以两种药材为研究实例,对加速溶剂萃取法(ASE)在中药材有效成分提取研究中的应用进行了简要介绍.采用正交试验法考察了提取丹参中丹酚酸B的提取条件(萃取温度、静态萃取时间、萃取溶剂以及料液比),确定了较好的实验条件.比较了ASE、水蒸气蒸馏法、超声波提取法及索氏提取法对木香挥发油的提取效果,结果表明ASE对木香挥发油的提取效果最好.
参考文献
[1] | Richter B E,Jones B A,Ezzell J L,Porter N L,Avdalovic N,Pohl C.Anal Chem,1996,68(6):1 033 |
[2] | Abend A M,Chung L,McCollum D G,Wuelfing W P.J Pharm Biomed Anal,2003,31(6):1 177 |
[3] | Dabrowski L,Giergielewicz-Mozajska H,Biziuk M,Gaca J,Nameisnik J.J Chromatogr A,2002,957:59 |
[4] | Giergielewicz-Mozajska H,Dabrowski L,Namiesnik J.Critical Reviews Anal Chem,2001,31(3):149 |
[5] | Urraca J L,Marazuela M D,Moreno-Bondi M C.Anal Chim Acta,2004,524:175 |
[6] | Bustamante-Rangel M,Delgado-Zamarreno M M,Sanchez-Perez A,Carabias-Martinez R.Anal Chim Acta,2007,587:216 |
[7] | Nording M,Sporring S,Wiberg K,Bjorklund E,Haglund P.Anal Bioanal Chem,2005,381:1 472 |
[8] | Li X,Zhang Y,Sun Y Z,Zhong W K,Qiu Y M,Chen Y Z,Wang D N.Chinese Journal of Chromatography (李翔,张垚,孙毅之,仲维科,邱月明,陈彦长,王大宁.色谱),2006,24(4):347 |
[9] | Shao B,Han H,Li D M,Zhao R,Meng J,Ma Y L.Chinese Journal of Chromatography (邵兵,韩灏,李冬梅,赵榕,孟娟,马亚鲁.色谱),2005,23(4):362 |
[10] | Wan J B,Yang F Q,Li S P,Wang Y T,Cui X M.J Pharm Biomed Anal,2006,41:1 596 |
[11] | Lao S C,Li S P,Kan K K W,Li P,Wan J B,Wang Y T,Dong T T X,Tsim K W K.Anal Chim Acta,2004,526:131 |
[12] | Peres V F,Saffi J,Melecchi M I S,Abad F C,de Assis Jacques R,Martinez M M,Oliveira E C,Caramao E B.J Chromatogr A,2006,1 105:115 |
[13] | Eng A T W,Heng M Y,Ong E S.Anal Chim Acta,2007,583:289 |
[14] | Yang F Q,Li S P,Chen Y,Lao S C,Wang Y T,Dong T T X,Tsim K W K.J Pharm Biomed Anal,2005,39:552 |
[15] | Tam C U,Yang F Q,Zhang Q W,Guan J,Li S P.J Pharm Biomed Anal,2007,44:444 |
[16] | Li P,Li S P,Lao S C,Fu C M,Kan K K W,Wang Y T.J Pharm Biomed Anal,2006,40:1 073 |
[17] | Jiang Y,Li P,Li S P,Wang Y T,Tu P.J Pharm Biomed Anal,2007,43:341 |
[18] | Ong E S,Len S M.Anal Chim Acta,2003,482:81 |
[19] | Jiang Y,Li S P,Chang H T,Wang Y T,Tu P F.J Chromatogr A,2006,1 108:268 |
[20] | Qin N Y,Yang F Q,Wang Y T,Li S P.J Pharm Biomed Anal,2007,43:486 |
[21] | Deng C H,Yang X H,Zhang X M.Talanta,2005,68:6 |
[22] | Yang F Q,Wang Y T,Li S P.J Chromatogr A,2006,1 134:226 |
[23] | Wan J B,Lai C M,Li S P,Lee M Y,Kong L Y,Wang Y T.J Pharm Biomed Anal,2006,41:274 |
[24] | Zhao J,Li S P,Yang F Q,Li P,Wang Y T.J Chromatogr A,2006,1 108:188 |
[25] | Wang J Q,Zhao M J,Lin L,Chai Y L,Zeng S.Chinese Traditional and Herbal Drugs (汪家权,赵民军,林岚,柴婴蕾,曾苏.中草药),2005,36(12):1 797 |
[26] | Li P,Wan J B,Li S P,Wang Y T.Chinese Journal of Natural Medicines (李鹏,万建波,李绍平,王一涛.中国天然药物),2004,2(3):157 |
[27] | Yu L H,Song Z G,Chen J H,Mou D H,Su L K,Teng J W.Chinese Journal of Analysis Laboratory (喻凌寒,宋之光,陈江韩,牟德海,苏流坤,腾久委.分析试验室),2006,25(8):68 |
[28] | Wang S H,Xiong Y,Wang X H.Chinese Journal of Pharmaceutical Analysis (王淑红,熊英,王祥红.药物分析杂志),2006,26(5):703 |
[29] | Wang Q,Liu S K,Fu C M,Li Z W.West China Journal of Pharmaceutical Sciences (王乾,刘三康,付春梅,李章万.华西药学杂志),2006,21(2):184 |
[30] | Su X G,Huang T L,Wang N S.Traditional Chinese Drug Research & Clinical Pharmacology (苏新国,黄天来,王宁生.中药新药与临床药理),2007,18(2):141 |
[31] | Xu H,Wang Z T,Liu S S,Jiang Y T,Liu K.Chinese Pharmaceutical Journal (许卉,王峥涛,刘生生,姜永涛,刘珂.中国药学杂志),2001,41(16):1 214 |
[32] | Yang H,Xie J L,Sun H D.Acta Botanica Yunnanica (杨辉,谢金伦,孙汉董.云南植物研究),1997,19(1):85 |
[33] | Yin H Q,Qi X L,Hua H M,Pei Y H.Chinese Journal of Medicinal Chemistry(尹宏权,齐秀兰,华会明,裴月湖.中国药物化学杂志),2005,15(4):217 |
[34] | Dai B,Qiu C E.Chinese Journal of Ethnomedicine and Ethnopharmacy (戴斌,丘翠嫦.中国民族民间医药杂志),1995,1:15 |
[35] | Test Methods for Evaluation Solid Waste,Method 3545.USEPA SW-846.Washington,D C:GPO,1995 |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%