采用原位复合法制备导电聚苯胺磁性复合颗粒,借助FTIR、XRD、UV-Vis、TEM和VSM等分析手段研究了复合粒子的形貌、结构及其光、电和磁性能.结果表明:BaFe8(Ti0.5Mn0.5)4O19以约12 nm的粒径分散在聚苯胺基体中,聚苯胺与铁氧体之间存在化学键合作用,一定程度上减小了铁氧体纳米粒子的团聚;PANI/BaFe8(Ti0.5Mn0.5)4O19复合颗粒同时具有导电性和磁性能,其导电性随聚苯胺含量的增加而增强,而比饱和磁化强度随之下降;当聚苯胺含量为54.91%时,复合颗粒电磁学性能为He=92 kA/m,σs=11.54 Am2/kg,σr=4.97 Am2/kg,σ=13.1 S/m.
参考文献
[1] | 杨青林,宋延林,万梅香,江雷,徐文国,李前树.导电聚苯胺与Fe3O4磁性纳米颗粒复合物的合成与表征[J].高等学校化学学报,2002(06):1105-1109. |
[2] | Paul A. Kilmartin;Graham A. Wright .Photoelectrochemistry and spectroscopy of substituted polyanilines[J].Synthetic Metals,1999(3):145-156. |
[3] | Wu Q.;Qi Z.;Wang F.;Xue Z. .Synthesis and characterization of PAn/clay nanocomposite with extended chain conformation of polyaniline[J].Polymer: The International Journal for the Science and Technology of Polymers,2000(6):2029-2032. |
[4] | Ding L;WANG X;GREGORY R V .Thermal properties of cherrically synthesized polyaniline EBpowder[J].Synthetic Metals,1999,104(02):73-78. |
[5] | Dhanabalan A;MALMONGE J A;RIUL A J et al.Study on X-ray irradiation of composite polyaniline LB films[J].THIN SOLID FILMS,1998,327 -329:808-812. |
[6] | 刘先松,钟伟,姜洪英,顾本喜,都有为.纳米晶复合SrM永磁铁氧体的制备和交换耦合作用[J].中国粉体技术,2001(05):6-9. |
[7] | 魏建红,官建国,陈文怡,袁润章.聚苯胺/钛酸钡纳米复合粒子的制备与表征[J].物理化学学报,2002(07):653-656. |
[8] | 刘少琼,于黄中,黄河,熊予莹.TiO2纳米微粒对聚苯胺性能的影响[J].高等学校化学学报,2002(01):161-163. |
[9] | 孟凡君,茹淼焱,刘爱祥,刘宗林,王新强,秦连杰.替代M-型钡铁氧体纳米粒子的微波吸收性能[J].无机化学学报,2002(10):1067-1070. |
[10] | Bidhan C. Roy;Maya Dutta Gupta;Leena Bhoumik .Spectroscopic investigation of water-soluble polyaniline copolymers[J].Synthetic Metals,2002(1):27-33. |
[11] | Oleg P. DImitriev .Confinement of Polyaniline Chains in Thin Layers of the Polymer Solution[J].Journal of Colloid and Interface Science,2001(2):380-382. |
[12] | Deng JG.;Ding XB.;Zhang WC.;Peng YX.;Wang JH.;Long XP.;Li P.;Chan ASC. .Magnetic and conducting Fe3O4-cross-linked polyaniline nanoparticles with core-shell structure[J].Polymer: The International Journal for the Science and Technology of Polymers,2002(8):2179-2184. |
[13] | Deng J;HE C;PENG Y et al.Magnetic and conductive Fes 04-Polyaniline nanoparticles with core-shell structure[J].Synthetic Metals,2003,139(02):295-301. |
[14] | 曾幸荣 .导电性聚苯胺的化学法合成、结构、掺杂、性能及锌-聚苯胺二次电池的研究[D].华南理工大学,1989. |
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