用TEM对640℃渗氮油淬,225℃等温3.5h的工业纯铁进行分析,观察部位的含氮量(w)约为2.2%～2.4%.在"未分解”的奥氏体选区衍射花样中γ＇-Fe4N和γ-Fe已明显分离为两套独立的斑点,在(200)γ＇的暗场像中显示出在高氮奥氏体内析出高密度纳米级沉淀γ＇,其平均尺寸约10nm,析出物之间的间距亦为纳米级.根据实验观察结果,提出用热处理方法制备大体积纳米材料的途径.
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