利用高速逆流色谱对传统中药黄柏中的生物碱类活性成分进行了制备分离.两相溶剂分离系统采用氯仿-甲醇-0.5 mol/L HCl(体积比为2∶1∶1),并对制备物进行了薄层色谱分析.证实了生物碱成分,检出了小檗碱.
参考文献
[1] | Ito Y. CRC Crit Rev Anal Chem, 1986, 17:65 |
[2] | Ito Y, Conway W D. High-Speed Countercurrent Chromatography. New York: John Wiley & Sons, Inc., 1996 |
[3] | YUAN Li-ming, FU Ruo-nong, ZHANG Tian-you.Chinese Journal of Pharmaceutical Analysis, 1998,18(1):60 袁黎明,傅若农,张天佑. 药物分析杂志,1998,18(1):60 |
[4] | YUAN Li-ming, FU Ruo-nong, ZHANG Tian-you. Chinese Journal of Chromatography, 1998,16(4):361袁黎明, 傅若农, 张天佑, 等. 色谱,1998,16(4):361 |
[5] | Yuan L M, Zi M, Ai P, et al. J Chromatogr A, 2001, 927(1-2):91 |
[6] | Yuan L M, Chen X X, Ai P, et al. J Liq Chromatogr Relat Technol, 2001, 24(19):2961 |
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