以金属锑为阳极,钛、不锈钢等导电材料为阴极,HCl溶液或含NaCl的HCl溶液为电解液,在单室电解槽中采用电化学牺牲阳极法溶解金属锑,制备了粒径为10 nm的超细金属锑,该金属锑与盐酸溶液反应生成了氯化锑溶液,再经水解得到了氯氧化锑Sb4O5Cl2.产品通过X射线粉末衍射(XRD)、扫描电子显微镜(SEM)和透射电镜(TEM)测试技术进行了表征.
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