采用沉淀法并用柠檬酸作分散剂合成HAP超细粉体.采用XRD,SEM等实验方法研究了柠檬酸的加入对产物粒径大小、团聚的影响,并对实验中的有关工艺参数进行了研究.结果表明,在用柠檬酸作分散剂的条件下,产品的粒径和分散性能得到改善.
参考文献
| [1] | Suchanek W.;Yoshimura M. .Processing and properties of hydroxyapatite-based biomaterials for use as hard tissue replacement implants [Review][J].Journal of Materials Research,1998(1):94-117. |
| [2] | 吕奎龙,孟祥才,李星逸,藤利群.纳米羟基磷灰石制备的研究进展[J].佳木斯大学学报(自然科学版),2002(04):384-388. |
| [3] | Li Y B;Wei J;Klein C P A T et al.Preparation and characterization of nanograde osteoapatite-like rod crystals[J].Journal of Material in Medicine,1994,5(05):252-257. |
| [4] | 王友法,闫玉华,梁飞,张宏泉.水热条件下针状羟基磷灰石单晶体的均相合成[J].硅酸盐通报,2001(02):30-34. |
| [5] | Suchanek W.;Yoshimura M. .Processing and properties of hydroxyapatite-based biomaterials for use as hard tissue replacement implants [Review][J].Journal of Materials Research,1998(1):94-117. |
| [6] | Liu Changsheng;Huang Yue;Shen Wei et al.Kinetics of hydroxyapatite precipitation at pH 10-11[J].Biomaterials,2001,22:301-306. |
| [7] | Tas AC .Synthesis of biomimetic Ca-hydroxyapatite powders at 37 degrees C in synthetic body fluids.[J].Biomaterials,2000(14):1429-1438. |
| [8] | Chai CS;Gross KA;Ben-Nissan B .Critical ageing of hydroxyapatite sol-gel solutions.[J].Biomaterials,1998(24):2291-2296. |
| [9] | 刘羽;钟康年;胡文云 .溶胶凝胶法合成条件与羟基磷灰石特征的关系[J].材料科学与工程,1997,15(01):63-65. |
| [10] | Deptula S;Lada W;Olczak T et al.Preparation of spherical powders of hydroxyapatite by sol-gel process[J].Journal of Non-Crystalline Solids,1992,147:537-541. |
| [11] | Lim G K;Wang J;Ng S C.Processing of fine hydroxyapatite powders via microemulsion route[J].Materials Letters,1996(28):431-436. |
| [12] | Lim GK.;Ng SC.;Chew CH.;Gan LM.;Wang J. .PROCESSING OF HYDROXYAPATITE VIA MICROEMULSION AND EMULSION ROUTES[J].Biomaterials,1997(21):1433-1439. |
| [13] | Vallet-Regf M;Gutienez-Rios M T;Alonso M P et al.Hydroxyapatite particles synthesized by pyrolysis of an aerosol[J].Solid-state chemistry,1994,112:58-64. |
| [14] | Moreno E C;Varughese K .Crystal growth of calcium apatite from dilute solutions[J].Journal of Materials Science,1987,22:247-250. |
| [15] | Moreno E C;Varughese K .Crystal growth of calcium apatite from dilute solutions[J].Journal of Crystal Growth,1981,53:20-30. |
| [16] | 韩颖超,王欣宇,李世普.纳米级磷灰石粉末制备工艺进展[J].硅酸盐通报,2002(03):27-29. |
| [17] | 张德正;王保锋;纪元玉 等.医用羟基磷灰石的制备与应用[J].中国陶瓷,1998,34(06):24-26. |
| [18] | 李宝娥.羟基磷灰石超细粉体的制备[J].陶瓷,2004(01):23-26. |
| [19] | Kaliszewski M S;Heuer A H .Alcohol Interaction with zirconia powders[J].Journal of the American Ceramic Society,1990,73:1504-1507. |
| [20] | Wen S L .Human enamel structrue studied by high resolution electron microscopy[J].Electron Microscopy Review,1989,2:1-6. |
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