以聚乙烯吡咯烷酮(PVP)为分散剂,偶氮二异丁腈(AIBN)为引发剂,乙醇/水混合溶剂为分散介质,用分散聚合方法制备出微米级甲基丙烯酸甲酯-苯乙烯共聚物微球.研究了分散介质组成、单体质量比、分散剂用量、反应温度等反应条件对聚合产物粒径及粒径分布的影响.并用红外光谱对产物结构进行了表征.
参考文献
[1] | Unsal E.;Camli ST.;Senel S.;Tuncel A. .Chromatographic performance of monodisperse-macroporous particles produced by "modified seeded polymerization" I: Effect of monomer/seed latex ratio[J].Journal of Applied Polymer Science,2004(1):607-618. |
[2] | Fang-Cheng Huang;Cheng-Ho Ke;Chen-Yu Kao;Wen-Chien Lee .Preparation and Application of Partially Porous Poly(Styrene-Divinylbenzene) Particles for Lipase Immobilization[J].Journal of Applied Polymer Science,2001(1):39-46. |
[3] | Guang-Hui Ma;Masatoshi Nagai;Shinzo Omi .Study on Preparation of Monodispersed Poly(styrene-co-N-dimethylaminoethyl methacrylate) Composite Microspheres by SPG (Shirasu Porous Glaa) Emulsification Technique[J].Journal of Applied Polymer Science,2001(13):2408-2424. |
[4] | 张凯,雷毅,王宇光,江璐霞.单分散聚苯乙烯微球的制备及影响因素研究[J].功能高分子学报,2002(02):189-193. |
[5] | 胡杰,刘百玲,汪地强.乙醇-水介质中单分散聚甲基丙烯酸甲酯微球的制备[J].高分子学报,2003(04):540-543. |
[6] | 张洪涛,江兵兵,黄锦霞.非水分散聚合制备交联聚苯乙烯微球--单体浓度对聚合速率和粒子大小的影响[J].高分子材料科学与工程,2002(04):57-61. |
[7] | 陆馨,辛忠,杨海.分散聚合法制备甲基丙烯酸甲酯-苯乙烯共聚物微球[J].功能高分子学报,2005(02):310-315. |
[8] | Hong-Tao Zhang;Xiao-Ya Yuan;Jin-Xia Huang .Study of kinetics and nucleation mechanism of dispersion copolymerization of methyl methacrylate and acrylic acid[J].Reactive & functional polymers,2004(issue 1):23-31. |
[9] | 李雅洁,阚成友,黄世明,刘德山.微米级单分散苯乙烯-甲基丙烯酸共聚物微球的制备[J].北京化工大学学报(自然科学版),2005(04):60-63,69. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%