欢迎登录材料期刊网

材料期刊网

高级检索

透明YAG陶瓷具有较好的化学稳定性、光学性能和高温性能,是单晶激光材料的有力替代品,纳米YAG粉体的合成有利于制备性能优异的YAG透明陶瓷.采用低温燃烧法,以Y2O3、Al(NO3)3·9H2O、柠檬酸、乙二醇为原料,采用TG/DSC, XRD和SEM等测试手段对YAG前驱体进行表征,对YAG前驱体在不同温度下进行煅烧.结果发现,在900 ℃左右已完全转变成YAG相,最终获得单分散、无团聚、形状规则的YAG纳米粉体.

参考文献

[1] Li Ji-guang;Lee Jong-heun;Mori T .Crystal phase and sinter ability of wet-chemicaly derived YAG powders[J].Ceram Soc Japan,2000,108(05):439-444.
[2] Ikesue A.;Kamata K.;Furusato I. .FABRICATION OF POLYCRYSTALLINE, TRANSPARENT YAG CERAMICS BY A SOLID-STATE REACTION METHOD[J].Journal of the American Ceramic Society,1995(1):225-228.
[3] Ikesue A.;Kamata K.;Yoshida K.;Kinoshita T. .FABRICATION AND OPTICAL PROPERTIES OF HIGH-PERFORMANCE POLYCRYSTALLINE ND-YAG CERAMICS FOR SOLID-STATE LASERS[J].Journal of the American Ceramic Society,1995(4):1033-1040.
[4] Zhang Y M;Yu H M .Synthesis of YAG powders by co-precipitation method[J].Ceramics International,2009,35:2077-2081.
[5] Wen L;Sun X D;Xiu Z M et al.Synthesis of nanocrystalline yttria powderand fabrication of transparent YAG ceramics[J].European Ceramic Society,2004,24:2681-2688.
[6] Veith M;Mathur S;Kareiva A et al.Low temperature synthesis of nanocrystalline YAG and Ce-doped YAG via different sol-gel methods[J].Matar Chem,1999,9:306-3079.
[7] Sim S M;Keller K A .Phase formation in YAG powder synthesized by chemical methods[J].Materials Science,2000,35:713-717.
[8] Hreniak D;Strek W .Synthesis and optical properties of Nd:YAG nanoceramics[J].Journal of Alloys and Compounds,2002,341:183-186.
[9] Xudong Zhang;Hong Liu .Synthesis of monodisperse and spherical YAG nanopowder by a mixed solvothermal method[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,2004(1/2):300-303.
[10] M. B. Kakade;S. Ramanathan;P. V. Ravindran .Yttrium aluminum garnet powders by nitrate decomposition and nitrate-urea solution combustion reactions - a comparative study[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,2003(1/2):123-129.
[11] Shi SK.;Wang JY. .Combustion synthesis of Eu3+ activated Y3Al5O12 phosphor nanoparticles[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,2001(1/2):82-86.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%