利用制备高效液相色谱法从大豆总异黄酮提取物中制备出了3种大豆异黄酮糖苷.在Nova-Pak HR C18色谱柱(100 mm×25 mm i.d.,6 μm)上,以甲醇-体积分数为0.1%的乙酸水溶液(体积比为23∶77)为流动相,流速为20 mL/min,采用等度洗脱方式,制备了3种大豆异黄酮糖苷,经质谱分析,确认它们分别为大豆苷、黄豆苷和染料木苷.高效液相色谱分析表明,所制备的3种化合物的纯度均达到了99%以上.
参考文献
| [1] | Yang Hu.Journal of Cereals & Oils (杨虎.粮食与油脂),2006(1):44 |
| [2] | Ma Guizhi,Gao Xiaoli.Chinese Traditional Patent Medicine(马桂芝,高晓黎.中成药),2002,24(6):461 |
| [3] | Guan Junjun,Fang Xixiu.China Western Cereals & Oils Technology (管军军,方希修.西部粮油科技),2003(6):59 |
| [4] | Wiseman H,Casey K,Clarke D B,Barnes K A,Bowey E.J Agric Food Chem,2002,50(6):1 404 |
| [5] | Sun Junming,Ding Anlin,Dong Huiru.Soybean Science (孙君明,丁安林,东惠茹.大豆科学),2000,19(1):15 |
| [6] | Fang N B,Yu S G,Badger T M.J Agric Food Chem,2002,50(9):2 700 |
| [7] | Wu Q L,Wang M F,Sciarappa W J,Simon J E.J Agric Food Chem,2004,52(10):2 763 |
| [8] | Qu Liping,Mi Heming,Fan Guorong.Journal of Pharmaceutical Practice (曲丽萍,宓鹤鸣,范国荣.药学实践杂志),2006,24(2):69 |
| [9] | Yuan Jian,J?Xingrong.Food Science (袁建,鞠兴荣.食品科学),2002,23(8):118 |
| [10] | Yuan Qipeng,Zhang Huai,Qian Zhongming.Soybean Science (袁其朋,张怀,钱忠明.大豆科学),2002,21(3):177 |
| [11] | Rostagno M A,Palma M,Barroso C G.J Chromatogr A,2003,1 012:119 |
| [12] | Pan Liaoming.Journal of Sichuan University:Engineering Science Edition (潘廖明.四川大学学报:工程科学版),2004,36(1):74 |
| [13] | Yao Kai,Jia Dongying,He Qiang,Lü Yuanping.Journal of Sichuan University:Engineering Science Edition (姚开,贾冬英,何强,吕远平.四川大学学报:工程科学版),2004,36(3):77 |
| [14] | Liu Pingping,Li Yunzheng,Zhang Qingshan.Fine Chemicals (刘苹苹,李云政,张青山.精细化工),2004,21(3):200 |
| [15] | Xu Deping,Jiang Hanhu,Xiao Kai,Xuan Lijiang.Journal of Nanjing Agricultural University (徐德平,江汉湖,肖凯,宣利江.南京农业大学学报),2001,24(3):8 |
| [16] | Yang F Q,Ma Y,Ito Y.J Chromatogr A,2001,928:163 |
| [17] | Du Q Z,Li Z H,Ito Y.J Chromatogr A,2001,923:271 |
| [18] | Jiang Heyuan,Tai Jianxiang,Lü Feijie.Food Science (江和源,台建祥,吕飞杰.食品科学),2004,25(1):85 |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%