建立了测定纺织品中烷基酚(AP)和烷基酚聚氧乙烯醚(APnEO)(n=2～16)的正相高效液相色谱法.以甲醇为提取溶剂,用索氏抽提法提取纺织品中的AP和APnEO,用正相高效液相色谱法测定,并对提取溶剂、提取方式和净化条件等前处理条件进行优化.该方法的检出限为1.0 mg/kg,回收率为90.4% ～104.1% ,相对标准偏差为0.64% ～4.21% .采用该方法对多种基质纺织品进行检测,可满足残留检测要求.
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