采用机械合金化+热压工艺制备了Laves相NbCr2增强的Nb基复合材料.研究了Nb-22.5Cr配比成分的Nb,Cr元素粉经MA 30h后在1250℃分别热压10min,20min和30min所获得的Nb/NbCr2复合材料的组织和性能.结果表明:三种热压时间均可制备出组织均匀,致密度高的Nb/NbCr2复合材料,体积分数约为30%的近等轴状的Laves相NbCr2颗粒弥散分布于Nb固溶体基体中.热压20min的试样具有最佳的组织和性能,其Laves相NbCr2的晶粒尺寸达到亚微米级,致密度达到99.2%,维氏硬度为9.41GPa,屈服强度为2950 MPa,抗压强度为3345 MPa,塑性应变达到了7.01%,充分实现了Laves相NbCr2颗粒强化和细晶强韧化的效果.
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