SnO2纳米棒的固相反应制备与表征

功能材料与器件学报 , 2006, 12(1): 10-14. doi: 10.3969/j.issn.1007-4252.2006.01.003

SnO2纳米棒的固相反应制备与表征

赵鹤云 ^1, , 柳清菊 ^2, , 吴兴惠 ^3, , 赵怀志 ^4,

1.昆明理工大学材料与冶金工程学院,昆明,650093;云南大学材料科学与工程系,昆明,650091

2.云南大学材料科学与工程系,昆明,650091

3.云南大学材料科学与工程系,昆明,650091

4.昆明贵金属研究所,昆明,650022

基金项目: 云南省教育厅资助项目(04Z205A) 云南大学校科研和教改项目(2003Q003A) 云南大学校科研和教改项目国家科技攻关项目(2002AA327090)

关键词：固相反应 , SnO2纳米棒 , 熔盐介质

Synthesis and characterization of SnO2 nanorods prepared by solid state reaction

利用室温固相反应方法,合成了SnO2纳米颗粒前驱物.在NaCl、KCl等熔盐介质中,在600～785℃对前驱物进行焙烧,前驱物纳米颗粒自组装生长形成SnO2纳米棒.利用TEM、XRD和XPS对SnO2纳米棒形貌、成分进行了表征和分析,SnO2纳米棒直径为20～80 nm,长度从几百纳米到几个微米.研究了SnO2纳米颗粒前驱体熔盐介质中的生长,探讨了SnO2纳米颗粒在熔盐介质中的固相转变生长机理.

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SnO2纳米棒的固相反应制备与表征

Synthesis and characterization of SnO2 nanorods prepared by solid state reaction

参考文献