建立了马铃薯、洋葱、大蒜中马来酰肼(MH)的高效离子排斥色谱(HPIEC)检测方法.样品经提取、净化、过滤后进行色谱分析,以3 mmol/L 甲酸水溶液-乙腈(70:30, v/v)为流动相,流速0.8 mL/min,采用Ionpac ICE-AS1(250 mm×9 mm)HPIEC色谱柱分离,紫外检测波长205 nm,外标法定量.结果表明,MH的线性范围为0.006~1.0 mg/L,相关系数为 0.9999,回收率为91% ~103% ,相对标准偏差(RSD)均小于3% ,检出限为0.002 mg/L (S/N=3).该方法灵敏度高,前处理简便,可用于马铃薯、洋葱、大蒜中MH的检测.
参考文献
[1] | Marcano L,Carruyo I,Del C A,et al.Envir Res,2004,94(2):221 |
[2] | AOAC,Official Method 963.24 |
[3] | Pei M L,Jiang Z H,Wang Q S,et al.Journal of Instrumental Analysis (裴明黎,蒋振辉,王秋霜,等.分析测试学报),2009,28(5):611 |
[4] | John L D,Barnes K A,Wilkinson K,et al.J Chromatogr A,1996,750(1/2):391 |
[5] | Yang S S.J Chromatogr A,1992,595(1/2):346 |
[6] | Renaud J M,Keller I,Vuillaume G.J Chromatogr A,1992,604(2/3):243 |
[7] | Tang J H,Li R F.Journal of Kunming Medical College (汤健华,李儒发.昆明医学院学报),1990,11(1):38 |
[8] | Fang Y J,Yan S L,Ning B A,et al.Biosens Bioelectron,2009,24(8):2323 |
[9] | Li L,Zhou M,Fang Y J,et al.Food Science and Technology (李莉,周敏,房彦军,等.食品科技),2008,3:223 |
[10] | Alberto S A,Esperanza B,Manuel C,et al.Talanta,2007,71(1):430 |
[11] | Mou S F,Liu K N,Ding X J.Ion Chromatographic Method and Its Application.2nd ed.Beijing:Chemical Industry Press (牟世芬,刘克纳,丁晓静.离子色谱方法及应用.2版.北京:化学工业出版社),2005 |
[12] | Mori M,Iwata T,Satori T,et al.J Chromatogr A,2008,1213(2):125 |
[13] | Dias J C,Suzuki E,Cibele L,et al.J Pharm B,2009,49(4):1128 |
[14] | Geng Z M,Jiang R,Chen M.J Food Comp,2008,21(2):178 |
[15] | Nakatani N,Kozaki D,Masuda W,et al.Anal Chim Acta,2008,619(1):110 |
[16] | Iwata T,Mori M,Itabashi H,et al.Talanta,2009,79(4):1026 |
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