综述了近年来电感耦合等离子体质谱(ICP-MS)技术的发展趋势,重点对其关键部件离子透镜系统、碰撞/反应池、质量分析器及检测器的现状及研究进展进行了评述.归纳了ICP-MS及激光剥蚀电感耦合等离子体质谱(LA-ICP-MS)技术在冶金分析中的应用,阐述了其中的干扰问题及消除与校正方法,并介绍了冶金分析中定量分析方法.
参考文献
| [1] | E. Hywel Evans;Matthew Horstwood;Jorge Pisonero.Atomic spectrometry update: review of advances in atomic spectrometry and related techniques[J].Journal of Analytical Atomic Spectrometry,20136(6):779-800. |
| [2] | Simon Carter;Andy S. Fisher;Michael W. Hinds.Atomic spectrometry update. Review of advances in the analysis of metals, chemicals and materials[J].Journal of Analytical Atomic Spectrometry,201312(12):1814-1869. |
| [3] | E. Hywel Evans;Jorge Pisonero;Clare M. M. Smith.Atomic spectrometry updates: Review of advances in atomic spectrometry and related techniques[J].Journal of Analytical Atomic Spectrometry,20145(5):773-794. |
| [4] | Butler, Owen T.;Cairns, Warren R. L.;Cook, Jennifer M.;Davidson, Christine M..2014 atomic spectrometry update - a review of advances in environmental analysis[J].Journal of Analytical Atomic Spectrometry,20151(1):21-63. |
| [5] | 余兴.电感耦合等离子体四极杆质谱离子光学系统的现状与进展[J].冶金分析,2011(01):23-29. |
| [6] | 余兴.电感耦合等离子体四极杆质谱碰撞/反应池技术现状与进展[J].冶金分析,2013(03):14-23. |
| [7] | Wei Guo;Shenghong Hu;Yufang Xiao;Hongfei Zhang;Xianjun Xie.Direct determination of trace cadmium in environmental samples by dynamic reaction cell inductively coupled plasma mass spectrometry[J].Chemosphere: Environmental toxicology and risk assessment,201011(11):1463-1468. |
| [8] | Guo, W.;Hu, S.;Zhao, J.;Jin, S.;Liu, W.;Zhang, H..Removal of spectral interferences and accuracy monitoring of trace cadmium in feeds by dynamic reaction cell inductively coupled plasma mass spectrometry[J].Microchemical Journal: Devoted to the Application of Microtechniques in all Branches of Science,20112(2):154-159. |
| [9] | Guo, W.;Hu, S.;Wang, Y.;Zhang, L.;Hu, Z.;Zhang, J..Trace determination of selenium in biological samples by CH_4-Ar mixed gas plasma DRC-ICP-MS[J].Microchemical Journal: Devoted to the Application of Microtechniques in all Branches of Science,2013:106-112. |
| [10] | Yi Hua Wei;Jin Yan Zhang;Da Wen Zhang;Lin Guang Luo;Tian Hua Tu.Simultaneous determination of Se, trace elements and major elements in Se-rich rice by dynamic reaction cell inductively coupled plasma mass spectrometry (DRC-ICP-MS) after microwave digestion[J].Food Chemistry,2014Sep.15(Sep.15):507-511. |
| [11] | Petrucci, Francesco;Senofonte, Oreste.Determination of Cr(VI) in cosmetic products using ion chromatography with dynamic reaction cellinductively coupled plasma-mass spectrometry (DRC-ICP-MS)[J].Analytical methods,201512(12):5269-5274. |
| [12] | Catalani, Simona;Fostinelli, Jacopo;Gilberti, Maria Enrica;Apostoli, Pietro.Application of a metal free high performance liquid chromatography with inductively coupled plasma mass spectrometry (HPLC-ICP-MS) for the determination of chromium species in drinking and tap water[J].International journal of mass spectrometry,2015:31-37. |
