应用化学, 2012, 29(5): 520-526. doi: 10.3724/SP.J.1095.2012.00300
二正丁基锡二(邻氯苯甲酸)酯配合物{[n-Bu2Sn(O2CC6H4C1)]2O}2的微波固相合成、结构及体外抗癌活性
张复兴 {"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"综述了变形高温合金和等轴晶铸造高温合金研制过程中的有关应用基础理论,主要涉及3个方面:变形高温合金和微量元素的作用机理;等轴晶铸造高温合金和蠕变机理研究;抗热腐蚀高温合金和新相变的发现及蠕变-疲劳-环境交互作用.","authors":[{"authorName":"郭建亭","id":"a9cb1e2a-3d60-416f-9686-16472f66513b","originalAuthorName":"郭建亭"}],"doi":"10.3724/SP.J.1037.2010.00474","fpage":"1303","id":"4531cd6a-3beb-4075-a0f0-d151a3961796","issue":"11","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"1d236411-5c40-4216-bec8-610266f1a5c6","keyword":"变形高温合金","originalKeyword":"变形高温合金"},{"id":"903fcf96-b7a5-45f4-8a3c-9f8a58a7f6dd","keyword":"等轴晶铸造高温合金","originalKeyword":"等轴晶铸造高温合金"},{"id":"d86ec499-b281-4d35-b9a1-52c10a7dbc44","keyword":"微量元素作用机理","originalKeyword":"微量元素作用机理"},{"id":"e2e623e4-11ac-46c8-a13a-b7313e224e3a","keyword":"蠕变机理","originalKeyword":"蠕变机理"},{"id":"478c4006-f22d-44fe-9930-60c2640b2df0","keyword":"相变","originalKeyword":"相变"}],"language":"zh","publisherId":"jsxb201011003","title":"变形高温合金和等轴晶铸造高温合金材料与应用基础理论研究","volume":"46","year":"2010"},{"abstractinfo":"综述了变形高温合金和等轴晶铸造高温合金研制过程中的有关应用基础理论, 主要涉及3个方面: 变形高温合金和微量元素的作用机理; 等轴晶铸造高温合金和蠕变机理研究; 抗热腐蚀高温合金和新相变的发现及蠕变-疲劳-环境交互作用.","authors":[{"authorName":"郭建亭","id":"4ac08f23-7122-4ff5-a6b7-29b441559340","originalAuthorName":"郭建亭"}],"categoryName":"|","doi":"DOI: 10.3724/SP.J.1037.2010.00474","fpage":"1303","id":"94a10eaf-b947-4dbd-80d0-b55af2f9e5c8","issue":"11","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"0895d49e-b898-4dcd-b5a2-597b80a1bfdf","keyword":"变形高温合金","originalKeyword":"变形高温合金"},{"id":"a698450e-c224-422c-b377-7e12254c50ab","keyword":" equiaxed crystal cast superalloy","originalKeyword":" equiaxed crystal cast superalloy"},{"id":"9f4b2b4c-6891-4afd-ad81-7c30ef743f56","keyword":"mechanism of effect of minor elements","originalKeyword":"mechanism of effect of minor elements"},{"id":"95003388-6f1b-4622-955d-e4106614a915","keyword":"creep mechanism","originalKeyword":"creep 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transformation"}],"language":"zh","publisherId":"0412-1961_2010_11_9","title":"变形高温合金和等轴晶铸造高温合金材料与应用基础理论研究","volume":"46","year":"2010"},{"abstractinfo":"评述了镍基铸造高温合金的热等静压(HIP)处理对组织和力学性能的影响.镍基铸造高温合金由于存在着铸造工艺难以消除的气孔类缺陷,严重影响着合金的使用可靠性和成品率.