建立了同时测定厚朴温中胶囊中山姜素、甘草酸、和厚朴酚、小豆蔻明、木香烃内酯、去氢木香内酯及厚朴酚含量的反相高效液相色谱法.固定相为Scienhome C18柱(250 mm×4.6 mm,5 μm),流动相为甲醇-乙腈-0.06%磷酸溶液(体积比为38:27:35),流速为1.0 mL/min,柱温为30℃,检测波长为235 nm.在上述条件下,山姜素、甘草酸、和厚朴酚、小豆蔻明、木香烃内酯、去氢木香内酯及厚朴酚的质量浓度分别在0.885~17.7,107~2 140,8.85~17.7,1.035~20.7,4.85~97,5.9~118和17.5~350 mg/L时与色谱峰面积之间的线性关系良好;回收率分别为96.9%~101.1%,96.0%~100.5%,100.396~100.8%,97.7%~101.4%,100.4%~102.3%,96.0%~102.3%和96.2%~100.6%.该方法简便、快速、准确.可用于厚朴温中胶囊的质量控制.
参考文献
[1] | Xie M.Modern research of Chinese Medicine Prescription:the First Volume.Beijing:Academy Press (谢鸣.中医方剂现代研究:上卷.北京:学苑出版社),1997 |
[2] | Huang J Y.Clinical Journal of Anhui Traditional Chinese Medicine (黄家瑜.安徽中医临床杂志),1997,9(2):97 |
[3] | Wang L Q,Jiang R G.Chen H F.Chinese Traditional and Herbal Drugs (王立青,江荣高,陈蕙芳.中草药),2005,36 (10):1 591 |
[4] | Chen Q S.World Phytomedicines (陈泉生.国外医药:植物药分册),1981,3:38 |
[5] | Lin Y R,Chen H H,Ko C H,et al.Life Sciences,2007,81:1 071 |
[6] | Xu Q,Yi L T,Pan Y,et al.Progr Neuro Psychopharmacol Biol Psychiatry,2008,32:715 |
[7] | Lees E,Shin H T,Hwang H J,et al.Phytotherapy Research,2003,17(9):1041 |
[8] | AhmadS,Israf D A,Lajis N H,et al.Eur J Pharmacol,2006,538:188 |
[9] | Yue J M,Fan C Q,DongL,etal.China Patent 跃建民,樊成奇,董雷,等.中国专利),CN 200510024891.5.2005-10-26 |
[10] | Lai X R,Meng B H,Jiang Z R,et al.Progress in Modern Biomedicine (赖先荣,孟保华,江志尧,等.现代生物医学进展),2008,8(1);34 |
[11] | Wang Y B,Wang Q,Mao F L,et al.Journal of China Pharmaceutical University (王永兵,王强,毛富林,等.中国药科大学学报),2001,32(2):146 |
[12] | Rao W W,Lin Y D.Chinese Pharmaceutical Journal (饶伟文.林泳德.中国药学杂志),1998,33(12):743 |
[13] | Zou C Y,Liu P H,Li S G.China Journal of Chinese Materia Medica (邹婵英,刘培洪,李神革.中国中药杂志),2005,30(22):1 776 |
[14] | Tong R S.China Pharmacist(童荣生.中国药师),2006,9 (8):706 |
[15] | Meng C,Wu F,Ma L.Natural Product Research Development (孟超,吴丰,马林.天然产物研究与开发),2007,19:1 024 |
[16] | Li H,Chen B T,Weng L D,et al.Chinese Traditional and Herbal Drugs (李慧,陈宝田,翁立冬,等.中草药),2007,38(11):1659 |
[17] | Lee Y C,Huang C Y,Wen K C,et al.J Chromatogr A,1995,692:137 |
[18] | Sheu S J,Lu C F.J Chromatogr A,1995,704:518 |
[19] | Wu X N,Chen X G,Hu Z D.Talanta,2003,59:115 |
[20] | Li H,Lu D Q,Liu W M.Chinese Journal of Chromatography (李晖,卢定强,刘伟民.色谱),2004,22(3):258 |
[21] | Yuan C,Du K,Zhu L Q,et al.Chinese Journal of Chromatography (袁成,杜昆,朱丽青,等.色谱),2000,18(3):229 |
[22] | Gan G P,Jiang W,Liu Y W.China Pharmacist(干国平,江维,刘焱文.中国药师),2007,10(5):438 |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%