| [13] | C. Derrick Quarles Jr;Deanna R. Jones;Jeffery M. Jarrett.Analytical method for total chromium and nickel in urine using an inductively coupled plasma-universal cell technology-mass spectrometer (ICP-UCT-MS) in kinetic energy discrimination (KED) mode[J].Journal of Analytical Atomic Spectrometry,20142(2):297-303. |
| [14] | Pellet, Bastien;Ayrault, Sophie;Tusseau-Vuillemin, Marie-Helene;Gourlay-France, Catherine.Quantifying diet-borne metal uptake in Gammarus pulex using stable isotope tracers[J].Ecotoxicology and Environmental Safety,2014Dec.(Dec.):182-189. |
| [15] | Xiao Li;Shifeng Dai;Weiguo Zhang.Determination of As and Se in coal and coal combustion products using closed vessel microwave digestion and collision/reaction cell technology (CCT) of inductively coupled plasma mass spectrometry (ICP-MS)[J].International Journal of Coal Geology,2014:1-4. |
| [16] | Larissa Leffers;Christoph A. Wehe;Sabine Huwel;Marc Bartel;Franziska Ebert;Mojtaba S. Taleshi;Hans-Joachim Galla;Uwe Karst;Kevin A. Francesconi;Tanja Schwerdtle.In vitro intestinal bioavailability of arsenosugar metabolites and presystemic metabolism of thio-dimethylarsinic acid in Caco-2 cells[J].Metallomics. integrated biometal science,20138(8):1031-1042. |
| [17] | Wehe,C.A.;Beyer,G.;Sperling,M.;Ciarimboli,G.;Karst,U..Assessing the intracellular concentration of platinum in medulloblastoma cell lines after Cisplatin incubation[J].Journal of trace elements in medicine and biology: Organ of the Society for Minerals and Trace Elements (GMS),20142(2):166-172. |
| [18] | Brinkhaus, Sigrid Grosse;Bornhorst, Julia;Chakraborty, Sudipta;Wehe, Christoph A.;Niehaus, Rebecca;Reifschneider, Olga;Aschner, Michael;Karst, Uwe.Elemental bioimaging of manganese uptake in C-elegans[J].Metallomics. integrated biometal science,20143(3):617-621. |
| [19] | Wehe, Christoph A.;Thyssen, Georgina M.;Herdering, Christina;Raj, Indra;Ciarimboli, Giuliano;Sperling, Michael;Karst, Uwe.Elemental Bioimaging by Means of Fast Scanning Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry[J].Journal of the American Society for Mass Spectrometry,20158(8):1274-1282. |
| [20] | Mirian C.Santos;Joaquim A.Nobrega;Solange Cadore.Determination of Cd, Cr, Hg and Pb in plastics from waste electrical and electronic equipment by inductively coupled plasma mass spectrometry with collision-reaction interface technology[J].Journal of hazardous materials,20111/3(1/3):833-839. |
| [21] | Lucimar L Fialho;Catarinie D. Pereira;Joaquim A. Nobrega.Combination of cool plasma and collision-reaction interface for correction of polyatomic interferences on copper signals in inductively coupled plasma quadrupole mass spectrometry[J].Spectrochimica Acta, Part B. Atomic Spectroscopy,20115(5):389-393. |
| [22] | Silvia Diez Fernandez;Naoki Sugishama;Jorge Ruiz Encinar;Alfredo Sanz-Medel.Triple Quad ICPMS (ICPQQQ) as a New Tool for Absolute Quantitative Proteomics and Phosphoproteomics[J].Analytical chemistry,201214(14):5851-5857. |
