采用Gleeble-1500D热模拟机,研究电场作用下预设升温速度对55wt%(Ti+C)-45wt%Fe体系在从室温加热至800℃过程中燃烧合成的影响,结果表明:预设升温速度对体系燃烧合成有较大影响,当预设升温速度为5℃/s时,不能实现燃烧合成;而在10~1500℃/s范围内,体系能实现燃烧合成,且点火温度大幅度降低,在336~742℃之间;随预设升温速度提高,点火温度降低,点火延迟时间缩短;合成产物主要由TiC、Fe和少量C组成,且随预设升温速度提高,TiC颗粒变小,并出现少量Fe2 Ti,但较低和过高的预设升温速度的合成产物中不会出现Fe2Ti.
参考文献
[1] | Subrahmanyam J;Vijayakumar M .Review:self-propagating high-temperature synthesis[J].Journal of Materials Science,1992,27:6249-6273. |
[2] | 傅正义.SHS技术研究进展--纪念SHS技术诞生三十周年[J].复合材料学报,2000(01):5-10. |
[3] | Alexander G. Merzhanov .SHS processes in microgravity activities: first experiments in space[J].Advances in Space Research: The Official Journal of the Committee on Space Research(COSPAR),2002(4):487-495. |
[4] | Z. A. Munir .The effect of external electric fields on the nature and properties of materials synthesized by self-propagating combustion[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2000(2):125-137. |
[5] | Grave O A;Munir Z A .The effect of an electric field on the microstructural development during combustion synthesis of TiN-TiC composites[J].Journal of Alloys and Compounds,2002,340:79-87. |
[6] | 冯可芹,杨屹,沈保罗,杨春楣,郭路宝,何洪.电场作用下Fe含量对Fe-Ti-C体系低温燃烧合成的影响[J].稀有金属材料与工程,2004(02):161-165. |
[7] | Feng Keqin,杨屹,沈保罗,林慧敏,何洪.电场作用下压坯密度对Fe-Ti-C体系低温燃烧合成的影响[J].稀有金属材料与工程,2005(03):479-482. |
[8] | 蔡泊獯.固体物理基础[M].北京:高等教育出版社,1990:63. |
[9] | Chen Wayne.Gleeble System and application[M].New.York,USA:Gleeble System School,1998:52-54. |
[10] | Lee W C;Chung S L .Ignition phenomena and reaction mechanisms of the self-propagation high-temperature synthesis reaction in the Ti + C system[J].Journal of Materials Science,1995,30:1478-1494. |
[11] | Saidi A;Chrysanthou A et al.Characterizes of the combustion synthesis of TiC and Fe-TiC composites[J].Journal of Materials Science,1994,29:4993-4998. |
[12] | Y.S.Shi,S.C.Chen,X.L.LU,S.H.Huang.IGNITING SHS BY LASER AND ITS APPLICATION TO SELECTIVE LASER SINTERING OF METALLIC POWDER MATERIAL[J].金属学报(英文版),2004(05):694-704. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%