通过HIP处理后的合金,不仅可有效地消除合金中的缺陷,获得致密合金,而且还可改善合金的显微组织,提高合金的拉伸、持久和疲劳性能,显著地减小性能分散度.","authors":[{"authorName":"呼和","id":"a13baa13-d340-49ab-9ce5-c3f0c7f533f6","originalAuthorName":"呼和"}],"categoryName":"|","doi":"","fpage":"1199","id":"c3fe4d19-5333-44f3-8b1c-56f26b847345","issue":"11","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"1ee9d56c-ba87-42cf-9365-9e6083943c63","keyword":"镍基铸造高温合金","originalKeyword":"镍基铸造高温合金"},{"id":"d0acba40-154a-4e88-b13e-e56d1919a9e3","keyword":"null","originalKeyword":"null"},{"id":"f3b02d7e-905e-4143-bd7e-d7b5cbc91426","keyword":"null","originalKeyword":"null"}],"language":"zh","publisherId":"0412-1961_2002_11_7","title":"镍基铸造高温合金的热等静压处理","volume":"38","year":"2002"},{"abstractinfo":"评述了镍基铸造高温合金的热等静压(HIP)处理对组织和力学性能的影响.镍基铸造高温合金由于存在着铸造工艺难以消除的气孔类缺陷,严重影响着合金的使用可靠性和成品率.通过HIP处理后的合金,不仅可有效地消除合金中的缺陷,获得致密合金,而且还可改善合金的显微组织,提高合金的拉伸、持久和疲劳性能,显著地减小性能分散度.","authors":[{"authorName":"呼和","id":"d159f347-a10b-413a-8a65-ed2564dd51a7","originalAuthorName":"呼和"}],"doi":"10.3321/j.issn:0412-1961.2002.11.013","fpage":"1199","id":"a057d861-cf1d-4716-bfb7-41f0fd880604","issue":"11","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"f0272987-d674-4ea4-9635-549f263e43e1","keyword":"镍基铸造高温合金","originalKeyword":"镍基铸造高温合金"},{"id":"ce9fc8d4-e4c1-4512-b296-73f4caaafb88","keyword":"热等静压","originalKeyword":"热等静压"},{"id":"e4351879-a433-4134-8517-a8d3ae75cd5c","keyword":"显微组织","originalKeyword":"显微组织"},{"id":"e9c81611-d409-470d-9b85-ae06b2024a31","keyword":"力学性能","originalKeyword":"力学性能"}],"language":"zh","publisherId":"jsxb200211013","title":"镍基铸造高温合金的热等静压处理","volume":"38","year":"2002"},{"abstractinfo":"普通铸造K403合金具有很好的高温力学性能,但塑性和中温力学性能差.为了提高K403合金的塑性和中温力学性能,采用细晶铸造工艺进行铸造,并对铸件进行热等静压和热处理.研究结果表明,细晶铸造K403合金经1190～1200℃/120～160Mpa/3～4h热等静压和1180℃/4h+980℃/6h热处理后,合金在中温下的拉伸、持久和低周疲劳性能得到大幅度的提高,且高温持久性能与普通铸造K403合金相当.","authors":[{"authorName":"汤鑫","id":"e48f9b8b-46eb-40d8-b34d-355b97db7fe1","originalAuthorName":"汤鑫"},{"authorName":"刘发信","id":"da823d24-5ec6-4f61-9d65-d77e9c56a53d","originalAuthorName":"刘发信"},{"authorName":"李爱兰","id":"9db744ac-1981-4072-9911-21494bc030d4","originalAuthorName":"李爱兰"},{"authorName":"盖其东","id":"67cac0ef-a6a3-4f4e-ac31-be3423e4cdd0","originalAuthorName":"盖其东"},{"authorName":"韩梅","id":"d5798808-20e5-4537-9090-63346b29903b","originalAuthorName":"韩梅"}],"doi":"10.3969/j.issn.1005-5053.2003.z1.011","fpage":"45","id":"8d9a1ddb-0d20-425d-9d26-13b8008eeeb8","issue":"z1","journal":{"abbrevTitle":"HKCLXB","coverImgSrc":"journal/img/cover/HKCLXB.jpg","id":"41","issnPpub":"1005-5053","publisherId":"HKCLXB","title