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Nano-silver loaded montmorillonite (Ag-MMT) was prepared by ion-exchange and then a UV-photoreduction two-step approach was applied. The silver content in Ag-MMT determined by Volhard method was about 6.4 wt%. The morphology and structure of as-synthesized Ag-MMT were characterized by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results showed that the Ag nanoparticles were spherical and their diameters were about 15-20 nm. Moreover, the structure of MMT did not change. The minimum inhibition concentration (MIC) of Ag-MMT was 100×10-6 and the sterilizing efficiency (SE) of Ag-MMT was approximately 100% against Escherichia coli ATCC 11229 (E. coli. In addition, the slow release property of silver in Ag-MMT was also demonstrated.

参考文献

[1] B.Concepcion-Rosabal;G.Rodriguez-Fuentes;N.Bogdanchikova;M.Avalos;P.Bosch;V.H.Lara .Comparative study of natural and synthetic clinoptilolites containing silver in different states[J].Microporous and Mesoporous Materials,2005(1/3):249-255.
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