应用化学, 2013, 30(8): 971-973. doi: 10.3724/SP.J.1095.2013.20530
邻氯苯甲腈的新合成法
朱益忠 1, , 张喜全 2, , 刘飞 3, , 顾红梅 {"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"通过四种不同的分步淬火热处理工艺,相应地获得了四种不同组织的双相钢.研究表明,随着马氏体含量的增加,双相钢的最大拉伸强度随之增加,延伸率随着马氏体的增加而降低.试样的铁素体晶粒大小在不同的马氏体范围内对强度和延伸率有不同的影响.","authors":[{"authorName":"曹同友","id":"7eaf104c-a699-4894-9eb9-54f1a1f64a0e","originalAuthorName":"曹同友"}],"doi":"10.3969/j.issn.1001-1447.2006.04.006","fpage":"24","id":"65f43d0f-3577-42ec-8bc9-9ed76bbf2ded","issue":"4","journal":{"abbrevTitle":"GTYJ","coverImgSrc":"journal/img/cover/GTYJ.jpg","id":"29","issnPpub":"1001-1447","publisherId":"GTYJ","title":"钢铁研究"},"keywords":[{"id":"d941d796-88f1-46f9-9b62-6b71e40eff87","keyword":"双相钢","originalKeyword":"双相钢"},{"id":"3d524566-478a-430b-9efa-1d4125552f27","keyword":"分步淬火","originalKeyword":"分步淬火"},{"id":"f87c1ef2-e250-4f40-aee1-05135236c160","keyword":"马氏体含量","originalKeyword":"马氏体含量"},{"id":"f4e25380-ba01-484e-824c-5a4c21770611","keyword":"性能","originalKeyword":"性能"}],"language":"zh","publisherId":"gtyj200604006","title":"双相碳钢性能与马氏体含量和晶粒大小关系初析","volume":"34","year":"2006"},{"abstractinfo":"通过四种不同的分步淬火热处理工艺,相应地获得了四种不同组织的双相钢.研究表明,随着马氏体含量的增加,双相钢的最大剪切应力随之增加.绝热剪切带的出现和由它引起的裂纹是动态扭矩试验时的重要特征.","authors":[{"authorName":"曹同友","id":"55e620f5-7a79-478f-a816-be94b372f1b3","originalAuthorName":"曹同友"}],"doi":"10.3969/j.issn.1001-1447.2006.01.005","fpage":"16","id":"21f171af-c90b-48c8-a359-d8afe6c24d12","issue":"1","journal":{"abbrevTitle":"GTYJ","coverImgSrc":"journal/img/cover/GTYJ.jpg","id":"29","issnPpub":"1001-1447","publisherId":"GTYJ","title":"钢铁研究"},"keywords":[{"id":"01b65763-d0b8-4e80-92d6-5b08b9c6c170","keyword":"双相钢","originalKeyword":"双相钢"},{"id":"a8c40f92-6f34-407d-b47a-a177625674de","keyword":"马氏体含量","originalKeyword":"马氏体含量"},{"id":"33517b00-4f4a-4952-82ad-08ef276d76e4","keyword":"动态扭矩","originalKeyword":"动态扭矩"},{"id":"a4a61606-523b-424e-9dcb-d50c04824c6b","keyword":"绝热剪切带","originalKeyword":"绝热剪切带"}],"language":"zh","publisherId":"gtyj200601005","title":"双相碳钢动态扭矩性能和马氏体含量关系的研究","volume":"34","year":"2006"},{"abstractinfo":"采用不同的两相区温度保温和盐水淬火处理,在实验室条件下得到不同马氏体含量的含钒双相钢.利用扫描电子显微镜对不同马氏体含量的试样的断口和断口侧面分析,发现在高马氏体含量下,双相钢变形和断裂与马氏体含量和组织形态有关.且其均匀变形阶段的应变硬化指数n值及应变硬化速率也会随着马氏体含量的增加而显著升高.