以无毒、绿色的葡萄糖为还原剂,在没有稳定剂、温和的液相反应条件下,同时还原氧化石墨和银氨溶液中的银氨离子,原位制备石墨烯-银纳米粒子复合材料.采用X射线衍射、红外吸收光谱、拉曼光谱、扫描电镜和透射电子显微镜对所制备的石墨烯-银纳米粒子复合材料进行了表征.结果表明:氧化石墨和银离子在反应过程中同时被葡萄糖还原,银纳米粒子均匀分布于石墨烯片层之间,生成的银纳米粒子中大多数存在着孪晶界,银纳米粒子的大小和分布受硝酸银用量的影响,在合适的银离子浓度下,负载在石墨烯片层上的银纳米粒子的粒径分布集中在25 nm左右；复合材料中石墨烯的拉曼信号由于银粒子的存在增强了7倍.
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