| [23] | Lieve Balcaen;Glenn Woods;Martin Resano.Accurate determination of S in organic matrices using isotope dilution ICP-MS/MS[J].Journal of Analytical Atomic Spectrometry,20131(1):33-39. |
| [24] | Yasumi Anan;Yoshiko Hatakeyama;Maki Tokumoto.Chromatographic Behavior of Selenoproteins in Rat Serum Detected by Inductively Coupled Plasma Mass Spectrometry[J].Analytical Sciences: The International Journal of The Japan Society for Analytical Chemistry,20138(8):787-792. |
| [25] | Takeshi Ohno;Yasuyuki Muramatsu;Yasuyuki Shikamori.Determination of uItratrace ~(129)l in soil samples by Triple Quadrupole ICP-MS and its application to Fukushima soil samples[J].Journal of Analytical Atomic Spectrometry,20138(8):1283-1287. |
| [26] | Masaharu Tanimizu;Naoki Sugiyama;Emmanuel Ponzevera.Determination of ultra-low ~(236)U/~(238)U isotope ratios by tandem quadrupole ICP-MS/MS[J].Journal of Analytical Atomic Spectrometry,20139(9):1372-1376. |
| [27] | Katharina Boting;Simon Treu;Peter Leonhard.First experimental proof of asymmetric charge transfer in ICP-MS/MS (ICP-QQQ-MS) through isotopically enriched oxygen as cell gas[J].Journal of Analytical Atomic Spectrometry,20143(3):578-582. |
| [28] | Asta H. Petursdottir;Nils Friedrich;Stanislav Musil.Hydride generation ICP-MS as a simple method for determination of inorganic arsenic in rice for routine biomonitoring[J].Analytical methods,201414(14):5392-5396. |
| [29] | Amaral, Clarice D. B.;Amais, Renata S.;Fialho, Lucimar L.;Schiavo, Daniela;Nogueira, Ana Rita A.;Nobrega, Joaquim A..Determination of carbon in digested samples and amino acids by inductively coupled plasma tandem mass spectrometry[J].Microchemical Journal: Devoted to the Application of Microtechniques in all Branches of Science,2015:29-32. |
| [30] | Amais, Renata S.;Virgilio, Alex;Schiavo, Daniela;Nobrega, Joaquim A..Tandem mass spectrometry (ICP-MS/MS) for overcoming molybdenum oxide interferences on Cd determination in milk[J].Microchemical Journal: Devoted to the Application of Microtechniques in all Branches of Science,2015:64-68. |
| [31] | Amaral, Clarice D. B.;Amais, Renata S.;Fialho, Lucimar L.;Schiavo, Daniela;Amorim, Tatiane;Nogueira, Ana Rita A.;Rocha, Fabio R. P.;Nobrega, Joaquim A..A novel strategy to determine As, Cr, Hg and V in drinking water by ICP-MS/MS[J].Analytical methods,20153(3):1215-1220. |
| [32] | Bishop, David P.;Hare, Dominic J.;Fryer, Fred;Taudte, Regina V.;Cardoso, Barbara R.;Cole, Nerida;Doble, Philip A..Determination of selenium in serum in the presence of gadolinium with ICP-QQQ-MS[J].The Analyst: The Analytical Journal of the Royal Society of Chemistry: A Monthly International Publication Dealing with All Branches of Analytical Chemistry,20158(8):2842-2846. |
| [33] | Bolea-Fernandez, Eduardo;Balcaen, Lieve;Resano, Martin;Vanhaecke, Frank.Interference-free determination of ultra-trace concentrations of arsenic and selenium using methyl fluoride as a reaction gas in ICP-MS/MS[J].Analytical and bioanalytical chemistry,20153(3):919-929. |
