以Mg3Al-CO3-HTLcs水滑石煅烧产物为前驱体,采用焙烧还原法,辅助微波手段合成了纳米Mg3Al-EDT-HTLcs.研究表明,所合成的纳米Mg3Al-EDTA-HTLcs粒径为20～80nm,分散性较好,颗粒团聚少;反应温度为50～100℃、反应时间为0.5～6h、微波晶化时间为5～45min,均能合成出结晶良好、晶相单一的Mg3Al-EDTA-HTLcs.采用该方法均能快速合成出结晶良好的Mg3Al-EDTA-HTLcs.
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