对冷作模具钢SDC99盐浴渗V中VC覆层形成机理进行了研究.采用高分辨SEM和金相显微镜观察了渗V试样的横截面形貌及VC覆层微观形貌,并利用EDS对表面元素进行了能谱分析,利用XRD对盐浴试样表层进行了物相结构分析；采用原位纳米力学测试系统TriboIndenter对渗V试样截面硬度梯度进行了测试.结果表明:盐浴温度越高,在相同浸渗时间下形成的覆层越厚；VC覆层硬度约为22 GPa,远高于基体硬度7.0 GPa,覆层与基体之间硬度以较缓速度下降,表明界面处基体组织能对VC覆层起到良好的支撵作用.覆层生长的过程为:初始晶粒形核、长大,并有亚微晶粒在其表面生长；受钢中C活度的影响,覆层晶粒长成等轴晶,越靠近基体与覆层的界面,晶粒尺寸越小.在覆层晶粒生长初始阶段,SDC99钢上晶粒生长择优取向从(200)晶面转变为(111)晶面,随着时间的延长,覆层晶粒生长无明显择优取向,生长为等轴晶.
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