采用电刷镀的方法,通过在刷镀溶液中加入不同类型及含量的表面活性剂,在铁基体上制备出了纳米晶镍镀层.通过原子力显微镜、扫描电子显微镜观察,分析纳米晶镍镀层的二维和三维表面形貌.利用X-射线衍射仪,估算纳米晶镍镀层的晶粒平均尺寸.
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