而加入钒,其碳化物弥散分布在铁素体中,增强了双相钢的应变硬化能力,提高了双相钢的力学性能.","authors":[{"authorName":"黄群飞","id":"0a098f03-33a2-4c6d-a0b7-698737510471","originalAuthorName":"黄群飞"},{"authorName":"何燕霖","id":"beff9633-5409-4a3c-a9bc-d718eaac28e0","originalAuthorName":"何燕霖"},{"authorName":"罗娟娟","id":"9d2b7691-eee7-47a7-a747-4eb3b2161b18","originalAuthorName":"罗娟娟"},{"authorName":"史文","id":"ff2e7381-3be6-484b-8d8b-f4f96638c87e","originalAuthorName":"史文"},{"authorName":"李麟","id":"af3ed87e-34c2-482b-9491-0002b8ad721a","originalAuthorName":"李麟"}],"doi":"","fpage":"49","id":"e1226942-9fa3-46cf-8fad-36ad93020962","issue":"5","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"39276124-5d62-4177-8695-15da6569089a","keyword":"高马氏体量双相钢","originalKeyword":"高马氏体量双相钢"},{"id":"2818107c-8bec-4fe2-93ec-cb5ff32cf378","keyword":"组织","originalKeyword":"组织"},{"id":"063ed0cf-ff9a-4c0a-99aa-c185c1217d71","keyword":"应变硬化指数","originalKeyword":"应变硬化指数"},{"id":"c583d6cb-cc83-4521-b0a4-b87c9dba6db5","keyword":"应变硬化速率","originalKeyword":"应变硬化速率"}],"language":"zh","publisherId":"jsrclxb200805012","title":"高马氏体含量双相钢组织及变形研究","volume":"29","year":"2008"},{"abstractinfo":"用X射线衍射技术研究了304奥氏体不锈钢变形诱发马氏体相变倾向对成分的敏感性。在液氮内的拉伸结果表明： C、Mn、Cr和Ni的含量从标准范围的上限降到下限，显著增大形变诱发马氏体相变倾向和形变强化能力，尤其是C、Mn、Cr和Ni的含量接近下限的钢在室温下拉伸形成ε马氏体和α′马氏体，其中α′马氏体快速形成使流变应力迅速上升；此外发现，在液氮温度下，变形早期ε马氏体与α′马氏体同时存在，α′马氏体的体积分数累积到约70%后，ε马氏体消失。","authors":[{"authorName":"卓越","id":"f54ad30e-3ca4-4f42-851c-34e77731da59","originalAuthorName":"卓越"},{"authorName":"苏杰","id":"7b5f9301-0bf0-4aa6-b35b-d8172e74aa51","originalAuthorName":"苏杰"},{"authorName":"陈嘉砚","id":"4fa7f42b-53d9-4bfd-9ef9-0afb1426fb3d","originalAuthorName":"陈嘉砚"},{"authorName":"熊建新","id":"eb490379-b7ba-4dc7-9246-06dc84581fbf","originalAuthorName":"熊建新"}],"categoryName":"|","doi":"","fpage":"61","id":"9c80262e-d064-45a1-ba2d-9d144f8070c4","issue":"5","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"f501b9b7-6e52-4b45-86f3-75afb3690f12","keyword":"304不锈钢;形变诱发;马氏体相变;形变强化","originalKeyword":"304不锈钢;形变诱发;马氏体相变;形变强化"}],"language":"zh","publisherId":"0449-749X_2007_5_19","title":"C、Cr、Ni和Mn含量对304不锈钢变形诱发马氏体相变的影响","volume":"42","year":"2007"},{"abstractinfo":"用X射线衍射技术研究了304奥氏体不锈钢变形诱发马氏体相变倾向对成分的敏感性.