/Cr摩尔比为0.50,水解温度70℃,溶液pH值=3～4,金属离子浓度为2.5～3.5mol/L,煅烧温度为900℃时,制备的颜料主晶相为CrL3Fe0.7O3,平均颗粒尺寸为50～150nm,在700～2500nm波段内的平均反射率为77.58％.","authors":[{"authorName":"张潇予","id":"5c286d73-1a8f-4800-863f-fe8896c22a1e","originalAuthorName":"张潇予"},{"authorName":"张玉军","id":"e5546d41-06fb-4da4-866b-1979da63f4d2","originalAuthorName":"张玉军"},{"authorName":"龚红宇","id":"f10180b9-04e0-4c3a-90fc-3a1f308f2727","originalAuthorName":"龚红宇"},{"authorName":"王翠玲","id":"0bf478fd-5ec6-4a06-8227-039386a44b9f","originalAuthorName":"王翠玲"},{"authorName":"赵新巧","id":"b409c58f-efad-434b-8bb8-07e81e82f93c","originalAuthorName":"赵新巧"},{"authorName":"朱洪立","id":"4b6ce684-a41c-4d66-b690-c2913af18166","originalAuthorName":"朱洪立"},{"authorName":"熊天农","id":"af4780ea-5eeb-4a16-a9a6-c39487a369c0","originalAuthorName":"熊天农"}],"doi":"","fpage":"417","id":"e13b926e-5ef6-45fd-9dc0-cd8b8ac3132b","issue":"3","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"34a16a33-0d31-4479-8a36-14eb9aa908d8","keyword":"溶胶-凝胶","originalKeyword":"溶胶-凝胶"},{"id":"181683e0-32eb-4e35-84e3-0f9423ad177a","keyword":"近红外","originalKeyword":"近红外"},{"id":"e5f64a9e-c754-465e-9428-520b0f3022f7","keyword":"高反射率","originalKeyword":"高反射率"},{"id":"bb2c1547-876b-4a4a-8ba0-06202b5403e7","keyword":"纳米","originalKeyword":"纳米"},{"id":"3d4ad28c-6136-4326-9edd-82c39499255f","keyword":"颜料","originalKeyword":"颜料"}],"language":"zh","publisherId":"gncl201303028","title":"溶胶-凝胶法制备纳米近红外高反射率黑色陶瓷颜料","volume":"44","year":"2013"},{"abstractinfo":"结合野外工作和前人资料,对华熊地块熊耳山地区金矿床进行了分析,认为该区金矿床从控矿构造和围岩蚀变特征上可划分为两类,矿床的流体包裹体、成矿温度以及盐度特征,说明了它们的形成均与中生代富钾质、富含挥发组分的花岗质岩体(100～140Ma)有关,主要形成于挤压向拉张环境中.该区金矿床属于与侵入岩有关的金矿系统中的浅成低温热液矿床,可与近年来在环太平洋带发现的斑岩型金矿对比.","authors":[{"authorName":"马桂霞","id":"e551ff77-bf17-4c56-95e2-e3dd23b1dff0","originalAuthorName":"马桂霞"},{"authorName":"朱海","id":"77bcaeb7-13cc-4f71-a0f2-b238e2edcf74","originalAuthorName":"朱海"}],"doi":"10.3969/j.issn.1001-1277.2004.10.005","fpage":"15","id":"17268516-903f-4f7c-9420-307022cc8449","issue":"10","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"0ae9ffbe-2a7b-4afe-a5d8-35c2167eaf84","keyword":"华熊地块","originalKeyword":"华熊地块"},{"id":"509ec8be-f883-4b6b-ae3f-343aab5f4341","keyword":"金矿床","originalKeyword":"金矿床"},{"id":"3a8413a1-2823-48ba-94c9-2d95a076df65","keyword":"浅成低温热液型","originalKeyword":"浅成低温热液型"},{"id":"23266d01-2191-4d7b-bbd8-7a44a6b20275","keyword":"控制因素","originalKeyword":"控制因素"}],"language":"zh","publisherId":"huangj200410005","title":"华熊地块熊耳山地区金矿床特征及控矿因素研究","volume":"25","year":"2004"},{"abstractinfo":"农坪金(铜)矿床是以英云闪长斑岩为赋矿主岩的斑岩型矿床,矿床受斑岩体、闪长玢岩脉及断裂构造控制.