采用机械合金化方法制备出了Mg55Ni35 Si10非晶合金粉体,采用XRD、HRTEM、FESEM以及DSC试验,对所得粉末的微结构、相组成、颗粒形貌及热稳定性进行了表征.结果表明:对于配比为Mg55Ni35Si10的粉末,经约68 h的球磨可以获得完全非晶态的合金粉末,其晶化温度约为420℃,证明该材料具有相对较高的热稳定性.
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