为了研究ZrO2增强羟基磷灰石(HA)复合涂层在牛血清润滑环境下的摩擦磨损性能,首先,采用等离子喷涂技术在钛合金基体上制备了ZrO2含量分别为0、15wt%和30wt%的HA生物陶瓷涂层;然后,分析了ZrO2/HA复合涂层的物相成分和结合强度;最后,采用UMT-3销盘摩擦试验机研究了ZrO2/HA复合涂层在牛血清润滑环境下的摩擦磨损性能,观察涂层磨损表面微观形貌并分析了磨损机制.结果表明:HA涂层的主要物相为HA,15wt% ZrO2/HA复合涂层和30wt%ZrO2/HA复合涂层中的ZrO2以立方相形式存在,并且衍射峰强度高于HA的.随着ZrO2含量增大,涂层的结合强度明显增大.ZrO2/HA复合涂层与纯HA涂层相比,有更好的耐磨性和更低的摩擦系数.纯HA涂层的磨损机制以犁沟效应和磨粒磨损为主,而15wt% ZrO2/HA复合涂层和30wt% ZrO2/HA复合涂层的磨损机制为脆性剥落磨损.
参考文献
[1] | 周宏明;曾麟;易丹青;李荐;贾晓慧;郭雁军.电泳沉积制备BG/BG-FHA复合涂层[J].复合材料学报,2011(6):194-199. |
[2] | 郑学斌;谢有桃.热喷涂生物陶瓷涂层的研究进展[J].无机材料学报,2013(1):12-20. |
[3] | 黄紫洋;李鹏;刘榕芳;肖秀峰.钛涂覆多孔羟基磷灰石涂层的制备及其生物活性[J].复合材料学报,2010(5):68-72. |
[4] | M. Khalid;M. Mujahid;A. Nusair Khan.Effect of arc current on microstructure, texturing and wear behavior of plasma sprayed CaZrO_3 coatings[J].CERAMICS INTERNATIONAL,20133(3):2293-2302. |
[5] | Webster TJ.;Doremus RH.;Siegel RW.;Bizios R.;Ergun C..Enhanced functions of osteoblasts on nanophase ceramics[J].Biomaterials,200017(17):1803-1810. |
[6] | M. C. Kuo;S. K. Yen.The process of electrochemical deposited hydroxyapatite coatings on biomedical titanium at room temperature[J].Materials science & engineering, C. Biomimetic and supramolecular systems,20021/2(1/2):153-160. |
[7] | 纪美茹;傅小奇;张雷;王国伟;赵谦;姜廷顺.碳纳米管/羟基磷灰石复合材料的制备及表征[J].复合材料学报,2012(3):85-89. |
[8] | Dejiu, S.;Jingrui, C.;Guolong, L.;Donglei, H.;Lailei, W.;Haojie, M.;Yonghong, X.;He, C.;Yaqian, Y..Effect of ultrasonic on microstructure and growth characteristics of micro-arc oxidation ceramic coatings on 6061 aluminum alloy[J].Vacuum: Technology Applications & Ion Physics: The International Journal & Abstracting Service for Vacuum Science & Technology,2014:143-148. |
[9] | Rui Luo;Zhongde Liu;Feixiang Yan;Yang Kong;Yingtao Zhang.The biocompatibility of hydroxyapatite film deposition on micro-arc oxidation Ti6A14V alloy[J].Applied Surface Science: A Journal Devoted to the Properties of Interfaces in Relation to the Synthesis and Behaviour of Materials,2013Feb.1(Feb.1):57-61. |
[10] | S Yugeswaran;C P Yoganand;A Kobayashi;K M Paraskevopoulos;B Subramanian.Mechanical properties, electrochemical corrosion and in-vitro bioactivity of yttria stabilized zirconia reinforced hydroxyapatite coatings prepared by gas tunnel type plasma spraying.[J].Journal of the mechanical behavior of biomedical materials,2012:22-33. |
[11] | 袁明;陈萍华;蒋华麟;舒红英;谢伟杰;何伟;邹芳;林艺.氧化锆陶瓷增韧方法的研究进展[J].江西化工,2013(1):1-4. |
[12] | Cizek J;Khor KA;Prochazka Z.Influence of spraying conditions on thermal and velocity properties of plasma sprayed hydroxyapatite[J].Materials science & engineering, C. Biomimetic and supramolecular systems,20072(2):340-344. |
[13] | M. F. Morks;Akira Kobayashi;N. F. Fahim.Abrasive wear behavior of sprayed hydroxyapatite coatings by gas tunnel type plasma spraying[J].Wear: an International Journal on the Science and Technology of Friction, Lubrication and Wear,20071/2(1/2):204-209. |
[14] | Singh, G.;Singh, S.;Prakash, S..Surface characterization of plasma sprayed pure and reinforced hydroxyapatite coating on Ti6Al4V alloy[J].Surface & Coatings Technology,201120(20):4814-4820. |
[15] | 翟倩倩;赵士贵;王孝海;李秀芝;李文杰;郑亚森.仿生纳米含硅羟基磷灰石的合成与表征[J].无机材料学报,2013(1):58-62. |
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