综述了阻燃剂 9, 10-二氢-9氧杂-10-膦杂菲-10-氧化物( DOPO)的制备过程,对每一步中间产品的制备方法做了详细的评述 ,着重对反应过程物料配比、反应温度、反应时间、体系压力等工艺参数以及提纯方法进行了比较、分析,提出了建议.
参考文献
| [1] | Annakurtty K S;Kishore K.Flame retardant polyphosphate esters:1.Condensation polymers of bisphenols with aryl phosphorodichloridates:Synthesis,characterization and ther- mal studies[J].POLYMER,1988(29):756-761. |
| [2] | Kishore K;Annakurtty K S;Mallick I M .Flame retardant polyphosphate esters:2.Condensation polymers of bisphenol A with alkyl phosphorodichloridates:Synthesis,characteriza- tion and thermal studies[J].Polymer,1988,29:762-766. |
| [3] | Shui-Yu Lu;Ian Hamerton .Recent developments in the chemistry of halogen-free flame retardant polymers[J].Progress in Polymer Science,2002(8):1661-1712. |
| [4] | 白景瑞,滕进.阻燃剂的应用与研究进展[J].宇航材料工艺,2001(02):10-12,55. |
| [5] | 黄汉生.日本非卤素阻燃剂发展动向[J].现代化工,2002(12):52-55. |
| [6] | 欧育湘.国外阻燃剂发展动态及对发展我国阻燃剂工业之浅见[J].精细与专用化学品,2003(02):3-6. |
| [7] | 尹国强,廖列文,康正.塑料阻燃剂的合成研究进展[J].应用化工,2003(04):12-15. |
| [8] | 李响,钱立军,孙凌刚,周政懋.阻燃剂的发展及其在阻燃塑料中的应用[J].塑料,2003(02):79-83. |
| [9] | 鹿海军,马晓燕,颜红侠.磷系阻燃剂研究新进展[J].化工新型材料,2001(12):7-10. |
| [10] | 贺峥杰;陈文彬;唐除痴 .有机磷阻燃剂研究进展[J].化学工业与工程,1997,14(03):43-49. |
| [11] | Chang SJ.;Chang FC. .Characterizations for blends of phosphorus-containing copolyester with poly(ethylene terephthalate)[J].Polymer engineering and science,1998(9):1471-1481. |
| [12] | 蒋建中,蔡春.新型阻燃剂中间体DOPO合成与应用概述[J].江苏化工,2004(01):12-15,39. |
| [13] | Chun Shan Wang;Ching Hsuan Liu .Synthesis and Properties of Phosphorus-Containing Epoxy Resins by Novel Method[J].Journal of Polymer Science, Part A. Polymer Chemistry,1999(21):3903-3909. |
| [14] | LIU Y L.Flame retardent epoxy resins from novel phos- phorus-containing novolac[J].POLYMER,2001(42):3445-3454. |
| [15] | Liu YL.;Wu CS.;Hsu KY.;Chang TC. .Flame-retardant epoxy resins from o-cresol novolac epoxy cured with a phosphorus-containing aralkyl novolac[J].Journal of Polymer Science, Part A. Polymer Chemistry,2002(14):2329-2339. |
| [16] | WANG CHUN SHAN .Synthesis and Properties of Phosphorus Containing Advanced Epoxy Resins[J].Journal of Applied Polymer Science,2000(3):429-436. |
| [17] | Wang C S;Shieh J Y .Synthesis and flame retardancy of phosphorus containing polycarbonate[J].Journal of Polymer Research,1999,6(03):149-154. |
| [18] | 杨锦飞;丁海嵘.磷系阻燃剂现状与展望[J].江苏化工(27):1-6. |
| [19] | 张治华.新型无卤阻燃技术[J].塑胶工业,2002(05):7-9. |
| [20] | Liu YL. .Epoxy resins from novel monomers with a bis-(9,10-dihydro-9-oxa-10-oxide-10-phosphaphenanthrene-10-yl-) substituent[J].Journal of Polymer Science, Part A. Polymer Chemistry,2002(3):359-368. |
| [21] | 陈红,吴良义.磷系阻燃环氧树脂与固化剂[J].热固性树脂,2002(01):39-43. |
| [22] | Wang CS.;Sun YM.;Shieh JY. .Synthesis and properties of phosphorus containing PET and PEN (I)[J].Journal of Applied Polymer Science,1998(10):1959-1964. |
