欢迎登录材料期刊网

材料期刊网

高级检索

本文采用KOH:H2O=3:20~1:25(质量比)的KOH溶液,对Si基外延GaN进行湿法腐蚀.腐蚀后用扫描电子显微镜(SEM)观察,GaN面出现了六角腐蚀坑,它是外延层中的位错露头,密度约108/cm2.腐蚀坑的密度随腐蚀时间延长而增加,说明GaN外延生长过程中位错密度是逐渐降低的,部分位错因相互作用而终止于GaN体内.观察缺陷腐蚀形貌还发现,接近裂纹处腐蚀坑的密度要高于远离裂纹处腐蚀坑的密度,围绕裂纹有许多由裂纹引起的位错.腐蚀坑的密度可以很好地反映GaN晶体的质量.晶体质量较差的GaN片,腐蚀后其六角腐蚀坑的密度高.

参考文献

[1] Y. Chen;R. Schneider;S. Y. Wang .Dislocation reduction in GaN thin films via lateral overgrowth from trenches[J].Applied physics letters,1999(14):2062-2063.
[2] Xie S Y;Zheng Y D;Chen P et al.Optical Properties of Mg-implanted GaN[J].Applied Physics A,2002,75:363.
[3] Halsall M P;Harmer P;Parbrook P J et al.Raman Scattering and Absorption Study of the High-pressure Wurtzite to Rocksalt Phase Transition of GaN[J].Physical Review B,2004,69:235207.
[4] U. Bangert;A. Gutierrez-Sosa;A. J. Harvey;C. J. Fall;R. Jones .Electron energy loss studies of dislocations in GaN thin films[J].Journal of Applied Physics,2003(5):2728-2735.
[5] N. V. Joshi;A. Cros;A. Cantarero;H. Medina;O. Ambacher;M. Stutzmann .Role of defect centers in recombination processes in GaN monocrystals[J].Applied physics letters,2002(16):2824-2826.
[6] Akira Sakai;Haruo Sunakawa;Akira Usui .Transmission electron microscopy of defects in GaN films formed by epitaxial lateral overgrowth[J].Applied physics letters,1998(1/6):481-483.
[7] Wang T.;Naoi N.;Sakai S.;Morishima Y. .A new method for a great reduction of dislocation density in a GaN layer grown on a sapphire substrate[J].Journal of Crystal Growth,2000(1/2):188-192.
[8] Rotter T;Aderhald J;Mistele D et al.Smooth GaN Surfaces by Photoinduced Electro-chemical Etching[J].Materials Science and Engineering B,1999,59:350.
[9] J. L. Weyher;F. D. Tichelaar;H. W. Zandbergen;L. Macht;P. R. Hageman .Selective photoetching and transmission electron microscopy studies of defects in heteroepitaxial GaN[J].Journal of Applied Physics,2001(12):6105-6109.
[10] P. Visconti;K. M. Jones;M. A. Reshchikov .Dislocation density in GaN determined by photoelectrochemical and hot-wet etching[J].Applied physics letters,2000(22):3532-3534.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%