在液氮内的拉伸结果表明: C、Mn、Cr和Ni的含量从标准范围的上限降到下限,显著增大形变诱发马氏体相变倾向和形变强化能力,尤其是C、Mn、Cr和Ni的含量接近下限的钢在室温下拉伸形成ε马氏体和α'马氏体,其中α'马氏体快速形成使流变应力迅速上升;此外发现,在液氮温度下,变形早期ε马氏体与α'马氏体同时存在,α'马氏体的体积分数累积到约70%后,ε马氏体消失.","authors":[{"authorName":"杨卓越","id":"52b80f46-7862-4ee0-b08b-e78197e8237e","originalAuthorName":"杨卓越"},{"authorName":"苏杰","id":"23968658-8bce-4dec-b272-170581b1c789","originalAuthorName":"苏杰"},{"authorName":"陈嘉砚","id":"40042771-daaf-4022-8e5a-9cc043ffa3e6","originalAuthorName":"陈嘉砚"},{"authorName":"熊建新","id":"f6b8445a-9ef3-4ef0-ae25-236f94618644","originalAuthorName":"熊建新"}],"doi":"","fpage":"61","id":"ce70b8bb-89c4-46ee-80cf-38bfcb960c0f","issue":"5","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"fa83f584-1de9-4e41-bc7d-978a8c7cb4e0","keyword":"304不锈钢","originalKeyword":"304不锈钢"},{"id":"5feff9bc-6965-4af2-a654-7b26ae86a080","keyword":"形变诱发","originalKeyword":"形变诱发"},{"id":"1bfb9626-0b40-45d9-8399-cecf74446079","keyword":"马氏体相变","originalKeyword":"马氏体相变"},{"id":"be20e590-6bbe-4bed-af97-761753811ae4","keyword":"形变强化","originalKeyword":"形变强化"}],"language":"zh","publisherId":"gt200705015","title":"C、Cr、Ni和Mn含量对304不锈钢变形诱发马氏体相变的影响","volume":"42","year":"2007"},{"abstractinfo":"利用Gleeble 1500热模拟试验机进行单轴压缩,通过基于马氏体温变形和两相区短时间退火的工艺制备了两种C含量的高锰TRIP钢,并结合扫描电镜、X射线和室温拉伸等实验研究了C含量对高锰TRIP钢制备过程的组织演变和室温力学性能的影响.结果表明,C含量从0.08％提高到0.18％,降低了逆转变奥氏体的化学驱动力,不利于温变形过程中逆转变奥氏体的形成.但由于马氏体分解可得到较多的渗碳体粒子,提高C含量使得退火组织中马奥岛含量和残留奥氏体含量增多且残留奥氏体C含量增加,因此提高了高锰TRIP钢的强度和塑性.","authors":[{"authorName":"郭志凯","id":"ddc4997f-ca41-46ef-9d82-81393c836a4f","originalAuthorName":"郭志凯"},{"authorName":"李龙飞","id":"231ce270-6090-4afc-9a30-59afa0c13ab7","originalAuthorName":"李龙飞"},{"authorName":"杨王玥","id":"ad7d50b6-a80e-497b-9f60-fc43111f30a1","originalAuthorName":"杨王玥"},{"authorName":"孙祖庆","id":"71a2fa1d-0ce1-4a86-b7d9-f32c59069b11","originalAuthorName":"孙祖庆"}],"doi":"","fpage":"144","id":"452f84da-76b1-492a-ae94-3f0b492e2787","issue":"7","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"c8c85332-797d-48be-a3be-10cc417a72c4","keyword":"高锰TRIP钢","originalKeyword":"高锰TRIP钢"},{"id":"c88d9535-d6d4-4bd5-8641-52309d0496e5","keyword":"马氏体温变形","originalKeyword":"马氏体温变形"},{"id":"8d5e3ffb-3a8e-46c5-8e8d-f2b15e23eeda","keyword":"C含量","originalKeyword":"C含量"},{"id":"65b67938-b908-4bea-8694-54c5ab9f3400","keyword":"残留奥氏体","originalKeyword":"残留奥氏体"},{"id":"f1f1f0e3-4c14-4cf1-a5bb-9669aa8f42d1","keyword":"力学性能","originalKeyword":"力学性能"}],"language":"zh","publisherId":"jsrclxb201507024","title":"C含量对基于马氏体温变形的高锰TRIP钢的影响","volume":"36","year":"2015"},{"abstractinfo":"为了研究不同B含量对马氏体耐热钢的微观组织和力学性能的影响,制备了B含量分别为0.012％、0.02％和0.03％的样件,讨论了不同B含量对基体中BN相形貌的影响机制.