采用水热法制备了冰晶石型氟化物Na3FeF6,通过粉末X射线衍射、扫描电子显微镜、差热-热重分析等手段对化合物的性质进行了表征.该化合物空间群为单斜晶系.晶胞参数为a=5.513(A),b=5.728(A),c=7.964(A),并对其磁学性质进行了研究.
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