利用单铜辊甩带法制备Fe40Ni38Mo4B(18－x)Six(x＝0,2,4,6,8,10和12)非晶合金带材,并用X射线衍射仪(XRD)、差示扫描量热仪(DSC)、振动样品磁强计(VSM)以及精密磁性器件分析仪研究Si元素对FeNiMoBSi合金带材的非晶形成能力和软磁性能影响.结果表明,随着Si元素的添加,合金带材的矫顽力Hc先减小后增大,并在x＝4时最小为5．8A/m；Fe40Ni38Mo4B14Si4合金带材在405℃保温10min热处理后获得较高的饱和磁化强度为112．63A?m2/kg,在345℃保温10min热处理后获得较低的矫顽力为7．0A/m.
Amorphous Fe40 Ni38 Mo4B18 (x =0,2,4,6,8,10,12)alloy ribbons were prepared by the single roller melt-spinning method.The effect of Si addition on glass forming ability and magnetic properties of FeNiMoB al-loy ribbons was investigated by X-ray diffraction(XRD),differential scanning calorimeter (DSC)and vibrating sample magnetometer (VSM)and precision magnetics analyzer.It was found that as the Si element content add-ed,the coercovity showed a decreasing trend firstly and increased again,Fe40 Ni38 Mo4B14 Si4 amorphous alloy has a lower Hc of 5.8 A/m.It was found that Fe40 Ni38 Mo4B14 Si4 ribbon has the highest B s about 1 12.63 A ?m2/kg at annealed at 405 ℃ for 10 min and the lowest Hc about 7.0 A/m at annealed at 345 ℃ for 10 min.
参考文献
| [1] | Luborsky F E .Applications of amorphous alloys[J].IEEE Transactions on Magnagnetics,1978,14(5):1008-10121. |
| [2] | Li J. .Microstructure of nanostructured Fe40Ni38Mo4B18 alloy[J].Journal of Materials Science,1999(1):111-114. |
| [3] | Stoyanov PG.;Grimes CA. .A remote query magnetostrictive viscosity sensor[J].Sensors and Actuators, A. Physical,2000(1):8-14. |
| [4] | A.P. Srivastava;D. Srivastava;G.K. Dey .A study on microstructure, magnetic properties and kinetics of the nanocrystallization of Fe_(40)Ni_(38)B_(18)Mo_4 metglass[J].Journal of Magnetism and Magnetic Materials,2006(1):147-155. |
| [5] | Garcia, I;Iturriza, N;del Val, JJ;Grande, H;Pomposo, JA;Gonzalez, J .Magnetic force microscopy characterization of heat and current treated Fe40Ni38Mo4B18 amorphous ribbons[J].Journal of Magnetism and Magnetic Materials,2010(13):1822-1827. |
| [6] | Liang Cai;Gooneratne Chinthaka;Cha Dongkyu et al.Devolopment of FeNiMoB thin film materials for micro-fabricated magnetoelastics sensors[J].Journal of Applied Physics,2012,112(11):113912-113912-8. |
| [7] | Saiseng S;Winotai P;Nilpairuch S et al.Nancrystalliza-tion in amorphous Fe40 Ni40(Si+B)19 Mo1-2 ribbons[J].Journal of Magnetism and Magnetic Materials,2004,278:172-178. |
| [8] | Lu K;Wang J T .A micromechanism for crystallization of amorphous alloys I.An in situ TEM observation[J].Jour-nal of Crystal Growth,1991,112(2):525-530. |
| [9] | 陈木主,陈先朝,杨元政,谢致薇,江再勇.添加Ni对FeZrNbB合金的非晶形成能力与软磁性能的影响[J].功能材料,2013(18):2612-2615. |
| [10] | Fan, X.D.;Men, H.;Ma, A.B.;Shen, B.L. .Soft magnetic properties in Fe_(84-x)B_(10)C_6Cu_x nanocrystalline alloys[J].Journal of Magnetism and Magnetic Materials,2013(1):22-27. |
| [11] | Gong Weiyu;Ruan Jianzhong;Yuan Wangzhi et al.The influence of annealing on performance of magneto - a-coustic markers[J].Journal of Materials Science and En-gineering,2007,25(6):935-937. |
| [12] | Kai-Yuan He;Yu-Hua Zhao;Guo-Gang Li;Li-Zhi Cheng;Bo Wu;Man-Ling Sui;Wen-Zhi Chen .Studies of crystallization and soft magnetic properties of FeNiMoB(Si) alloys[J].Journal of Magnetism and Magnetic Materials,2007(1):34-39. |
| [13] | Kong F;Wang A;Fan X et al.High B s Fe(84-x)Si4 B4 P4 Cux(x =0-1.5)nanocrystalline allors with excel-lent magnetic softness[J].Journal of Applied Physics,2011,109(7):1-3. |
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