欢迎登录材料期刊网

材料期刊网

高级检索

利用扫描电镜(SEM)、激光粒度分析仪(LDPSA)、X射线衍射仪(XRD)以及比表面积分析仪(SSA)等检测方法,研究了烧结对于羟基磷灰石微球的微观结构、形貌以及粒径、比表面积和孔隙率等性能的影响.结果表明,经800℃热处理,微球的比表面积、孔隙率及其表面形貌均会发生明显的变化;经1000℃烧结后,部分羟基磷灰石相发生热分解,生成较多的的杂质相,如α-磷酸三钙(α-TCP)和β-磷酸三钙(β-TCP).

参考文献

[1] T S PRADEESH;M C SUNNY;H K VARMA .Preparation of microstructured hydroxyapatite microspheres using oil in water emulsions[J].Bulletin of Materials Science,2005(5):383-390.
[2] Starling L B;Stephan J E .Calcium phosphate microcarriers and microspheres[P].US 6358532
[3] Nasser Y. Mostafa .Characterization, thermal stability and sintering of hydroxyapatite powders prepared by different routes[J].Materials Chemistry and Physics,2005(2/3):333-341.
[4] pramanik S;Agarwal A K;Rai K N;Garg A .Development of high strength hydroxyapatite by solid-stste-sintering process[J].Ceramics International,2006,xxx:xxx.
[5] Bailliez S;Nzihon A .The kinetics of surface area reduction dining isothermal sintering of hydroxyapatite adsorbent[J].Chemical Engincering Journal,2004,98:141-152.
[6] El Shafei GMS;Philip CA;Moussa NA .Fractal analysis of hydroxyapatite from nitrogen isotherms[J].Journal of Colloid and Interface Science,2004(2):410-416.
[7] Bhattacharjee S;Swain SK;Sengupta DK;Singh BP .Effect of heat treatment of hydroxyapatite on its dispersibility in aqueous medium[J].Colloids and Surfaces, A. Physicochemical and Engineering Aspects,2006(1/3):164-170.
[8] Haberko K;Bunko M M;Brzezi(n)ka-Miecznik J;Haberko M Mozgawa W Panz T Pyda A Zarebski J .Natural hydroxyapatite-its behaviour during heat trentment[J].Journal of the European Ceramic Society,2006,26:537-542.
[9] Patel N;Gibson I R;Ke S;Best S M Bonfield W .Calcining influence on the powder properties of hydroxyapatite[J].Jonrnal of materials:materials in medicine,2001,12:181-188.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%