| [23] | Wang C S;Liu Y L;Chiu Y S.Preparation of phosphorus -containing poly(epichlorohydrin)and polyurethane from a novel synthesis route[J].Journal OF APPLIED POLYMER SCIENCE,2002(85):2254-2259. |
| [24] | Wang CS.;Chen CY.;Lin CH. .Synthesis and properties of Phosphorus-Containing Polyesters Derived from 2-(6-oxido-6H-dibenz{c,e}{1,2}oxaphosphorin-6-yl)-1,4-hydroxyethoxy phenylene[J].Journal of Polymer Science, Part A. Polymer Chemistry,1998(17):3051-3061. |
| [25] | Wang C S;Lin C H.Synthesis and properties of phospho- rus containing polyarylates derived from 2- (6-oxid-6H- dibenz〈 c,e〉〈 1,2〉 oxaphosphorin-6-yl)-1,4-dihydroxy phenylene[J].POLYMER,1999(40):4387-4398. |
| [26] | Liou GS.;Hsiao SG. .Synthesis and properties of aromatic poly(ester amide)s with pendant phosphorus groups[J].Journal of Polymer Science, Part A. Polymer Chemistry,2002(4):459-470. |
| [27] | Chun Shan Wang;Ching Hsuan Lin .Synthesis and properties of phosphorus-containing PEN and PBN copolyesters[J].Polymer: The International Journal for the Science and Technology of Polymers,1999(3):747-757. |
| [28] | Wang XD.;Zhang Q. .Synthesis, characterization, and cure properties of phosphorus-containing epoxy resins for flame retardance[J].European Polymer Journal,2004(2):385-395. |
| [29] | Lin C H;Wang C S.Novel phosphorous-containing epoxy resins partⅠ.synthesis and properties[J].POLYMER,2001(42):1869-1878. |
| [30] | 马庆丰,康惠宝,王利生.新型阻燃剂中间体9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物的合成[J].精细石油化工进展,2002(01):46-48. |
| [31] | Buysch H J;Glock V;Griehsel B et al.Process for preparing 6-oxo-(6H)-dibens- [c,e][1,2]- oxaphosphorins (ODOPS)[P].US 5560530,1997-07-22. |
| [32] | Saito T;Hirayama T;Kohguchl Y .Process for producting 2-(2-hydroxyphenyl) phenylphosphinic acid and derivatives[P].US 6107506,2000-08-22. |
| [33] | Rathfelder P;Rieckert H;Dietrich J .Process for the per- parition of a DOP-containing mixture[P].DE:19322876,1998-10-13. |
| [34] | 熊友情,康惠宝,王利生.一种新型含磷阻燃剂的合成[J].应用化工,2003(02):41-43. |
| [35] | 吴宝庆,果学军,吴茫.涤纶磷系共聚阻燃剂及阻燃聚酯制备方法[J].合成纤维工业,2002(06):39-40. |
| [36] | Wang CS.;Shieh JY. .Synthesis and properties of epoxy resins containing 2-(6-oxid-6H-dibenz[c,e][1,2]oxaphosphorin-6-yl)1,4-benzenediol[J].Polymer: The International Journal for the Science and Technology of Polymers,1998(23):5819-5826. |
| [37] | Kleiner H J .Method for preparing 6H-dibenzo[c,e][1,2]oxaphosphorin-6-one[P].US 5481017,1996-02-02. |
| [38] | 果学军,娄颖,吴宝庆,吴茫.新型含磷化合物膦菲的开发与应用[J].化工时刊,2001(02):5-10. |
| [39] | 王良恩;吴燕翔;朱跃资 .缩聚磷酸苯酯的研制[J].福州大学学报(自然科学版),1995,23(01):89-91. |
| [40] | 程能林.溶剂手册[M].北京:化学工业出版社,1994:249-251. |
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