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利用金相显微镜(OM)、X衍射(XRD)、扫描电镜(SEM)和能谱(EDS)等测试设备分析了微量硼元素对Nb-40Ti-15Al合金的晶粒细化作用以及硼在晶粒内和晶界的分布情况.结果表明,当合金中硼含量高于0.5%(质量分数)时,晶粒细化开始变得显著,预期对合金的低温脆性有一定程度的改善效果.背散射电子像(BSE)显示硼元素大量富集在晶界上,从而得出硼的细晶作用主要缘于其在合金的B2/β相基体中固溶度甚小,从而导致凝固前沿成分过冷.

参考文献

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