| [34] | Jackson, Brian P.;Liba, Amir;Nelson, Jenny.Advantages of reaction cell ICP-MS on doubly charged interferences for arsenic and selenium analysis in foods[J].Journal of Analytical Atomic Spectrometry,20155(5):1179-1183. |
| [35] | Lieve Balcaen;Eduardo Bolea-Fernandez;Martin Resano.Accurate determination of ultra-trace levels of Ti in blood serum using ICP-MS/MS[J].Analytica chimica acta,2014:1-8. |
| [36] | Nelson, Jenny;Hopfer, Helene;Silva, Fabio;Wilbur, Steve;Chen, Jianmin;Ozawa, Kumi Shiota;Wylie, Philip L..Evaluation of GC-ICP-MS/MS as a New Strategy for Specific Heteroatom Detection of Phosphorus, Sulfur, and Chlorine Determination in Foods[J].Journal of Agricultural and Food Chemistry,201518(18):4478-4483. |
| [37] | Takeshi Ohno;Yasuyuki Muramatsu.Determination of radioactive cesium isotope ratios by triple quadrupole ICP-MS and its application to rainwater following the Fukushima Daiichi Nuclear Power Plant accident[J].Journal of Analytical Atomic Spectrometry,20142(2):347-351. |
| [38] | Diez Fernandez, Silvia;Ruiz Encinar, Jorge;Sanz-Medel, Alfredo;Isensee, Kirsten;Stoll, Heather M..Determination of low B/Ca ratios in carbonates using ICP-QQQ[J].Geochemistry, geophysics, geosystems,20156(6):2005-2014. |
| [39] | Gong, Jiawei;Solivio, Morwena J.;Merino, Edward J.;Caruso, Joseph A.;Landero-Figueroa, Julio A..Developing ICP-MS/MS for the detection and determination of synthetic DNA-protein crosslink models via phosphorus and sulfur detection[J].Analytical and bioanalytical chemistry,20159(9):2433-2437. |
| [40] | Aureli, Federica;D'Amato, Marilena;Raggi, Andrea;Cubadda, Francesco.Quantitative characterization of silica nanoparticles by asymmetric flow field flow fractionation coupled with online multiangle light scattering and ICP-MS/MS detection[J].Journal of Analytical Atomic Spectrometry,20156(6):1266-1273. |
| [41] | Jhanis J. Gonzalez;Dayana D. Oropeza;Henry Longerich.Rapid bulk analysis using femtosecond laser ablation inductively coupled plasma time-of-flight mass spectrometry[J].Journal of Analytical Atomic Spectrometry,20129(9):1405-1412. |
| [42] | Erin Ehrlinger;Alyssa Poplaski;Ellen M. Hondrogiannis.Use of Laser Ablation-lnductively Coupled Plasma-Time of Flight-Mass Spectrometry To Identify the Elemental Composition of Vanilla and Determine the Geographic Origin by Discriminant Function Analysis[J].Journal of Agricultural and Food Chemistry,201347(47):11332-11337. |
| [43] | S. Mark Monk;Steven M. Lev.Toxicological applications of cryogenic laser ablation inductively coupled plasma time of flight mass spectrometry (CLA-ICP-TOF-MS)[J].Journal of Analytical Atomic Spectrometry,20132(2):274-279. |
| [44] | K. Jurowski;M. Szewczyk;W. Piekoszewski.A standard sample preparation and calibration procedure for imaging zinc and magnesium in rats' brain tissue by laser ablation-inductively coupled plasma-time of flight-mass spectrometry[J].Journal of Analytical Atomic Spectrometry,20148(8):1425-1431. |
