欢迎登录材料期刊网

材料期刊网

高级检索

探讨了 SiC引入方式对反应熔渗原位20wt%纳米 SiC/MoSi2复合材料 TEM组织及力学性能的影响。结果表明:完全原位反应熔渗硅可获得基体相和增强相均为纳米尺度的 SiC/MoSi2复合材料,其组织中存在大量晶内层错等缺陷,可能会使纳米 SiC/MoSi2复合材料力学性能的提高不十分显著;而部分原位反应熔渗法中,SiC初始粉末的引入可缓解剧烈物相反应,所得纳米 SiC/MoSi2复合材料晶内缺陷消失,断口出现大量撕裂棱,复合材料力学性能大幅提高。

The effects of introduction methods of SiC on TEM structure and mechanical properties of 20wt% nano SiC/MoSi2 composites prepared by reactive melt infiltration were studied.The results show that,the nanometer scale of matrix phase and reinforced phase of SiC/MoSi2 composites can be obtained in the process of complete in-situ reactive infiltration silicon,but maybe due to the large number of fault defects inner crystals of the structure,the mechanical properties of the nano SiC/MoSi2 composites improve not too much;when preparing the composites in partial in-situ reactive melt infiltration method to relieve the severe phase reaction,the defects inner crystal in nano SiC/MoSi2 composites disappear,and there are a large number of tear ridges in the fracture,also,the mechanical properties of composites increase obviously due to the introduction of SiC initial powder.

参考文献

[1] Esmaeily, Soheila;Kermani, Milad;Razavi, Mansour;Rahimipour, Mohammad Reza;Zakeri, Mohammad.An investigation on the in situ synthesis-sintering and mechanical properties of MoSi2-xSiC composites prepared by spark plasma sintering[J].International Journal of Refractory Metals & Hard Materials,2015:263-271.
[2] Milad Kermani;Mansour Razavi;Mohammad Reza Rahimipour.The effect of temperature on the in situ synthesis-sintering and mechanical properties of MoSi_2 prepared by spark plasma sintering[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,2014:229-233.
[3] Dan Zhu, Mingxia Gao;Hongge Pan;Zhanglian Hong.Fabrication and mechanical properties of SiC_w/MoSi_2-SiC composites by liquid Siinfiltration of pyrolyzed rice husk preforms with Mo additions[J].International Journal of Refractory Metals & Hard Materials,2012Nov(Nov):152-158.
[4] Beata Ballokova;Michal Besterci;Pavol Hvizdos.High Temperature Properties of the MoSi_2 and MoSi_2-SiC Nonocomposites[J].HIGH TEMPERATURE MATERIALS AND PROCESSES,20095(5):271-276.
[5] C. Suryanarayana.Structure and properties of ultrafine-grained MoSi2 +Si3N4 composites synthesized by mechanical alloying[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,20081/2(1/2):23-30.
[6] Qiaodan Hu;Peng Luo;Youwei Yan.Microstructures and densification of MoSi_2-SiC composite by field-activated and pressure-assisted combustion synthesis[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,20091/2(1/2):136-142.
[7] Shahrouz Zamani;Hamid Reza Bakhsheshi-Rad;Ali Shokuhfar.Synthesis and characterization of MoSi_2-Mo_5Si_3 nanocomposite by mechanical alloying and heat treatment[J].International Journal of Refractory Metals & Hard Materials,2012Mar.(Mar.):236-241.
[8] Jianguang Xu;Fang Chen;Feng Tan.In-situ preparation of SiC-MoSi_2 composite by microwave reaction sintering[J].CERAMICS INTERNATIONAL,20128(8):6895-6898.
[9] 张小立;金志浩;张振国;王志新.反应熔渗SiC/MoSi_2和SiC/Mo(Si,Al)_2复相材料抗氧化行为[J].复合材料学报,2010(1):104-108.
[10] M ZAKERI;M AHMADI.Effect of starting composition on formation of MoSi_2-SiC nanocomposite powder via ball milling[J].Bulletin of Materials Science,20124(4):533-538.
[11] Manish Patel;J. Subramanyuam;V.V. Bhanu Prasad.Synthesis and mechanical properties of nanocrystalline MoSi_2-SiC composite[J].Scripta materialia,20083(3):211-214.
[12] 何子博;李贺军;史小红;付前刚;吴恒.化学气相浸渗/反应法制备MoSi2-SiC涂层的合成机理及其氧化性能[J].中国有色金属学报(英文版),2013(7):2100-2106.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%