":"航空材料学报"},"keywords":[{"id":"ee733668-07d1-4ba1-9eaa-63e764abc17e","keyword":"细晶铸造","originalKeyword":"细晶铸造"},{"id":"c76ad816-c26c-42ae-9a6e-2a198e1cc54d","keyword":"热等静压","originalKeyword":"热等静压"},{"id":"b7a9f8b2-bb6d-40a5-aed4-fa5cd352433d","keyword":"热处理","originalKeyword":"热处理"},{"id":"11233c42-8d0c-4ccc-b232-9b4e833a43ee","keyword":"力学性能","originalKeyword":"力学性能"}],"language":"zh","publisherId":"hkclxb2003z1011","title":"细晶铸造K403合金热等静压及热处理工艺研究","volume":"23","year":"2003"},{"abstractinfo":"研究分析了不同保温温度、冷却水温等条件对铝合金等轴晶形核率、柱状晶形核率、柱状晶向等轴晶转变(CET)位置的影响规律.试验结果表明:降低保温温度、升高冷却水温,会增大等轴晶区的面积；降低冷却水温、降低保温温度会增大铸件柱状晶和等轴晶的形核率.还根据获得的CET位置实验结果,讨论了国内外文献提出的CET位置判据对本研究的适用性,并针对本文的实验条件,提出了具有更高预测精度的CET转变判据.","authors":[{"authorName":"侯忠霖","id":"8ee644e6-a7de-43a0-a8ca-7194e35bd7db","originalAuthorName":"侯忠霖"},{"authorName":"姚山","id":"7bc4a33f-e0ba-4c0c-9a55-fc6ceadab624","originalAuthorName":"姚山"},{"authorName":"李婷","id":"41e82a43-c126-4895-92be-cb5a654c9847","originalAuthorName":"李婷"},{"authorName":"沙明红","id":"38c06282-3f29-432d-b1a9-c448495f68dc","originalAuthorName":"沙明红"}],"doi":"","fpage":"120","id":"9a915906-6030-4cc5-b834-ea72f407cf31","issue":"2","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"247b4d44-8d6f-46bb-8e57-2c32f70e4be6","keyword":"铝合金","originalKeyword":"铝合金"},{"id":"ef7ec700-c5c1-4d5f-bc80-022772ca9c70","keyword":"凝固","originalKeyword":"凝固"},{"id":"5c8e3b91-8624-4705-bfbd-421ff602f3be","keyword":"柱状晶向等轴晶转变(CET)","originalKeyword":"柱状晶向等轴晶转变(CET)"},{"id":"bd1ad656-6fc7-4480-866e-b7de0f0fdc62","keyword":"判据","originalKeyword":"判据"}],"language":"zh","publisherId":"jsrclxb201302024","title":"铝合金凝固过程柱状晶向等轴晶转变的研究","volume":"34","year":"2013"},{"abstractinfo":"对涡轮叶轮用铸造高温合金进行热等静压处理.结果表明,通过热等静压处理,铸造高温合金的疏松缺陷减少,显微组织均匀细化,合金致密度提高,而且力学性能得到了改善.","authors":[{"authorName":"张树才","id":"2ece2c72-7240-43f5-83f2-abb38820d4d1","originalAuthorName":"张树才"},{"authorName":"郭志俊","id":"985dd700-d214-40ee-8997-d19e276b3858","originalAuthorName":"郭志俊"},{"authorName":"王跃旗","id":"f568688b-fc69-430a-bcaa-c107bb989995","originalAuthorName":"王跃旗"},{"authorName":"李爱民","id":"ebdb0f8f-5816-4366-b8b6-f14a650821f7","originalAuthorName":"李爱民"},{"authorName":"王晋伟","id":"672b90df-fb3e-431a-b57b-d6a4fc95059b","originalAuthorName":"王晋伟"},{"authorName":"冯云虎","id":"80853c06-c5c9-4927-8920-b8be7f72e435","originalAuthorName":"冯云虎"}],"doi":"33-1331/TJ.20110704.2233.007","fpage":"67","id":"3ba4841c-83b9-479d-aad4-ed409f4ebeee","issue":"4","journal":{"abbrevTitle":"BQCLKXYGC","coverImgSrc":"journal/img/cover/BQCLKXYGC.jpg","id":"4","issnPpub":"1004-244X","publisherId":"BQCLKXYGC","title":"兵器材料科学与工程 "},"keywords":[{"id":"d7360e7f-4c81-41e4-bd9e-7660a38c86c0","keyword":"涡轮叶轮","originalKeyword":"涡轮叶轮"},{"id":"98fa637d-ae36-4a2d-96da-16832dcd9a1c","keyword":"铸造高温合金","originalKeyword":"铸造高温合金"},{"id":"51c58e6c-410f-44eb-93a6-821364e26a21","keyword":"热等静压","originalKeyword":"热等静压"}],"language":"zh","publisherId":"bqclkxygc201104019","title":"涡轮叶轮用铸造高温合金的热等静压处理研究","volume":"00","year":"2011"},{"abstractinfo":"通过传统铸造方法和细晶铸造工艺制备一种铸造镍基高温合金的6种不同形态与尺寸的晶粒.结果表明,细晶铸造工艺制备的样品心部为0.5 mm左右的等轴晶,外部为柱状晶.相比传统铸造方法,细晶铸造工艺获得的晶粒较为细小.y'相和碳化物随晶粒尺寸减小而变得细小.室温拉伸性能和550℃下高周疲劳性能随晶粒尺寸降低而提高;在760℃和应力662MPa条件下,合金的持久性能随晶粒尺寸减小而增加;但在982℃和应力186MPa条件下,合金的持久性能随之降低.细化晶粒提高了合金的中、低温力学性能,但对其高温力学性能不利.","authors":[{"authorName":"杨金侠","id":"aac238ba-186d-4ce1-85b5-ccfe38a7044b","originalAuthorName":"杨金侠"},{"authorName":"孙元","id":"4c1d69b7-1ab0-4379-b25d-6f1e702df39d","originalAuthorName":"孙元"},{"authorName":"金涛","id":"e05d5802-35be-4976-bb01-3d59c51c47ce","originalAuthorName":"金涛"},{"authorName":"孙晓峰","id":"c16e2659-e51a-4ac9-b9ab-520c5d45404f","originalAuthorName":"孙晓峰"},{"authorName":"胡壮麒","id":"d7b5beeb-e66a-43c7-9959-8c0f304a6497","originalAuthorName":"胡壮麒"}],"doi":"10.3724/SP.J.1037.2013.00745","fpage":"839","id":"dc9f7792-7bac-45c6-8fb0-1856fe240e39","issue":"7","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"fe4c9bca-597a-4a8b-8914-99267f7105f4","keyword":"镍基高温合金","originalKeyword":"镍基高温合金"},{"id":"cc05d63a-abb9-4354-85dc-5e7fa154e875","keyword":"细化剂","originalKeyword":"细化剂"},{"id":"9b9dd27e-743c-492d-b906-34d7f98ba9af","keyword":"持久性能","originalKeyword":"持久性能"},{"id":"585c6f35-188c-4ebb-bae7-5ca1155690c6","keyword":"高周疲劳性能","originalKeyword":"高周疲劳性能"}],"language":"zh","publisherId":"jsxb201407009","title":"一种细晶铸造镍基高温合金的组织与力学性能","volume":"50","year":"2014"},{"abstractinfo":"本文对TC11钛合金棒材显微组织不均匀缺陷产生原因及消除途径进行了研究。结果表明,由于铸锭最初锻造温度在β相区,随后两相区锻造变形量不大且分布不均匀,致使部分晶界α和二次α聚集并粗化呈块状,或沿主变形方向拉长呈条状,或遗留下原晶界α。若采用(α+β)中间形变热处理+β处理、水冷+再结晶退火、空冷的工艺,可完全消除晶界α,拉长α和块状α相,获得均匀细小等轴α组织,初生等轴α相的平均直径可细化至1.9μm。","authors":[{"authorName":"苏祖武","id":"b05594bf-7fdb-4282-9615-41617ef9fa25","originalAuthorName":"苏祖武"},{"authorName":"孟国文","id":"f3c4e746-4c18-4995-802a-3081a3e10661","originalAuthorName":"孟国文"},{"authorName":"郭鸿镇","id":"5b0fe10c-88be-4be3-b397-ceb3329f9a32","originalAuthorName":"郭鸿镇"},