对在超声场作用下采用氨水中和氯氧锑(Sb4O5Cl2)制备超细立方晶型Sb2O3的工艺过程和条件进行了研究.结果表明,在超声场作用下制得的Sb2O3为立方晶型,当超声功率为100W,超声时间30min,温度为20℃时,Sb2O3的平均粒径为0.777μm,其分散性较好.通过XRD、SEM和激光粒度仪等测试手段,探讨了超声功率、超声时间、氯氧锑与蒸馏水的调浆液固比和温度等条件对Sb2O3晶型和颗粒粒径的影响.
参考文献
| [1] | 李文杰,徐本富(LI Wen-Jie,et al).广东工学院学报(Journal of Guangdong Institute of Technology),1993,10(2):51-58. |
| [2] | 段学臣,赵天从(DUAN Xue-Chen,et al).中国有色金属学报(The Chinese Journal of Nonferrous Metals),1996,6(1):36-39. |
| [3] | 甘庆民,杨秉文(GAN Qing-Min,et al).材料工程(Material Engineering),1997,(8):27,46. |
| [4] | 张多默,肖松文,刘志宏,等(ZHANG Duo-Mo,et al).中南大学学报(Journal of Central South University),2000,31(2):121-123. |
| [5] | 肖松文,刘志宏,李启厚,等(XIAO Song-Wen,et al).矿冶工程(Mining and Metallurgical Engineering),1999,19(3):39-41. |
| [6] | Suslick K S,Hyeon T,Fang M,Materials Science and Engineering:A,1995,204(1-2):186-192. |
| [7] | Kristl M,Drofenik M.Inorganic Chemistry Communications,2003,6 (12):1419-1422. |
| [8] | Cui H M,Liu H,Wang J Y,et al.Journal of Crystal Growth,2004,271 (3-4):456-461. |
| [9] | 张昭,吴潘,王乐飞,等(ZHANG Zhao,et al).中国有色金属学报(The Chinese Journal of Nonferrous Metals),2005,15(2):321-326. |
| [10] | 吴争平,尹周谰,陈启元,等(WU Zhen-Ping,et al).过程工程学报(The Chinese Journal of Process Engineering),2002,2(1):26-31. |
| [11] | Borkovska L V,Baran M P.Korsunska N O,et al.Physica,2003,B340-342:258-262. |
| [12] | Kumar R Vijaya,Elgamioel R,Koltypin Yu,et al.Journal of Crystal Growth,2003,250 (3-4):409-417. |
| [13] | 徐华蕊,李凤生,陈舒林,等(XU Hua-Rui,et al).化工进展(Chemical Industry and Engineering Process),1996,(5):20-31,57. |
| [14] | 陈雪梅,陈彩凤,陈志刚(CHEN Xue-Mei,et al).中国有色金属学报(The Chinese Journal of Nonferrous Metals),2003,13(10):122-126. |
| [15] | 梁新义,秦永宁,齐晓周,等(LIANG Xin-Yi,et al).化学物理学报(Chinese Journal of Chemical Physics),1998,11(4):375～378. |
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