采用微波辅助加热的方法从三乙醇胺出发合成聚酰胺-胺树形分子核.结合IR和1H NMR表征手段,证明合成产物与目标分子结构一致.通过单因素对比实验研究了微波功率与产率之间的关系,并综合实验数据确定出了合适的微波反应条件.微波反应30,60,50min,中间产物三腈、三酯及目标产物三胺的产率分别达到72.5%,73.8%,69.3%.
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