该文在总结了矿床成矿地质特征及控矿因素基础上,提出了寻找该类型矿床的主要找矿标志.","authors":[{"authorName":"孙超","id":"d0c9146c-d687-4e5a-bb1c-742e6be55242","originalAuthorName":"孙超"},{"authorName":"张继武","id":"27d5f19f-7bc3-4c6f-8eed-fac7ab129509","originalAuthorName":"张继武"}],"doi":"10.3969/j.issn.1001-1277.2002.07.002","fpage":"4","id":"eda812e0-10ca-4ae2-b003-59465ddb47db","issue":"7","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"83a42d2b-32b0-4905-9f41-980acf6d2d47","keyword":"斑岩型金(铜)矿床","originalKeyword":"斑岩型金(铜)矿床"},{"id":"5b1979e8-0a6e-4a51-8462-acfb00bc8035","keyword":"地质特征","originalKeyword":"地质特征"},{"id":"d32bca1b-5acc-48fb-be06-9502e555f942","keyword":"找矿标志","originalKeyword":"找矿标志"}],"language":"zh","publisherId":"huangj200207002","title":"农坪斑岩型金(铜)矿床地质特征及找矿标志","volume":"23","year":"2002"},{"abstractinfo":"以熊果酸为原料,经C-3羟基氧化、C-28羧基苄酯化保护、C-2乙酰化及水解、还原、脱保护得到2β-羟基熊果酸,6步反应的总收率为60.1％.中间体及目标化合物结构经IR、1H NMR、13C NMR和MS测试技术确证.以噻唑蓝(MTT)比色法检测2β-羟基熊果酸对人白血病细胞K562及人肺癌细胞A549肿瘤细胞的体外抑制活性,结果表明,对2种肿瘤细胞的生长均表现出一定的抑制作用.","authors":[{"authorName":"黄丽荣","id":"dab6c25a-0ad0-43fc-a3c0-9081a9edb84c","originalAuthorName":"黄丽荣"},{"authorName":"陈磊","id":"02be7a59-238d-421b-8194-8fa5b3e2a5df","originalAuthorName":"陈磊"},{"authorName":"杨小生","id":"eb03355d-4e7e-43d4-8c8f-881c664ff69b","originalAuthorName":"杨小生"},{"authorName":"马琳","id":"e5630229-c9c8-4eac-b49f-81a24a5e1d7f","originalAuthorName":"马琳"},{"authorName":"张建新","id":"6be150c8-948f-479e-b682-fb4cf4bb48a0","originalAuthorName":"张建新"},{"authorName":"王道平","id":"a4171871-c142-430b-b2d8-188fb2bb57e0","originalAuthorName":"王道平"}],"doi":"10.3724/SP.J.1095.2013.20561","fpage":"1133","id":"1be51063-f0b1-4774-88c5-d2c00d6f7bc6","issue":"10","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"9a63df3a-4b4d-4b50-8c90-6b37e56665af","keyword":"熊果酸","originalKeyword":"熊果酸"},{"id":"0bacad31-2a08-4051-82db-19325cfa96f8","keyword":"2β-羟基熊果酸","originalKeyword":"2β-羟基熊果酸"},{"id":"b9379751-2685-47f1-b3ca-5fb1bca4eeba","keyword":"合成","originalKeyword":"合成"},{"id":"8fe50738-8da6-43ad-82ce-2a43b289c44e","keyword":"体外肿瘤细胞抑制活性","originalKeyword":"体外肿瘤细胞抑制活性"}],"language":"zh","publisherId":"yyhx201310006","title":"2β-羟基熊果酸的合成及其抗肿瘤活性","volume":"30","year":"2013"},{"abstractinfo":"熊耳山地区是华北陆块南缘重要的金多金属成矿带,成矿构造复杂,成矿条件优越,区域内金矿床类型复杂,按容矿建造和定位空间将熊耳山地区的金矿床划分为4种金矿床类型.熊耳山地区金矿床的形成受多重因素的共同控制,主要有地层、构造和岩浆岩因素,且构造控矿因素占主导地位.","authors":[{"authorName":"徐刚","id":"5aae445a-5f4d-4c89-b60f-380c73724eb8","originalAuthorName":"徐刚"},{"authorName":"张有","id":"ac8722a4-0ff1-4943-93f2-811361a713e4","originalAuthorName":"张有"},{"authorName":"方荣","id":"5e6c10e4-0b7a-4694-99d5-6a3602cf6926","originalAuthorName":"方荣"},{"authorName":"左家","id":"ea4ad984-bcd5-414c-aef7-b6145a6c49c1","originalAuthorName":"左家"}],"doi":"10.11792/hj20130207","fpage":"25","id":"4fc4ae64-42de-4dae-bed5-81978a60b3a8","issue":"2","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"e5e0942c-44ae-4b5a-8884-82c17e9f3302","keyword":"金矿床类型","originalKeyword":"金矿床类型"},{"id":"21c58cce-db33-4723-9a63-719f8f71fb00","keyword":"控矿因素","originalKeyword":"控矿因素"},{"id":"3814db1f-e0a4-4497-9a55-60931045f204","keyword":"熊耳山地区","originalKeyword":"熊耳山地区"}],"language":"zh","publisherId":"huangj201302007","title":"河南省熊耳山地区金矿床类型及控矿因素分析","volume":"34","year":"2013"},{"abstractinfo":"建立了美白类化妆品中熊果苷的两种光学异构体α-熊果苷和β-熊果苷及烟酰胺的高效液相色谱检测方法.样品用氯化钠水溶液-氯仿(2∶1, v/v)进行萃取.固定相为依利特ODS-BP柱(200 mm×4.6 mm, 5 μm),流动相为甲醇-水(10∶90, v/v),柱温为25 ℃,检测波长为220 nm,流速为0.5 mL/min,进样量为20 μL.在上述条件下α-熊果苷、β-熊果苷和烟酰胺的质量浓度依次在0.07～50, 0.06～50, 0.05～50 mg/L 时与色谱峰面积之间的线性关系良好,相对标准偏差(n=7)分别为1.65% 、1.73%和1.33% .将该方法用于化妆品的检测,回收率为91.7% ～109.6% .该法简便、快速、准确,可用于化妆品美白成分的测定.","authors":[{"authorName":"程鹏","id":"b9c9a5bc-7e1b-4ed5-b5d1-cacb911c3929","originalAuthorName":"程鹏"},{"authorName":"陈梅兰","id":"74b04805-77aa-4e4b-8fa2-c64483fea866","originalAuthorName":"陈梅兰"},{"authorName":"朱岩","id":"9082e3e6-3efe-4d93-be62-4ca49995bc82","originalAuthorName":"朱岩"}],"doi":"10.3724/SP.J.1123.2010.00089","fpage":"89","id":"5eb0ba43-6634-4f71-bd68-ca152c4d6164","issue":"1","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"f6bfbb92-46ba-4ba2-8ba2-35c4401652ff","keyword":"高效液相色谱","originalKeyword":"高效液相色谱"},{"id":"c136ea75-5061-41f2-b1a2-04cdb300bcef","keyword":"α-熊果苷","originalKeyword":"α-熊果苷"},{"id":"bb39b326-5cea-4dd4-b1ba-b57a5e3392ec","keyword":"β-熊果苷","originalKeyword":"β-熊果苷"},{"id":"c555eeac-d8e7-43e8-beb9-cd21fef9fe69","keyword":"烟酰胺","originalKeyword":"烟酰胺"},{"id":"6f927bd8-f637-44d4-9a02-d32145225d06","keyword":"化妆品","originalKeyword":"化妆品"}],"language":"zh","publisherId":"sp201001015","title":"高效液相色谱法测定化妆品中α-、β-熊果苷及烟酰胺","volume":"28","year":"2010"},{"abstractinfo":"利用黄单胞菌(Xanthomonas) BT-112进行发酵,生物催化合成α-熊果苷. 考察了反应温度、摇床转速和菌体对对苯二酚的最大耐受度、反应物浓度比、反应时间及糖的种类等因素对反应的影响. 结果表明,用本方法合成的产物为单一的α-熊果苷. 在温度35 ℃, 摇床转速180 r/min, 对苯二酚浓度48 mmol/L, 蔗糖与对苯二酚的摩尔比2∶1, 反应48 h的条件下,高达94.3%的对苯二酚转化为α-熊果苷.","authors":[{"authorName":"刘春巧","id":"6ccda5b4-9cbe-4eb0-817c-a45794efb2ab","originalAuthorName":"刘春巧"},{"authorName":"张淑荣","id":"f8f61eb0-4023-44d6-be6b-617868e63471","originalAuthorName":"张淑荣"},{"authorName":"张鹏","id":"b7a4d835-1a81-485d-9237-e1778e1f3ae7","originalAuthorName":"张鹏"}],"doi":"","fpage":"361","id":"96e791f6-4ec2-450e-85ec-770f944fa8b4","issue":"4","journal":{"abbrevTitle":"CHXB","coverImgSrc":"journal/img/cover/CHXB.jpg","id":"18","issnPpub":"0253-9837","publisherId":"CHXB","title":"催化学报 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