以邻苯二酚与二甘醇二取代物为原料,氢氧化钾为碱和模板剂,在微波辅助下,采用“一锅煮”法合成二苯并-18-冠-6.经单因素及正交实验考察了原料、溶剂、时间、温度和功率对反应收率的影响,获得了最佳的工艺条件:以邻苯二酚与二氯乙醚为原料,二甲亚砜为溶剂,反应温度70℃,时间60 min,功率500 W,收率可达46.3％.
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