{"authorName":"刘建超","id":"b5013875-c513-483d-a674-545a475b7b5a","originalAuthorName":"刘建超"},{"authorName":"姚泽坤","id":"acec6d5b-27bc-4e1e-8157-3c9f6c6463a6","originalAuthorName":"姚泽坤"},{"authorName":"杨昭苏","id":"4b803334-c4e4-4773-a1ca-efef89c26bb4","originalAuthorName":"杨昭苏"},{"authorName":"胡宗式","id":"cfceac02-883d-4d32-9011-7e22387ab349","originalAuthorName":"胡宗式"}],"categoryName":"|","doi":"","fpage":"79","id":"f688e389-919f-4847-8609-ba0b49fd569a","issue":"5","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"fe91acb3-9a04-4bfe-a007-0256b0305b9c","keyword":"TC11钛合金","originalKeyword":"TC11钛合金"},{"id":"d139a585-05a5-41fd-811d-f3abee894c78","keyword":"forging","originalKeyword":"forging"},{"id":"a9cf3ce1-4d78-4062-adec-463d2aaceb5b","keyword":"microstructure","originalKeyword":"microstructure"},{"id":"e87d7aed-7fd0-4033-bca2-0de53a319236","keyword":"equiaxed grain refinement","originalKeyword":"equiaxed grain refinement"}],"language":"zh","publisherId":"0412-1961_1991_5_8","title":"TC11钛合金棒材显微组织等轴细晶化工艺研究","volume":"27","year":"1991"},{"abstractinfo":"采用适当热等静压工艺处理铸造高温合金,利用高温高压实现铸件内部疏松孔洞的蠕变扩散,达到闭合疏松和均匀合金组织的目的,使铸造高温合金的综合力学性能,尤其是疲劳性能、塑性及合金力学性能的稳定性显著提高,大大提高了铸件使用的安全性和可靠性.介绍了热等静压工艺处理高温合金铸件的致密化原理、工艺因素及其对合金组织和性能的影响,同时概述了热等静压技术的应用成果及发展状况.","authors":[{"authorName":"邵冲","id":"6a65b512-e9dd-4534-b98c-c52faf23dc0d","originalAuthorName":"邵冲"},{"authorName":"刘慧渊","id":"4c789765-ff02-4c76-85d0-90b645aeec19","originalAuthorName":"刘慧渊"},{"authorName":"李俊涛","id":"c89884f2-1fbb-4b1a-abd8-faa6396236a8","originalAuthorName":"李俊涛"},{"authorName":"马章林","id":"f5883898-8879-4d98-8140-a2a0cd34e339","originalAuthorName":"马章林"},{"authorName":"赵明汉","id":"30dce477-e135-4548-ba8c-fb74c1925894","originalAuthorName":"赵明汉"}],"doi":"","fpage":"121","id":"6f721a91-49cc-4546-b00b-45c3cf939fa2","issue":"19","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"497f2f8e-f4db-4bfc-ad70-9ceed4e9d17e","keyword":"热等静压","originalKeyword":"热等静压"},{"id":"07da87ec-c5cc-4410-b94a-5a9465357bd7","keyword":"致密化","originalKeyword":"致密化"},{"id":"43529cc9-ca83-4c45-8612-7b3c4b8a31b6","keyword":"显微组织","originalKeyword":"显微组织"},{"id":"4f44f02a-80d1-4195-8b05-21c083a7fa57","keyword":"力学性能","originalKeyword":"力学性能"},{"id":"a1902338-568e-40c7-8ab2-308a5fe62a03","keyword":"高温合金","originalKeyword":"高温合金"}],"language":"zh","publisherId":"cldb201219027","title":"热等静压在铸造高温合金领域的应用","volume":"26","year":"2012"}],"totalpage":10187,"totalrecord":101868}