利用光学显微镜和扫描电镜对Ni3Al基单晶合金IC21的铸态组织和不同热处理制度后的组织进行了观察,研究了固溶温度和时效温度对合金热处理组织的影响.研究结果表明,IC21单晶合金的铸态组织由γ’相、γ相以及枝晶间的白色块状析出相组成,枝晶干上γ’相尺寸比枝晶间的γ’相尺寸大.IC21单晶合金的初熔温度约为1345℃,热处理窗口约为65℃.枝晶间γ’相的溶解温度低于枝晶干γ’相的溶解温度.固溶温度越高,时效处理后γ’相的尺寸越均匀.一级时效处理温度对γ’相的尺寸、形态和数量有明显影响.随着一级时效温度的增加,γ’相的体积分数和尺寸增加,形状由类球状向立方状再向长条状转变.1320 ℃/10 h/aac+ 1060℃/2 h/ac +870℃/32 h/ac热处理后可使合金获得γ’相尺寸和分布均匀且立方度高的优良组织.
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