高效液相色谱法检测食品中多种香料共存时的罂粟壳

1.贵州大学化学系,贵州,贵阳,550025

2.贵州大学化学系,贵州,贵阳,550025

Determination of Pericarpium Papaveris in Foods Accompanied with Some Fragrant Substances by High Performance Liquid Chromatography

采用高效液相色谱法检测食品中多种香料共存时的罂粟壳.样品经碱化后采用氯仿-乙醇(体积比为9:1)提取,在苯基柱上以乙腈-甲醇-水为流动相进行分离,外标法定量.罂粟碱,吗啡,可待因在1.2mg/L～100mg/L范围内线性关系良好,平均回收率为79.3%～86.1%.该方法的专属性和准确度较高.

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[2]	The Pharmacopoeia Commission of Ministry of Public Health, the People's Republic of China(卫生部药典委员会). Pharmacopoeia of People's Republic of China , Part 1(中华人民共和国药典(一部)).Beijing:People's Health Press(北京:人民卫生出版社),1990.330-331
[3]	RAO De-rong,SHAN Hou-an,LIN Chang-xiang,et al(饶德荣,单厚安,林昌祥,等 ). Food Science(食品科学),1993,157(1):58-60[ ZK)]

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