| [45] | Jurowski, Kamil;Buszewski, Boguslaw;Piekoszewski, Wojciech.Bioanalytics in Quantitive (Bio)imaging/Mapping of Metallic Elements in Biological Samples[J].Critical reviews in analytical chemistry,20154(4):334-347. |
| [46] | Alexander Gundlach-Graham;Elise A. Dennis;Steven J. Ray.First inductively coupled plasma-distance-of-flight mass spectrometer: instrument performance with a microchannel plate/phosphor imaging detector[J].Journal of Analytical Atomic Spectrometry,20139(9):1385-1395. |
| [47] | Engelhard, C..Inductively coupled plasma mass spectrometry: Recent trends and developments[J].Analytical and bioanalytical chemistry,20111(1):213-219. |
| [48] | A. K. Knight;R. P. Sperline;G. M. Hieftje;E. Young;C. J. Barinaga;D. W. Koppenaal;M. B. Denton.The development of a micro-Faraday array for ion detection[J].International journal of mass spectrometry,20021/3(1/3):131-139. |
| [49] | James H. Barnes;Gregory D. Schilling;Roger Sperline;M. Bonner Denton;Erick T. Young;Charles J. Barinaga;David W. Koppenaal;Gary M. Hieftje.Characterization of a Focal Plane Camera Fitted to a Mattauch-Herzog Geometry Mass Spectrograph. 2. Use with an Inductively Coupled Plasma[J].Analytical chemistry,20049(9):2531-2536. |
| [50] | Gregory D. Schilling;Francisco J. Andrade;James H. Barnes;Roger P. Sperline;M. Bonner Denton;Charles J. Barinaga;David W. Koppenaal;Gary M. Hieftje.Characterization of a Second-Generation Focal-Plane Camera Coupled to an Inductively Coupled Plasma Mattauch-Herzog Geometry Mass Spectrograph[J].Analytical chemistry,200613(13):4319-4325. |
| [51] | Gregory D. Schilling;Steven J. Ray;Roger P. Sperline.Optimization of Ag isotope-ratio precision with a 128-Channel array detector coupled to a Mattauch-Herzog mass spectrograph[J].Journal of Analytical Atomic Spectrometry,20103(3):322-327. |
| [52] | Gregory D. Schilling;Steven J. Ray;Arnon A. Rubinshtein;Jeremy A. Felton;Roger P. Sperline;M. Bonner Denton;Charles J. Barinaga;David W. Koppenaal;Gary M. Hieftje.Evaluation of a 512-Channel Faraday-Strip Array Detector Coupled to an Inductively Coupled Plasma Mattauch-Herzog Mass Spectrograph[J].Analytical chemistry,200913(13):5467-5473. |
| [53] | Arnon A. Rubinshtein;Gregory D. Schilling;Steven J. Ray.Characterization of a third-generation Faraday-strip array detector coupled to a Mattauch-Herzog geometry mass spectrograph with a dc-glow discharge ionization source[J].Journal of Analytical Atomic Spectrometry,20105(5):735-738. |
| [54] | Jeremy A. Eelton;Gregory D. Schilling;Steven J. Ray.Evaluation of a fourth-generation focal plane camera for use in plasma-source mass spectrometry[J].Journal of Analytical Atomic Spectrometry,20112(2):300-304. |
| [55] | Dirk Ardelt;Aleksandra Polatajko;Oliver Primm;Maurice Reijnen.Isotope ratio measurements with a fully simultaneous Mattauch–Herzog ICP-MS[J].Analytical and bioanalytical chemistry,20139(9):2987-2994. |
| [56] | Hao A. O. Wang;Daniel Grolimund;Charlotte Giesen;Camelia N. Borca;James R. H. Shaw-Stewart;Bernd Bodenmiller;Detlef Gunther.Fast Chemical Imaging at High Spatial Resolution by Laser Ablation Inductively Coupled Plasma Mass Spectrometry[J].Analytical chemistry,201321(21):10107-10116. |
