本文报道了用坩埚下降法生长Fe:LiNbO3晶体的新工艺.通过选择合适的原料配比、控制固液界面的温度梯度为20～40℃/cm及晶体生长速度0.8～1.5mm/h,生长出掺杂0.04mol%Fe2O3的无宏观缺陷LiNbO3单晶.XRD图谱和DTA曲线用来表征所得晶体,并且测定了从晶体下部到上部的紫外可见吸收光谱.结果表明:沿生长方向,晶胞参数a、c增大,熔点降低,晶体中的Fe2+浓度呈增加趋势,作者分析了造成成分不均匀分布的原因.
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