采用NaCl-KCl熔盐法合成了生长各向异性的片状SrBi4Ti4O15粉体,用XRD分析了粉体相的结构,用SEM观察了粉体的微观形貌,讨论了不同预烧温度对合成物结构和微观形貌的影响.与固相法相比,熔盐法合成的粉体具有(00l)择优生长的优点.在850~1050℃之间,合成粉体的片状结构趋于明显,粉体生长各向异性随温度的升高呈现出先增加后减小的趋势,各向异性明显的SrBi4Ti4O15粉体的最佳合成温度为900~1000℃.
参考文献
[1] | Macquart R et al.Structural Studies of Cation Disorder in the Ferroelectric Oxide SrBi2Ta2O9[J].Ferroelectrics,2000,248(02):27. |
[2] | Eiichiro Fokuchi;Toshio Kmura .Effect of Potassium Concentration on the Grain Orientation in Bismuth Solidium Potassium Titanate[J].European Ceramic Society,2002,85(06):14612. |
[3] | Thirumal M.;Ganguli AK.;Jain P. .Molten salt synthesis of complex perovskite-related dielectric oxides[J].Materials Chemistry and Physics,2001(1):7-11. |
[4] | Yanmei Kan;Xihai Jin;Peiling Wang;Yongxiang Li;Yi-Bing Cheng;Dongsheng Yang .Anisotropic grain growth of Bi_4Ti_3O_(12) in molten salt fluxes[J].Materials Research Bulletin: An International Journal Reporting Research on Crystal Growth and Materials Preparation and Characterization,2003(4):567-576. |
[5] | 朱信华;朱滔;朱健民 等.层状钙钛矿结构SrBi2Ta2O9铁电薄膜的微结构研究[J].人工晶体学报,2000,29(05):257. |
[6] | 赵成,朱骏,陈小兵.La、V掺杂对SrBi4Ti4O15性能影响对比研究[J].功能材料,2004(05):610-612. |
[7] | 郝华,刘韩星,马麟,欧阳世翕.SrBi4Ti4O15铁电陶瓷的制备工艺研究[J].现代技术陶瓷,2004(02):3-5. |
[8] | Kimura T;Yamaguchi T .Morphology Control of Electronic Ceramic Powders by Molten Salt Synthesis[J].Ceramic Powder Science,1987,21(40):177. |
[9] | Kimura T;Yamaguchi T .Morphology of Bi2WO6 Powders Obtained in the Presence of Fused Salts[J].Journal of Materials Science,1982,17(30):1869. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%