结果表明:随着B含量的增加,基体中BN相尺寸变大,0.03％B试样中BN相尺寸达到5um左右;0.012％B试样的抗拉和屈服强度最高;0.012％B试样断口韧窝中BN相为内部碎裂的块状,0.03％B试样中BN相出现薄片层叠堆积球状形态,是由于最初形成BN相的晶核以六方结构形式生长,达到临界尺寸后以B含量较高一侧局部优先生长方式生长,所以提高B含量增大了球形BN的极限尺寸.","authors":[{"authorName":"马煜林","id":"e4c0ba9b-3824-4c2e-9411-4d5bc4d96568","originalAuthorName":"马煜林"},{"authorName":"刘越","id":"1d31dd75-27ea-4805-a07d-70a38770acea","originalAuthorName":"刘越"},{"authorName":"张莉萍","id":"3a2dc8d1-61e4-4652-af89-bafbba6a37a5","originalAuthorName":"张莉萍"},{"authorName":"周玲","id":"05f3fca2-db91-48b1-9c90-4b2f96c040c5","originalAuthorName":"周玲"},{"authorName":"刘春明","id":"7cd37ad7-7648-4312-b17d-a0ec3f7ffa08","originalAuthorName":"刘春明"}],"doi":"10.11901/1005.3093.2016.057","fpage":"345","id":"8c68d37c-1342-4351-9078-82b697ad1967","issue":"5","journal":{"abbrevTitle":"CLYJXB","coverImgSrc":"journal/img/cover/CLYJXB.jpg","id":"16","issnPpub":"1005-3093","publisherId":"CLYJXB","title":"材料研究学报"},"keywords":[{"id":"4253bd1d-bf39-4ec4-b11e-73aedfd68125","keyword":"金属材料","originalKeyword":"金属材料"},{"id":"2b1de595-cdc0-4d40-a031-420813bd734c","keyword":"BN相","originalKeyword":"BN相"},{"id":"faa1a45b-cbd6-4710-8387-6a9dbca3ff8a","keyword":"B含量","originalKeyword":"B含量"},{"id":"fd4cd256-b827-4916-ac4d-187ebaae7abf","keyword":"马氏体耐热钢","originalKeyword":"马氏体耐热钢"}],"language":"zh","publisherId":"clyjxb201705004","title":"B含量对马氏体耐热钢中BN相形态及性能的影响","volume":"31","year":"2017"},{"abstractinfo":"用电阻法、光学显微镜和透射电镜研究了Mn含量对Cu-Al-Zn-Mn-Ni合金的相变点、马氏体形态和亚结构以及形状记忆效应的影响.结果表明:Mn含量增高导致相变温度显著降低,弹性马氏体相变温度范围变宽,并使马氏体形态由平行排列的长条状向自协作形态不断完善,马氏体亚结构由孪晶型向层错型过渡.马氏体的自协作完善程度和变体大小及淬火空位对合金的形状记忆效应有显著影响.","authors":[{"authorName":"赵连城","id":"86d81131-c9ed-4ee5-897a-69e3de075096","originalAuthorName":"赵连城"},{"authorName":"杨建华","id":"8c8031a9-e78b-4e6e-ae52-55814f400d06","originalAuthorName":"杨建华"}],"categoryName":"|","doi":"","fpage":"8","id":"756dec3a-bf1a-4c1c-8203-fe758a3621d5","issue":"4","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[],"language":"zh","publisherId":"0412-1961_1985_4_12","title":"Mn含量对Cu-Al-Zn-Mn-Ni合金弹性马氏体相变和形状记忆效应的影响","volume":"21","year":"1985"},{"abstractinfo":"通过优化钼和镍元素的含量,研制了一种焊接工艺优良的马氏体不锈钢硬面药芯焊丝,并采用埋弧焊堆焊方法在Q235钢基体上制备了堆焊层,研究了钼、镍含量对堆焊层组织、硬度和高温耐磨性能的影响.