用扫描电子显微镜(SEM)和电子背散射衍射(EBSD)技术研究了5%冷变形316不锈钢经1100℃不同时间退火样品的晶界特征分布(GBCD).结果表明:低ΣCSL(Σ≤29)晶界比例的提高是在再结晶过程中实现的.在退火40 min时再结晶完成,低ΣCSL晶界比例达到80%,其中Σ3晶界比例占总的低ΣCSL晶界80%左右,晶界特征分布得到优化;尺寸较大形状不规则的晶粒团簇(grain-clusters)形成,每个晶粒团簇内部存在大量孪晶界、多重孪晶界和特殊的三叉晶界节点.部分再结晶状态样品的显微组织特点和晶粒团簇内部孪晶链的分析表明再结晶过程中多重孪晶的发展是提高316不锈钢低ΣCSL晶界比例的关键.
参考文献
[1] | 毛林彬;杨治全;单润华.国产快堆燃料元件包壳材料316不锈钢的中子辐照效应[M].中国核动力研究设计院,2007:10. |
[2] | 罗宏,龚敏.奥氏体不锈钢的晶间腐蚀[J].腐蚀科学与防护技术,2006(05):357-360. |
[3] | Winning M .Grain Boundary Engineering by Application of Mechanical Stresses[J].Scripta Materialia,2006,54:987. |
[4] | Kumar M;Schwartz A J;King W E .Microstructural Evolution during Grain Boundary Engineering of Low to Medium Stacking Fault Energy fcc Materials[J].Acta Materialia,2002,50:2599. |
[5] | Lin P;Palumbo G;Erb U;Aust K T .Influence of Grain Boundary Character Distribution on Sensitization and Intergranular Corrosion of Alloy 600[J].Scripta Metallurgica et Materialia,1995,9(33):1387. |
[6] | Xia SA;Zhou BX;Chen WJ .Effect of single-step strain and annealing on grain boundary character distribution and intergranular corrosion in Alloy 690[J].Journal of Materials Science,2008(9):2990-3000. |
[7] | 夏爽,周邦新,陈文觉,王卫国.高温退火过程中铅合金晶界特征分布的演化[J].金属学报,2006(02):129-133. |
[8] | Randle V .Twinning-related Grain Boundary Engineering[J].Acta Materialia,2004,52:4067. |
[9] | Song K H;Chun Y B;Hwang S K .Direct Observation of Annealing Twin Formation in a Pb-base Alloy[J].Materials Science and Engineering,2007,A454-455:629. |
[10] | VALERIE RANDLE;HELEN DAVIES .Evolution of Microstructure and Properties in Alpha-Brass after Iterative Processing[J].Metallurgical and Materials Transactions, A. Physical Metallurgy and Materials Science,2002(6):1853-1857. |
[11] | Michiuchi M;Kokawa H;Wang Z J et al.Twin-induced Grain Boundary Engineering for 316 Austenitic Stainless Steel[J].Acta Materialia,2006,54:517. |
[12] | Yang, S;Wang, ZJ;Kokawa, H;Sato, YS .Reassessment of the effects of laser surface melting on IGC of SUS 304[J].Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing,2008(1/2):112-119. |
[13] | 丁霞,陈文觉.316不锈钢的晶界分布研究[J].上海金属,2006(04):14-17. |
[14] | Owen G;Randle V .On the Role of Iterative Processing in Grain Boundary Engineering[J].Scripta Materialia,2006,55:959. |
[15] | Randle V .Mechanism of Twinning-induced Grain Boundary Engineering in Low Stacking-fault Energy Materials[J].Acta Materialia,1999,47(15):4187. |
[16] | 方晓英,王卫国,周邦新.金属材料晶界特征分布(GBCD)优化研究进展[J].稀有金属材料与工程,2007(08):1500-1504. |
[17] | Palumbo G;Aust K T;Lehockey E M et al.On a More Restrictive Geometric Criterion for'Special'CSL Grain Boundaries[J].Scripta Materialia,1998,38(05):1685. |
[18] | Berger A;Wilbrandt P J;Ernst F .On the Generation of New Orientations during Recrystallization:Recent Results on the Recrystallization of Tensile-deformed fcc Single Crystals[J].Progress in Materials Science,1988,32:1. |
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