为优化Al2O3层状复合材料的制备工艺及力学性能,选用不同初始粉体为原料制备了系列Al2O3/Al2O3-ZrO2(3Y)层状复合材料.借助X射线衍射、冷场发射扫描电镜和万能试验机等手段,系统考察了粉体结构和形貌对层状复合材料显微结构和性能的影响.结果表明:初始粉体的颗粒尺寸及尺寸分布会显著影响层状复合材料的显微结构及力学性能,以球磨微-纳米复合粉体为原料制备的层状复合材料具有最佳的力学性能,其抗弯强度和断裂功分别可达740MPa及3892J ·m-2.同时,材料具有较高的层间结合强度,平行于层方向的抗弯强度高达436MPa.
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