欢迎登录材料期刊网

材料期刊网

高级检索

利用热蒸发法成功制备出了两种氧化锡纳米结构.利用X射线衍射法、拉曼光谱、扫描电子显微镜和透射电子显微镜对两种纳米结构的晶格结构和表面形貌做了详细分析,结果表明所制纳米结构为金红石型氧化锡晶体结构,氧化锡纳米结构的形貌与实验中所用的源材料有着很大的关系.以氧化锡和碳粉的混合物为源,制备出的纳米线长且直,直径在50~200nm之间,以氧化亚锡和碳粉为源,制备出的纳米结构短且多弯折,直径在150nm左右.研究了所制氧化锡纳米材料的室温光致发光性能,发光峰位于590、630和677nm处.

参考文献

[1] 徐红燕,陈兴桥,于庆江,曹丙强.基于正交试验的La_2O_3掺杂SnO_2气敏传感器的研究[J].功能材料,2011(10):1790-1794.
[2] Rezan Demir-Cakan;Yong-Sheng Hu;Markus Antonietti .Facile One-Pot Synthesis of Mesoporous SnO2 Microspheres via Nanoparticles Assembly and Lithium Storage Properties[J].Chemistry of Materials: A Publication of the American Chemistry Society,2008(4):1227-1229.
[3] Jiang Lingyan;Wu Xinglong;Guo Yuguo et al.SnO2-based hierarchical nanomicrostructure:facile synthesis and their applications in gas sensors and lithium-ion batteries[J].The Journal of Physical Chemistry C,2009,113(32):14213-14219.
[4] 王灵婕,林金阳,苏艺菁,游玉香,郭太良.衬底电极对SnO_2纳米材料场发射性能的影响[J].功能材料,2011(08):1380-1382.
[5] Jun Pan;Xuefeng Song;Jun Zhang .Switchable Wettability in SnO2 Nanowires and SnO2@SnO2 Heterostructures[J].The journal of physical chemistry, C. Nanomaterials and interfaces,2011(45):22225-22231.
[6] Bazargan S;Leung K T .Catalyst-assisted pulsed laser deposition of one-dimensional single-crystalline nanostructures of tin (Ⅳ) oxide:interplay of VS and VLS growth mechanisms at low temperature[J].The Journal of Physical Chemistry C,2012,116(09):5427-5434.
[7] Qin LP;Xu JQ;Dong XW;Pan QY;Cheng ZX;Xiang Q;Li F .The template-free synthesis of square-shaped SnO2 nanowires: the temperature effect and acetone gas sensors[J].Nanotechnology,2008(18):185705-1-185705-8-0.
[8] Zu Rong Dai;Zheng Wei Pan;Zhong L. Wang .Novel Nanostructures of Functional Oxides Synthesized by Thermal Evaporation[J].Advanced functional materials,2003(1):9-24.
[9] Wang JX.;Liu DF.;Yan XQ.;Yuan HJ.;Ci LJ.;Zhou ZP.;Gao Y.;Song L. Liu LF.;Zhou WY.;Wang G.;Xie SS. .Growth of SnO2 nanowires with uniform branched structures[J].Solid State Communications,2004(1/2):89-94.
[10] Chen YJ;Li QH;Liang YX;Wang TH;Zhao Q;Yu DP .Field-emission from long SnO2 nanobelt arrays[J].Applied physics letters,2004(23):5682-5684.
[11] Huang LS;Pu L;Shi Y;Zhang R;Gu BX;Du YW;Wright S .Controlled growth of well-faceted zigzag tin oxide mesostructures[J].Applied physics letters,2005(16):3124-1-3124-3-0.
[12] Qingyan Wang;Ke Yu;Feng Xu .Synthesis and field emission of two kinds of hierarchical SnO_2 nanostructures[J].Solid State Communications,2007(4/5):260-263.
[13] Porto S P S;Fleury P A;Damen T C .Raman spectra of TiO2,MgF2,ZnF2,FeF2 and MnF2[J].Physical Review,1967,154(02):522-526.
[14] Sato T;Asari T .Temperature dependence of the line width of the first order Raman spectrum for SnO2 crystal[J].Journal of the Physical Society of Japan,1995,64(04):1193-1199.
[15] Abello L.;Gaskov A.;Koudryavtseva S.;Lucazeau G. Roumyantseva M.;Bochu B. .Structural characterization of nanocrystalline SnO2 by X-ray and Raman spectroscopy[J].International Journal of Quantum Chemistry,1998(1):78-85.
[16] Wu J;Yu K;Li LJ;Xu JW;Shang DJ;Xu YE;Zhu ZQ .Controllable synthesis and field emission properties of SnO2 zigzag nanobelts[J].Journal of Physics, D. Applied Physics: A Europhysics Journal,2008(18):185302-1-185302-7-0.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%