| [57] | Richard F. J. Dams;Jan Goossens;Luc Moens.Spectral and Non-Spectral Interferences in Inductively Coupled Plasma Mass-Spectrometry[J].Mikrochimica Acta: An International Journal for Physical and Chemical Methods of Analysis,19953/4(3/4):277-286. |
| [58] | Sally M. McIntyre;Jill Wisnewski Ferguson;Travis M. Witte, R.S. Houk.Measurement of gas kinetic temperatures for polyatomic ions in inductively coupled plasma-mass spectrometry: Validation and refinements[J].Spectrochimica Acta, Part B. Atomic Spectroscopy,20113/4(3/4):248-254. |
| [59] | Maryam Aghaei;Luca Flamigni;Helmut Lindner.Occurrence of gas flow rotational motion inside the ICP torch: a computational and experimental study[J].Journal of Analytical Atomic Spectrometry,20142(2):249-261. |
| [60] | Olga Borovinskaya;Maryam Aghaei;Luca Flamigni.Diffusion-and velocity-driven spatial separation of analytes from single droplets entering an ICP off-axis[J].Journal of Analytical Atomic Spectrometry,20142(2):262-271. |
| [61] | 金献忠;谢健梅;张建波;林力;应海松;陈建国.氩气氛围电感耦合等离子体质谱分析性能的初步研究和应用[J].冶金分析,2014(10):7-13. |
| [62] | 聂西度;李立波;谢华林.电感耦合等离子体质谱法测定电解金属锰中痕量元素[J].冶金分析,2011(9):42-46. |
| [63] | 金献忠;陈建国;张建波.冷等离子体激光剥蚀电感耦合等离子体质谱法测定钢铁中14种元素[J].冶金分析,2014(1):10-16. |
| [64] | Quemet, A.;Brennetot, R.;Chevalier, E.;Prian, E.;Laridon, A.-L.;Mariet, C.;Fichet, P.;Laszak, I.;Goutelard, F..Analysis of twenty five impurities in uranium matrix by ICP-MS with iron measurement optimized by using reaction collision cell, cold plasma or medium resolution[J].Talanta: The International Journal of Pure and Applied Analytical Chemistry,2012:207-212. |
| [65] | 韩建华;孙传强;汪曣;赵学玒;蔡彪.电感耦合等离子体质谱中碰撞反应池的模拟探讨[J].冶金分析,2014(9):1-7. |
| [66] | 于媛君;亢德华;王铁.动态反应池-电感耦合等离子体质谱法测定钢铁及合金中硫[J].冶金分析,2011(12):6-10. |
| [67] | 李继东;王长华;郑永章.动态反应池-电感耦合等离子体质谱法测定高纯锑中23种痕量杂质元素[J].冶金分析,2011(12):21-25. |
| [68] | 陈永欣;黎香荣;韦新红;韩清娟;崔翔;何龙凉.碰撞反应界面-电感耦合等离子体质谱法测定磷酸中15种痕量杂质元素[J].冶金分析,2012(12):15-21. |
| [69] | 王征;赵学玒;孙传强;汪曣.电感耦合等离子体质谱法测定痕量铁元素时碰撞反应池条件的探讨[J].冶金分析,2015(6):1-7. |
| [70] | 胡净宇;王海舟.电感耦合等离子体质谱法测定高温合金中痕量镉和碲[J].冶金分析,2010(2):8-12. |
| [71] | NIE Xi-du;LIANG Yi-zeng;TANG You-gen;XIE Hua-lin.Determination of trace elements in high purity nickel by high resolution inductively coupled plasma mass spectrometry[J].中南大学学报（英文版）,2012(09):2416-2420. |
| [72] | Tom Tindemans;Andrew Dobney;Dorine Wambeke.Development and application of an analyte/matrix separation procedure for multi-element trace analysis of steel alloys by means of sector-field ICP-mass spectrometry[J].Journal of Analytical Atomic Spectrometry,20146(6):1073-1081. |
| [73] | 马海斌;孙自杰.电感耦合等离子体质谱仪中氩原子和钙离子的动力学温度及终端移动速率测量[J].冶金分析,2015(8):7-11. |
| [74] | 成勇;黄木辉.电感耦合等离子体质谱法测定钢铁中15种痕量元素[J].冶金分析,2011(5):31-35. |
| [75] | Valbona Celo;Ewa Dabek-Zlotorzynska;Jiujiang Zhao.An improved method for determination of lanthanoids in environmental samples by inductively coupled plasma mass spectrometry with high matrix introduction system[J].Analytica chimica acta,20111(1):89-96. |