结果表明:堆焊层显微组织均由马氏体、残余奥氏体、碳化物组成;添加钼和镍元素后能够提高堆焊层的硬度和高温耐磨性能;且当钼、镍的质量分数均为2％时,得到的堆焊层的硬度和高温耐磨性能均最好,硬度为47.8 HRC,磨损质量损失为3.6 mg.","authors":[{"authorName":"吕彦","id":"0e0e197d-fe2e-4d8d-83c5-b516a5f0a4ca","originalAuthorName":"吕彦"},{"authorName":"余圣甫","id":"a0b9825a-2021-47c9-bdb7-59321b00273d","originalAuthorName":"余圣甫"},{"authorName":"行舒乐","id":"21424a21-b8a8-4235-95df-1338d38c9f2b","originalAuthorName":"行舒乐"},{"authorName":"刘雨龙","id":"80620b8e-f412-4a7d-890b-f5446d4714c8","originalAuthorName":"刘雨龙"},{"authorName":"王乐虎","id":"f49f6525-fb9e-42a0-9f76-5fe77f6cdbb0","originalAuthorName":"王乐虎"}],"doi":"","fpage":"29","id":"a56f3e91-2f46-44b2-80b2-002db34239c4","issue":"9","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"aaeab6a3-8a3a-4baa-9c15-6d67b617a70c","keyword":"马氏体不锈钢","originalKeyword":"马氏体不锈钢"},{"id":"1c6659d2-eec3-4f00-adfb-f0105072288e","keyword":"埋弧焊","originalKeyword":"埋弧焊"},{"id":"d45e2fb5-2022-4c48-aa92-634abf473a03","keyword":"硬度","originalKeyword":"硬度"},{"id":"e50f70e9-8821-44a1-96e5-1b75221892ff","keyword":"高温耐磨性能","originalKeyword":"高温耐磨性能"}],"language":"zh","publisherId":"jxgccl201309008","title":"钼、镍含量对马氏体不锈钢硬面药芯焊丝堆焊层组织和性能的影响","volume":"37","year":"2013"},{"abstractinfo":"采用扫描电镜、光学显微镜、洛氏硬度计、拉伸试验机等研究了两相区淬火时间和温度对高马氏体含量双相钢显微组织和力学性能的影响.结果表明:在785 ℃淬火时,随保温时间的延长,双相组织中马氏体体积分数增加,铁素体体积分数减少,碳化物数量减少并发生固溶扩散,试验钢的硬度、屈服强度、抗拉强度均呈上升趋势,伸长率和断面收缩率均呈下降趋势;在785~830 ℃保温30 min淬火后,随温度升高,淬火组织中铁素体体积分数减少,马氏体体积分数增加,碳化物数量减少,当淬火温度为815 ℃时,组织基本全部为马氏体,试验钢的硬度、抗拉强度均呈上升趋势,伸长率和断面收缩率均呈下降趋势,屈服强度则先上升后略有下降.","authors":[{"authorName":"李勇","id":"9079e92d-befb-4916-9a2d-0181d15fed81","originalAuthorName":"李勇"},{"authorName":"雷文华","id":"4c27f5db-3e5f-4720-b3c1-b6a589fe6ff1","originalAuthorName":"雷文华"},{"authorName":"周毅","id":"64458522-6cdf-4f4f-a6b4-fafedc213496","originalAuthorName":"周毅"}],"doi":"10.11973/jxgccl201705005","fpage":"22","id":"b44de093-ce10-4a4a-814e-428b2d29ae46","issue":"5","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"08982d26-f037-46ef-9478-5c8265ccf903","keyword":"双相钢","originalKeyword":"双相钢"},{"id":"76cda0b2-72c3-4d2b-ac6d-0aec3fa8db15","keyword":"力学性能","originalKeyword":"力学性能"},{"id":"fe075806-11a2-494f-bd32-c91c60f643d5","keyword":"显微组织","originalKeyword":"显微组织"}],"language":"zh","publisherId":"jxgccl201705005","title":"不同工艺两相区淬火后高马氏体含量双相钢的显微组织与力学性能","volume":"41","year":"2017"}],"totalpage":2979,"totalrecord":29788}