通过测量极化和分散能力,对以Watts型电镀Ni溶液为基础的几种溶液进行了研究,考察了NiSO4和NaCl含量的影响,并采用SEM和XRD方法对Ni沉积层形貌及其结晶择优取向进行了分析.结果表明,综合考虑电导率和极化度的乘积,是显著提升溶液分散能力的重要途径;电沉积Ni镀层表面形貌主要受控于溶液中阴离子种类和数量,其晶粒尺寸和择优取向受控于过电位.
参考文献
| [1] | Zhang H X,Wang W.Electroplating Technique.Tianjin:Tianjin Science and Technology Press,2002:50(张宏祥,王位.电镀工艺学.天津:天津科学技术出版社,2002:50) |
| [2] | Ciszewski A,Posluszny S,Milczarek G,Baraniak M.Surf Coat Technol,2004; 183:127 |
| [3] | Gao C,Lu Y,Yue S,Wang H.Trans last Met Finish,1999; 77:75 |
| [4] | Miluskin A S.Zashch Met,1993; 29:275 |
| [5] | Gao C,Lu Y,Liu R.Plat Surf Finish,1997; 47:83 |
| [6] | Gamburg Y D,Grosheva M Y,Biallozor S,Hass M.Surf Coat Technol,2002; 150:95 |
| [7] | Ibrahim M A M,El Rehim S S A,El Wahaab S M A,Dankeria M M.Plat Surf Finish,1999; 86:69 |
| [8] | Marikkannu K R,Kalaignan G P,Vasudevan T.J Alloys Compd,2007; 438:332 |
| [9] | Wunsehe M,Dahms W,Meyer H,Schumacher R.Electrochim Acta,1994; 8-9:1133 |
| [10] | Hong R,Kuang S L.Electroplat Finish,1996; 15(4):2(洪榕,邝少林.电镀与涂饰,1996;15(4):2) |
| [11] | Zheng H J,Ma C A,Zhao J Q.Electroplat Pollution Control,2003; 23(1):7(郑华均,马淳安,赵建权.电镀与环保,2003;23(1):7) |
| [12] | Abdel-Hamid Z.Mater Chern Phys,1998; 53:235 |
| [13] | Zhou S M.Principle and Research Method for Metal Electrodeposition.Shanghai:Shanghai Science and Technology Press,1987:76(周绍民.金属电沉积-原理与研究方法.上海:上海科学技术出版社,1987:76) |
| [14] | Watanabe T,Minami S.J Jpn Inst Met,2000; 64:67(渡边澈,南修介.日本金属会志,2000;64:67) |
| [15] | Winand R.Electrochim Acta,1994; 38:1091 |
| [16] | Finch GI,Layton D N.J Electrodepositors Tech Soc,1951; 27:215 |
| [17] | Menzies I A,Ng C S.Trans Inst Met Finish,1969; 47:156 |
| [18] | Sibley F,Brook P A.Electrodeposition Surf Treat,1974; 2:117 |
| [19] | Jones M H,Kenez M G.Plating,1966; 153:995 |
| [20] | Vagramyan A T,Fotueva T A.J Electrochem Soc,1963; 110:1030 |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%