| [76] | Yanbei Zhu;Kazumi Inagaki;Hiroki Haraguchi.On-line elution of iron hydroxide coprecipitate carrier for determination of REEs in natural water by mix-gas ICP-MS[J].Journal of Analytical Atomic Spectrometry,20103(3):364-369. |
| [77] | Duan, Xiaoxia;Regelous, Marcel.Rapid determination of 26 elements in iron meteorites using matrix removal and membrane desolvating quadrupole ICP-MS[J].Journal of Analytical Atomic Spectrometry,201412(12):2379-2387. |
| [78] | 亢德华;于媛君;王铁.电感耦合等离子体质谱法测定钢中痕量钙[J].冶金分析,2010(10):6-10. |
| [79] | Okano, Gen;Igarashi, Shukuro;Ohno, Osamu;Yamamoto, Yuhei;Saito, Shotaro;Oka, Yoshio.Determination of Trace Amounts of Bismuth in Steel by ICP-MS Through a Cascade-preconcentration and Separation Method[J].ISIJ International,20151(1):332-334. |
| [80] | 李杰;李洁;张穗忠.电感耦合等离子体质谱法测定硅钢中痕量铜和镍[J].冶金分析,2011(5):16-19. |
| [81] | 张立锋;张翼明;周凯红.电感耦合等离子体质谱法测定钕铁硼中铝、钴、铜、镓、锆、铽、钛、铌[J].冶金分析,2011(3):50-54. |
| [82] | 张立锋;张秀艳;张翼明;李立刚.电感耦合等离子体质谱法测定镧镁合金中稀土杂质[J].冶金分析,2014(6):33-37. |
| [83] | 韩美;杨国武;齐荣;胡净宇.电感耦合等离子体质谱法测定镍钨合金中铈[J].冶金分析,2015(11):34-37. |
| [84] | 李杰;李洁;张穗忠;于录军.电感耦合等离子体质谱法测定硅钢中痕量铝钼钒钛铌[J].冶金分析,2013(1):22-26. |
| [85] | 王铁;亢德华;于媛君.电感耦合等离子体质谱法测定锰铁中痕量铅锡锑[J].冶金分析,2013(5):13-16. |
| [86] | 亢德华;于媛君;王铁;杨丽荣;顾继红.电感耦合等离子体质谱法测定铸铁中镁、锡、镧、铈、锑和铅[J].冶金分析,2011(6):54-57. |
| [87] | 刘宏伟;谢华林.电感耦合等离子体质谱法测定锂离子电池正极材料钴酸锂中20种杂质元素[J].冶金分析,2013(7):30-34. |
| [88] | 亢德华;王铁;于媛君;杨丽荣;顾继红.电感耦合等离子体质谱法测定生铁中痕量元素[J].冶金分析,2014(8):27-31. |
| [89] | 钟胜贤;卢现友;刘景麟;周志.电感耦合等离子体质谱法测定磷酸铁锂中杂质元素[J].冶金分析,2015(3):19-24. |
| [90] | 亢德华;王铁;于媛君;王翠艳;白轩.电感耦合等离子体质谱法测定硅铁中杂质元素[J].冶金分析,2013(10):64-68. |
| [91] | Kagawa, T;Ohno, M;Seki, T;Chikama, K.Online determination of copper in aluminum alloy by microchip solvent extraction using isotope dilution ICP-MS method[J].Talanta: The International Journal of Pure and Applied Analytical Chemistry,20094(4):1001-1005. |
| [92] | 聂玲清;纪红玲;陈英颖.激光烧蚀进样电感耦合等离子体质谱法在冶金分析中的应用进展[J].冶金分析,2007(5):30-36. |
| [93] | 胡净宇;王海舟.激光剥蚀-电感耦合等离子体质谱内标定量法测定高温合金中痕量元素[J].冶金分析,2008(1):1-5. |
| [94] | 胡净宇;王海舟.激光剥蚀-电感耦合等离子体质谱对高温合金中17种痕量元素的测定[J].分析测试学报,2010(4):359-363. |
| [95] | 韩美;胡净宇;陈玉红;王海舟.集合式屑状标准物质校正-激光烧蚀电感耦合等离子体质谱法分析镍基高温合金中痕量元素[J].冶金分析,2010(3):1-6. |
| [96] | 罗倩华;陈玉红;王海舟.激光剥蚀-电感耦合等离子体质谱法测定不锈钢中17种元素[J].冶金分析,2013(9):1-7. |
| [97] | Jingyu HU;Mei HAN;Liangjing YUAN.Original Position Statistic Distribution Analysis of Trace Element Segregation in Nickel-base Super Alloy by LA-ICP-MS[J].ISIJ International,201211(11):2055-2058. |
| [98] | 金献忠;陈建国;谢健梅.激光剥蚀电感耦合等离子体质谱法测定镀锌钢板镀层中的铅镉砷锡锑[J].冶金分析,2012(3):1-6. |
| [99] | 袁良经;于雷;韩美;王海舟.中低合金钢冲击断口表面的激光剥蚀电感耦合等离子体质谱原位统计分布分析[J].冶金分析,2010(6):1-6. |
| [100] | 韩美;胡净宇;王明海;王海舟.激光烧蚀-电感耦合等离子体质谱法应用于低合金钢焊缝中元素分布分析[J].冶金分析,2011(8):1-5. |
| [101] | 胡净宇;王海舟.高温合金痕量分析中激光剥蚀电感耦合等离子体质谱的分馏效应机理研究[J].分析测试学报,2009(3):277-282. |
| [102] | 王明海;韩美;罗倩华;杨国武.激光烧蚀-电感耦合等离子体质谱法测定高温合金中痕量元素的分馏效应及其校正[J].冶金分析,2014(7):1-6. |
| [103] | 陈玉红;王海舟.激光剥蚀-电感耦合等离子体质谱法分析小尺寸钢铁及合金的样品制备与定量方法研究[J].冶金分析,2009(2):1-7. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%