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研究在不施加和施加12 T强磁场条件下,于150~400°C下退火1 h后,经热轧和低温等径角挤压(cryoECAP)制备的1050铝合金的硬度和显微组织的演化规律。通过背散射电子衍射(EBSD)和透射电子显微镜(TEM)表征晶粒的显微结构和位错。研究表明:在cryoECAP变形前进行热轧可使cryoECAP制备的1050铝合金产生更多更小尺寸的等轴晶以及更多的大角度晶界(HABs),这些都能在随后的退火过程中促进合金的回复和再结晶且使合金组织变得更加均匀。在150~250°C施加强磁场退火能促进回复和再结晶过程,并且使硬度值明显降低。在300~400°C退火过程中施加磁场能够抑制晶粒的异常长大,促使晶粒尺寸分布更加均匀。

The evolution of hardness and microstructures of 1050 aluminum alloy prepared by hot rolling and subsequent equal- channel angular pressing at cryogenic temperature (cryoECAP) after annealing at 150?400 °C for 1 h without and with magnetic field of 12 T was investigated. The electron back scattering diffraction pattern (EBSD) and transmission electron microscopy (TEM) were utilized to characterize the grain microstructures and dislocations. It is demonstrated that the hot rolling before cryoECAP produces more equiaxed grains with a smaller average size and a higher fraction of high angle boundaries (HABs) in the subsequent cryoECAPed 1050 aluminum alloy, thus accelerating the recovery and recrystallization of cryoECAPed alloy and produces more homogeneous microstructure during annealing. The magnetic field promotes the recovery and recrystallization and leads to much lower hardness at 150?250 °C, while it can suppress the abnormal grain growth and form more homogeneous grain size distributions annealed at 300?400 °C.

参考文献

[1] Vladimir V. Stolyarov;Y. Theodore Zhu;Igor V. Alexandrov;Terry C. Lowe;Ruslan Z. Valiev.Influence of ECAP routes on the microstructure and properties of pure Ti[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,20011/2(1/2):59-67.
[2] 刘满平;蒋婷慧;王俊;刘强;吴振杰;Ying-da YU;Pl C SKARET;Hans J ROVEN.大塑性变形6013铝合金的时效特性与力学性能[J].中国有色金属学报(英文版),2014(12):3858-3865.
[3] M.H.SHAERI;M.SHAERI;M.T.SALEHI;S.H.SEYYEDEIN;F.DJAVANROODI.等径角挤压7075铝合金的显微组织和织构演变[J].中国有色金属学报(英文版),2015(05):1367-1375.
[4] A. Shokuhfar;O. Nejadseyfi.The Influence of Friction on the Processing of Ultrafine-Grained/Nanostructured Materials by Equal-Channel Angular Pressing[J].Journal of Materials Engineering and Performance,20143(3):1038-1048.
[5] K. Oh-Ishi;A. Horita.Communications optimizing the rotation conditions fro grain refinement in equal-channel angular pressing[J].Metallurgical and Materials Transactions, A. Physical Metallurgy and Materials Science,19987(7):2011-2013.
[6] P.VENKATACHALAM;S.RAMESH KUMAR;B.RAVISANKAR;V.THOMAS PAUL;M.VIJAYALAKSHMI.Effect of processing routes on microstructure and mechanical properties of 2014 Al alloy processed by equal channel angular pressing[J].中国有色金属学报(英文版),2010(10):1822-1828.
[7] 钱陈豪;李萍;薛克敏.变形道次对基于等径角挤扭法制备的SiCp/Al复合材料界面的影响[J].中国有色金属学报(英文版),2015(5):1376-1382.
[8] Langdon TG;Komura S;Utsunomiya A;Horita Z;Furukawa M;Nemoto M;Hasegawa H.Thermal stability of ultrafine-grained aluminum in the presence of Mg and Zr additions[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,19991/2(1/2):188-196.
[9] Valiev RZ.;Alexandrov IV.;Islamgaliev RK..Bulk nanostructured materials from severe plastic deformation [Review][J].Progress in materials science,20002(2):103-189.
[10] J.K. Kim;H.G. Jeong;S.I. Hong.Effect of aging treatment of heavily deformed microstructure of a 6061 aluminum alloy after equal channel angular pressing[J].Scripta materialia,20018(8):901-907.
[11] S. Ferrasse;V.M. Segal;F. Alford.Texture evolution during equal channel angular extrusion (ECAE) Part II. An effect of post-deformation annealing[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,20041/2(1/2):235-244.
[12] K. Harada;S. Tsurekawa;T. Watanabe;G. Palumbo.Enhancement of homogeneity of grain boundary microstructure by magnetic annealing of electrodeposited nanocrystalline nickel[J].Scripta materialia,20035(5):367-372.
[13] Tsurekawa S;Okamoto K;Kawahara K;Watanabe T.The control of grain boundary segregation and segregation-induced brittleness in iron by the application of a magnetic field[J].Journal of Materials Science,20054(4):895-901.
[14] L.Z. He;Y.H. Cao;X.T. Liu.Influences of magnetic annealing on the grain growth in a cryoECAPed 1050 aluminum alloy[J].Materials Characterization,2013:188-195.
[15] R B Morgunov.Spin micromechanics in the physics of plasticity[J].Physics - Uspekhi,20042(2):125-147.
[16] V. I. Alshits;E. V. Darinskaya;M. V. Koldaeva;E. A. Petrzhik.Magnetoplastic Effect: Basic Properties and Physical Mechanisms[J].Crystallography reports,20035(5):768-795.
[17] D. A. Molodov;G. Gottstein;F. Heringhaus;L. S. Shvindlerman.Motion of planar grain boundaries in bismuthbicrystals driven by a magnetic field[J].Scripta materialia,19978(8):1207-1213.
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